Current situation of the application of ICP - AES for the pharmaceutical analysis in China
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1 Chin J Pharm Anal * ICP - AES R917 A Current situation of the application of ICP - AES for the pharmaceutical analysis in China CHEN Yang JIN Wei YANG Yong - jian * Shanghai Institute for Food and Drug Control Shanghai China AbstractInductively coupled plasma - atomic emission spectrometryicp - AESis a common method for element analysis with many advantages such as low detection limit high accuracy wide dynamic linear range and simultaneous determination of multiple elements etc which has great application potential in pharmaceutical analysis fields. This paper reviews the application situation of ICP - AES in the domestic pharmaceutical analysis mainly including heavy metals in Chinese herbal medicine and Chinese patent medicine elemental impurities in chemical medicine assay of major elements determination of non - metal elements biochemical samples drug metabolism and pharmacokinetics etc and describes the prospect of the development of this technique. Key wordsicp - AESpharmaceutical analysisapplication situationoverviewheavy metal determinationbiochemical samples analysismetal foreign matternonmetals elementpharmacokinetics ICP - AES ICP - AES ICP - MS 1-4 ICP - AES ICP ICP - AES 1ICP ~ 5 5 CCD CID 1 * Tel E - mailyongjianyang@ 163. com
2 908 Chin J Pharm Anal ICP - AES As Cd Cu Fe 8 12 ICP - AES 20 Fe Mn Cu Zn 2000 Ni As Cd Pb ICP - AES Fe Pb Cd As 1 Pb As Cd 4 Hg 5 5 Cd Cd 5 Pb mg kg mg kg mg kg mg kg Pb Cd 0. 1% 2 Cd 6 ICP - MS ICP - AES 7 ICP - AES 18 ICP - AES 5 Cd Hg Pb 3 Zn 8 Cu Cd Pb As 9 Pb Ca Fe Zn Se ICP - AES Cu Pb Cd Pb Cd Cu Mn Ni Pb 10 ICP - AES Pb Cd
3 Chin J Pharm Anal As Ba Cd Cr Cu Pb 6 - Cu Pb As Cd Hg 5 30 ICP - AES 85% 20 K Ca Cu Na Mg Mn Fe Zn Pb Cd ICP - AES 25 Pb Cu Cd Cr ICP - AES ICP - AES 22 ICP - AES 31 < 232 > 4 ICP - AES Pb Cd Cu 32 Q3D 33 ICP - AES ICP - AES Al Mn Ni 3 ICP - AES ICP - AES HNO 3 - HClO 4-13 Ca Cu Zn Fe Mg Mn Pb 15 ICP - AES Cu Pb Zn As Sb Cd Hg Au Cu Pb Pb Cr Cd As Ag Pd Cd HCl - HNO Cu Al Pb 3 38 ICP - AES
4 910 Chin J Pharm Anal / ICP - AES 19 2 ICP - AES ICP - MS ICP - AES ICP - AES 40 ICP - AES 47 Pb As ICP - AES Hg ICP - AES ICP - AES H C N O F Cl 42 ICP - AES ICP - AES Mg Ca Cu Fe Mn K Zn Cr P Mo ICP - AES 51 - Si % 52 ICP - AES I 45 Ag ICP - AES nm I - I 2 46 ICP - MS ICP - AES 4 48 ICP - AES 2 2 ICP - AES 43 ICP - AES 49 ICP - AES B Mg Al B ICP - AES mg L - 1 B 50 B I μg g - 1
5 Chin J Pharm Anal ICP - AES ± 16. 2% D ICP - AES 59 ICP - AES 54 Pb Cr Cd As Hg % ~ % RSD 0. 5% ~ 1. 6% 6 - Zn - FDP Zn - 55 Zn - FDP - Zn - G 4 ICP - AES Zn Zn - FDP Hg Zn - G Zn - G Hg nm Zn - FDP 6 t 60 ICP - AES 1 G 61 ICP - AES Al ICP - AES 56 - / nm Al 96. 0% ~ 99. 5% 8 6 h ICP - AES Al PKS Al 2 Al 7 P < Gd - DTPA 57 Gd - DTPA - / - Gd - DTPA 58 ICP - AES Gd mg D 8 ICP - AES 0 ~ 24 ICP - AES h
6 912 Chin J Pharm Anal Cui - ying ICP - AES ICP - AES TANG Bo 1 XIN Ren - xuan. Analysis of Inductively Coupled Plasma - al. Determination of six harmful trace elements in Fructus Corni by Atomic Emission Spectrometry. Beijing ICP - OES Chemistry Industry Press Anhui Med Pharm J 2 GU Guo - ying. Historical development and basic properties of ICP - AESICP - AES. Spectrosc 15 ZHAO Ai - hong WANG Jian - hua SONG Spectral Anal Zhi - gang et al. Study on the determination of Cd and Pb 3 HE Jin - zhe. Application of ICP - AES in element analysisicp in Radix Salviae Miltiorrhizae by ICP - AESICP - AES - AES. J Zhejiang. Spectrosc Spectral Anal Univ Technol SHI Jing - yan LI Zhen - hai. Application of 16 JIN Hang WANG Yuan - zhong YANG Wei - ze ICP - AES Method in Chemical Analysis et al. Study on the determination of Cd and Pb in Genti- rigescens Franch. by ICP - AES -. Hebei Electric Powerana s 43 5 Ministry of Foreign Trade and Economic Cooperation PRC. Green Industry Standards of Medicinal Plants and Preparations for the Import and Export ChP VolⅠ Appendix 43 7 LI Chun - xiang WANG Ling - ling JING Jun - jie et al. Simultaneous determination of the contents of Cd Hg and Pb in traditional Chinese medicines by microwave digestion and ICP - AES /ICP - AES ICP - OESICP - OES. J Cd Hg Pb. Chin J Pharm Anal Linyi Norm Univ DI Zhi - guang SONG Wei LIANG Xia et al. Determination of copper cadmium lead and arsenic in the Chinese traditional medicine by microwave digestion and ICP - AES ICP - AES. Mod - ICP - AES Pb Cd. Chin J Ethnomed Ethnopharm WANG Qing - xiao LI Zhen - guo ZHANG et al. Determination of heavy metals and trace elements in Chinese angelica by ICP - AES with microwave digestion - ICP - AES. J Chin Med Mater HAN Min XIONG Fei. Determination of trace elements in blood - activatin and stasis - eliminating herbs by ICP - AES with microwave digestion ICP - AES. Chin J Spectrosc Lab 2010 LIU Xiu - qin. Determination of 5 elements in Ganoderma by ICP - OESICP - OES. Mod Chin Med DING Qing WU Yue XU Yi - liang et Chin J Spectrosc Lab WANG Yun - mei WANG Yuan - zhong ZHAO Zi - xian et al. Study on the determination of Cd and Pb in Rhodiola crenulata by ICP - AES. Lishizhen Med Mater Med Res XU Qing - cai SUN Ai - de JIA Ling - jie. Determination of heavy metals in Rudbeckia hybrida by 19 TANG Rui LI Tian - peng GU Xue - shi et al. Studies on six heavy metal elements dissolution characteristics of Andrographis Herb by ICP - OESICP - OES 6. Spectrosc Spectral A- nal Sci Instrum WANG Ji - yong WANG Yuan - zhong ZENG 9 WANG Geng LIU Qiang. Determination of trace elements in senecio. J Branch Campus First Mil Med Univ Yan et al. Spectrometric determination of trace elements in anticancer new medicine Fagopyrum dibotrys. Spectrosc Spectral Anal 10 CHEN Wang LIN Si - ding ZHANG Liang et al. Determination of Pb Cd in Radix Pseudostellariae and 21 GONG Ai - qin. Determination of Pb Cu Cd and Cr in Rubus Aleaefolius by microwave digestion - ICP - AES Chinese medicine herbs by GFAAS and ICP - AES. Chem Eng FAN Guang - hua WANG Dong. Research on
7 Chin J Pharm Anal ICP - AES determination of lead and cadmium and copper in traditional quirements for Registration of Pharmaceuticals for Human Use. Impu- Chinese medicine ICP - AES rities Q3DGuideline for Metal Impurities. http/ /www. ich. org /. Lab Sci products / guidelines / quality / article / quality - guidelines. html 23 E Er - deng - sang HANG Gai - ba - te - er34 CHI Hai - tao ZHANG Jing - hua ZHOU BA Tu. Determination of trace elements in Mongolian medicine Zidianling Curing Allergic Purpura disease by ICP - AES ICP - AES. Spectrosc Spectral Anal SHI Nan - ning ZHANG Jian - xin XU Luo Chin J Anal Chem s E Er - deng - sang BAO Yin - da - lai HANG Gai - ba - te - er. Determination of trace elements in Mongolian medicine Xirawrel by ICP - AES with microwave digestion. Chin Tradit Pat Med ICP - AES E Er - deng - sang BAO Yin - da - lai NA Ren - ge - ri - le. Determination of trace elements in Mongolian medicine Gardi - 13 by ICP - AES with microwave digestion ICP - AES WU Rong. Determination of Cu Al and Pb in iohexol by. Spectrosc Spectral Anal ICP - AESICP - AES. Chin J Spectrosc Lab LI Xiang - yang ZHU Jun - bo NI Ma - cai - rang et al. Determination of four metal elements in Tibetan medicine Zuotai by ICP - AES with microwave digestion ICP - AES 4. Chin Tradit Pat Med LONG Qi - fu LI Xiang - yang ZHU Jun - bo ICP - AES 40 ZHANG Yi - min JIANG Hui L Xue - bin. Determination of four metal elements in Tibetan medicine twenty - five - sort Songshiturquoisepills by ICP - AES with microwave digestion. Chin J Ethnomed Ethnopharm WAN Yi - qun YU Xiao - ran. Determination of lead chromium cadmium arsenic in danggui blood - supplementing decoction by inductively coupled plasma atomic emission spec- 41 GONG Xian - ling JIE Xin - ming XU Mei - trometry yi. Analysis of trace elements from carrageenan. J Anal Sci Tianjing Pharm 29 XU Yi - liang LIU Ai - qin. Determination of heavy metals and baneful elements in Flos Chrysanthemi and its pre- 42 WANG Xin - mei LI Li - min WANG Ke scription granule by ICP - OESICP - OES et al. ICP - OES simultaneous determination of 10 elements in. Mod Chin Med multivitamin and minerals drugsicp - OES Chin J Pharm Anal 30 SHI Nan - ning TONG Zheng - ben GONG Xiao - qing. Determination of organic germanium in 43 ZHENG Yong - jun CHEN Ming - yu YANG Fuzheng mixture by ICP - AES Guang et al. Determination of Mg and Al in Weishuping by. J Nanjing Railway Med CollICP - AES. J Jining Med Univ European Medicines Agency. Guideline on the specification limits for residues of metal catalysts or metal reagents. Doc. Ref. EMEA / CHMP /SWP /4446 / WANG Shui - feng GUO Jing - hua. Determination of Gd in dimeglumine gadopentetate injection by ICP - AES 32 U. S. Pharmacopeia. < 232 > Elemental impurities - limits. Pharma-. Chin J Anal Lab s 408 copoeia Forum Volume No http/ /www. usppf. com / pf /pub /index. html 33 The International Conference on Harmonisation of Technical Re- Ming - qiang et al. Study on Al Mn and Ni in caffeine by ICP - OESICP - OES Al Mn Ni. sheng. Determination of residual palladium in medicine by inductively coupled plasma - atomic emission spectrometry. Chin J Pharm 36 LIU Wei FANG Wei. Determination of Cu Pb Zn As Sb and Cd in artemether by ICP - AESICP - AES Cu Pb Zn As Sb Cd. Chin J Spectrosc Lab LI Guang - li XU Guang HE Jiao et al. Determination of trace Ag Pd and Cd in the anticancer medicine of oxaliplatin by ICP - AESICP - AES. Precious Metals CHEN Yang YANG Yong - jian. Determination of 19 elemental impurities in iohexol by ICP - AESICP - AES 19. Chin J Spectrosc Lab et al. Determination of lead and arsenic contents in amylum by ICP - AES methodologyicp - AES. Spectrosc Spectral Anal LI Ming - chun ZHAO Li - yan MA Shou - dong et al. Content determination of silver in nanometer silver gel by inductively coupled plasma - atomic emission spectrom-
8 914 Chin J Pharm Anal etry China Pharm LIU Li - juan ZHAO Guo - xiong ZHOU Jian 46 XU Feng - hua OUYANG Li LIU Ya - qiong. ICP - AES determination of carboplatin in polylactic - yeast hepatitis B vaccine by ICP - AES coglycolic acidmicrospheres by ICP - MS ICP - AES - /. Chin Pharm Aff Chin J Pharm Anal YING Yi ZHOU Shi - wen TANG Jian - lin 47 FAN Zhe - feng. Indirect determination of phenobarbital by ICP - AES using mercury nitrate as a precipitating agent ICP - AES. J Shanxi. Chin J Hosp Pharm Norm Univ CHEN Hong ZHANG Yi ZHU Rong. Determination 57 YING Yi ZHOU Shi - wen TANG Jian - lin of phosphate in electrolyte injection et al. Study on pharmacokinetics of carboplatin - poly D L -. West China J Pharm Sci 2007 lactide /glycolide microcapsules in mice - / JIN Hang WANG Yuan - zhong YANG Mei - quan et al. Determination of boron in gentiana rigescens Franch. by inductively coupled plasma atomic emission spectrometry ICP - AES. Chin J Pharm Anal LI Ya - nan. Study on boron in boric acid and zinc oxide ointment by ICP - AESICP - AES 59 LI Tie - fu WANG Yu - qing JIN Jie. Chin J Mod Drug Appl 2010 et al. Distribution and pharmacokinetics of Gd - DTPA liposomes in ZHUANG Xiao - hong ZHENG Ping. Determination of Si in osteoform compound calcium acid chelate capsule dissol- Shenyang Pharm Univ LUO Huan - min WANG Cheng - qi GAO ving in NaOH by ICP - AESICP - AES Qin et al. Comparison of zinc gluconate and zinc fructose -. West China J Pharm Sci diphosphate on pharmacokinetics in mice WANG Chun - mei ZHANG Shu - zhen WU Qiong et al. Study on the determination of iodine by ICP - AES. Spectrosc Spectral Anal YANG Ye - mei HE Yu - ping CHEN Jin - su et al. Determination of cisplatin or carboplatin in blood by ICP - AESICP - AES. Chin J Health Lab Technol ZHANG Ting - hong ZHOU Zhi - yong. ICP - AES determination of heavy metal elements in pancreatin materials ICP - AES. Chin J Pharm Anal et al. Determination of thimerosal content in recombinant. Distribution of carboplatin - poly D L - lactide /glycolidem icrocapsules in mice - /. Acta Acad Med Mil Tert ZHAO Li - mei CHEN Ming GUO Shan - bin et al. Relative bioavailability of compound cacium carbonate granules in healthy volunteers. Chin J Hosp Pharm mice. J. Chin J Clin Pharmacol Ther LI Yan ZHU Zhao - jing. Determination of Al of sucralfate in stomachs of rats by ICP - AESICP - AES. Chin J Spectrosc Lab RONG Li - na ZHANG Min XU Yun - long et al. Study on entrapment efficiency of paramagnetic liposomes. Chin J Pharm A- nal
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ANALYSIS REPORT CONTACT: Ann Eastman
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