SUPPLEMENTARY DATA. Waste-to-useful: Biowaste-derived heterogeneous catalyst for a green and sustainable Henry reaction
|
|
|
- Ἀριστοφάνης Καλογιάννης
- 5 χρόνια πριν
- Προβολές:
Transcript
1 Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 209 SUPPLEMENTARY DATA Waste-to-useful: Biowaste-derived heterogeneous catalyst for a green and sustainable Henry reaction Kalyani Rajkumari, Diparjun Das, Gunindra Pathak and Lalthazuala Rokhum * Department of Chemistry, National Institute of Technology Silchar, Silchar-0, Assam, India * Corresponding author. Tel.: ; fax: ; address: lalthazualarokhum@gmail.com; rokhum@che.nits.ac.in (L. Rokhum) Table of Contents XRF data of metallic and non-metallic concentration in recovered MAPA catalyst (Table S) 2 XPS survey and deconvulated spectra of Recovered MAPA catalyst (Fig: S) 3 EDX spectra and TEM-SEM images of the recovered MAPA catalyst (Fig: S2, S3) 4 Calculation of Atom economy and E-factor 5 Spectral data H NMR and 3 C NMR Spectra of 2-nitro--(4-nitrophenyl)ethanol (3a) H NMR and 3 C NMR Spectra of 2-Nitro--(2-nitrophenyl)ethan--ol (3c) H NMR and 3 C NMR Spectra of 2-nitro--(3-nitrophenyl)ethanol (3d) H NMR and 3 C NMR Spectra of -(4-Fluorophenyl)-2-nitroethan--ol (3e) H NMR and 3 C NMR Spectra of -(4-Chlorophenyl)-2-nitroethan--ol (3f) H NMR and 3 C NMR Spectra of -(4-Bromophenyl)-2-nitroethan--ol (3g) H NMR and 3 C NMR Spectra of -(4-methoxyphenyl)-2-nitroethan--ol (3h) H NMR and 3 C NMR Spectra of 2-nitro--(3,4,5-trimethoxyphenyl)ethan--ol (3j) H NMR and 3 C NMR Spectra of 2-Nitro--(p-tolyl)ethan--ol (3k) H NMR and 3 C NMR Spectra of -Nitropentan-2-ol (3l) H NMR and 3 C NMR Spectra of 6-((tert-butyldimethylsilyl)oxy)--nitrohexan-2-ol (3m)
2 H NMR and 3 C NMR Spectra of 2-Nitro--(4-nitrophenyl)propan--ol (3o) H NMR and 3 C NMR Spectra of 2-Nitro--(3-nitrophenyl)propan--ol (3p) H NMR and 3 C NMR Spectra of -(4-Chlorophenyl)-2-nitropropan--ol (3q) H NMR and 3 C NMR Spectra of 4-(-Hydroxy-2-nitropropyl)benzonitrile (3r) H NMR and 3 C NMR Spectra of -(2-Bromophenyl)-2-nitropropan--ol (3s) H NMR and 3 C NMR Spectra of 2-Nitro--(p-tolyl)propan--ol (3t) H NMR and 3 C NMR Spectra of 2-nitrohexan-3-ol (3u) H NMR and 3 C NMR Spectra of 5,9-Dimethyl-2-nitrodec-8-en-3-ol (3v) H NMR and 3 C NMR Spectra of 2-nitro-7-((tetrahydro-2H-pyran-2-yl)oxy)heptan-3-ol (3w)- 34 Table S: Metallic and non-metallic concentration in recovered MAPA after 0 th recyclability test as given by XRF analysis. Sl No Name of the % Mass fraction in fresh % Mass fraction in component in the MAPA recovered MAPA MAPA sample after 0 th recycles.. K 2 O SiO CaO P 2 O SO MgO Fe 2 O Al 2 O MnO CuO
3 Fig: S a) XPS survey spectrum, b) Cs, c) Os, d) K2p spectra of recovered MAPA. 3
4 Fig. S2: EDS analysis of the recovered catalyst (after 0 th cycle). Fig S3: a-b) TEM and b-c) SEM images of the recycled catalyst. 4
5 Calculation of Atom Economy and E-factor: Atom economy= = Mass of atoms in desired product Mass of atoms in reactant 0.22g ( )g 00% = 00% Total waste (g) E-factor = Product (g) Mass in the process= Aldehyde + Nitroalkane + Catalyst = ( ) g = g Product = g Total waste = ( ) g = g g E-factor = g = 0.5 Spectral data: 2-Nitro--phenylethanol (Table 4, entry 3a) 3a 5
6 Colorless oil, H NMR (400 MHz, CDCl 3 ): δ 2.68 (s, H), δ (m, 2H), δ (m, H), δ (m, 5H). 3 C NMR (00 MHz, CDCl 3 ): δ 73.08, 77.7, 3.65, 7.63, 27.4, 35.08; IR (KBr pellet, ν max /cm - ): 3429, 308, 2408, 553, 433, 22, 035, 963, 777, nitro--(4-nitrophenyl)ethan--ol (Table 4, entry 3b) O 2 N 3b Brown solid, H NMR (CDCl 3, 400 MHz): δ 3.62 (H, s), δ 4.6 (2H, d, J= 40 Hz), δ 5.62(H, m), δ 7.6 (2H,d, J=8Hz), δ 8.2 (2H, d, J=7.6 Hz); 3 C NMR (CDCl 3, 25 MHz): δ 69.98, 80.67, 24.3, 27.0, 45.3, 47.95; IR (KBr pellet, ν max /cm - ): 3320, 3075, 2965, 2885, 608,532, 508, 430, 358, 320, 2, 058, 765, Nitro--(2-nitrophenyl)ethan--ol (Table 4, entry 3c) 3c Oily liquid, H NMR (CDCl 3, 400 MHz): δ (m, H), δ 4.87 (H, d, J=3.6 Hz), δ 6.05 (H, d, J=9.2 Hz), δ 7.56 (H, t, J= 8Hz), δ 7.97 (H, d, J=7.6), δ 8.07 (H, d, J=8Hz), δ 8.3 (H, d, J=7.6 Hz), 3C-NMR (00 MHz, CDCl3, TMS): d 34.37, 34.6, 33.8, 3.3, 29.64, 28.77, 24.95, 66.79; IR (KBr pellet, ν max /cm - ): ν 3305, 3025, 2939, 2889, 2787, 553, 432, 379, 323, 28, 78, 2,
7 2-nitro--(3-nitrophenyl)ethanol (3d) O 2 N 3d Yellow solid, H NMR (CDCl 3, 400 MHz): δ.25 (H, s), δ (2H, m), δ (H, m), δ7.6 (H, t, J=8 Hz), δ7.79 (H, d, J=8 Hz), δ8.9 (H, d, J=8 Hz), δ8.3 (H, s); 3 C NMR (CDCl 3, 25 MHz): δ 69.84, 80.7, 2.4, 23.77, 30.4, 32.5, 40.35, 48.45; IR (KBr pellet, ν max /cm - ): ν 3304, 3075, 2956, 2870, 62,545, 5, 437, 368, 329, 095, 058, 775, (4-Fluorophenyl)-2-nitroethan--ol (3e) F 3e Light yellow liquid, H NMR (CDCl 3, 400 MHz): δ 2.92 (H, s), δ (H, m), δ (H, m), δ 4.78 (H, t, J=6.8 Hz), δ (m, H), δ 7.2 (2H, d, J=8.4 Hz), (H, dd, J=8 Hz), δ (H, dd, J= 8 Hz); 3C-NMR (00 MHz, CDCl 3, TMS): δ 6.66, 33.86, 27.74, 6.4, 5.93, 70.32; IR (KBr pellet, ν max /cm - ): ν 3425, 302, 2909, 200, 704, 526, 32, 879, (4-Chlorophenyl)-2-nitroethan--ol (3f) Cl 3f 7
8 Colorless liquid, H NMR (CDCl 3, 400 MHz): δ 2.57 (H, s), δ 4.56 (H, d, J= 3.6Hz), δ 4.80 (H, t, J= 7.2 Hz), δ (H, m), δ 7.8 (2H, d, J=8.4 Hz), δ 7.35 (H, d, J=8.4 Hz); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 70.29, 27.37, 29.8, 28.80, 32.67, 38.37; IR (KBr, ν max /cm - ): 3408, 3035, 2979, 2989, 2756, 536, 428, 389, 326, 275, 85, 5, 840, (4-Bromophenyl)-2-nitroethan--ol (3g) Br 3g Pale yellow oil, H NMR (CDCl 3, 400 MHz): δ 2.03 (H, s), δ (H, m), δ 4.79 (H, t, J= 7.2 Hz), δ (H, m), δ 7.29 (2H, d, J=8.4 Hz), δ 7.54 (H, d, J=8.4 Hz); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 70.33, 22.89, 27.68, 29.2, 32.4, 38.05; IR (KBr pellet, ν max /cm - ): ν345, 3025, 2939, 2889, 2787, 550, 440, 38, 33, 280, 84, 20, (4-methoxyphenyl)-2-nitroethan--ol (3h) MeO 3h Yellow liquid, H NMR (CDCl 3, 400 MHz): δ 2.92 (H, s), δ 3.80 (3H, s), δ 4.46 (H, d, J=2.4 Hz) ; δ 4.58 (H, t, J=0 Hz), δ 5.382(H,d, J=8 Hz), δ 6.90 (2H, d, J= 7.6 Hz), δ 7.30 (2H, d, J=7.2 Hz); 3 C NMR (CDCl 3, 25 MHz): δ 55.35, 70.65, 80.26, 4.35, 27.3, 28.55, 30.55, 59.96; IR (KBr pellet, ν max /cm - ): 3378, 3083, 2943, 2896, 2780, 62, 536, 425, 82, 050, 790,
9 2-nitro--(3,4,5-trimethoxyphenyl)ethan--ol (3j) MeO MeO OMe 3j Brown solid, H NMR (CDCl 3, 400 MHz): δ.25 (H, s), δ 3.82 (3H, s), δ 3.86 (6H, s), δ (2H, m), δ (H, m), δ 6.60 (2H, s); 3 C NMR (CDCl 3, 25 MHz): δ 56.3, 60.85, 8.33, 02.69, 33.97, , 53.58; IR (KBr pellet, ν max /cm - ): 3308, 3025, 2960, 2856, 2775, 608, 556, 423, 0, 043, Nitro--(p-tolyl)ethan--ol (3k) 3k Light yellow oil, H NMR (CDCl 3, 400 MHz): δ.52 (H, s), 2.34 (3H, s), δ (H, m), δ (H, m), δ (H, m), δ (H, dd, J=7.6Hz); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 2.6,70.90, 25.89, 29.67, 29.93, 38.89, 39.04;IR (KBr pellet, ν max /cm - ): ν 3429, 308, 2408, 553, 433, 22, 035, 963, 777, Nitropentan-2-ol (3l) 3l 9
10 Yellow liquid, H NMR (CDCl 3, 400 MHz): δ 0.96 (H, t, J=6.4 Hz), δ (H, s), 3.9 (H, s), 3.9 (H, s), (2H, m); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 5.95, 8.89, 35.4, 65.9, 86.47; IR (KBr pellet, ν max /cm - ): 336, 2846, 64, 520, 206, 7, 853, ((tert-butyldimethylsilyl)oxy)--nitrohexan-2-ol (3m) TBSO 3m Colorless oil; H-NMR (400 MHz, CDCl 3, TMS): δ 0.26 (6H,s),δ 0.83 (9H, s), δ (6H, m), δ (H, m), δ 3.89 (2H, t, J ¼ 7.2 Hz), δ (H, m), δ (H, m), δ 5.25 (H, s); 3C-NMR (00 MHz, CDCl3, TMS): d 80.60, 68.58, 62.83, 36.0, 33.35, 32.3, 25.95, 2.66, 5.3; IR (KBr pellet, ν max /cm - ): 753, 628, 528, 20,9, 865, 769, Nitro--(4-nitrophenyl)propan--ol (3o) O 2 N 3o Reddish liquid, H NMR (CDCl 3, 400 MHz): δ (H, dd, J=6.8 Hz), δ (2H, dd, J=6.8 Hz), δ3.26 (H, s), δ (H, m), δ 5.2 (H, d, J= 8.4 Hz), δ7.62 (2H, d, J= 4.8 Hz), δ (H, dd, J=4 Hz), δ (H, dd, J=4.4 Hz); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 6.6, 75.03, 87.88, 24.36, 28.0, 47.7, 48.; IR (KBr pellet, ν max /cm - ): ν 3435, 3330, 3025, 2889, 2789, 547, 440, 320, 284, 223, Nitro--(3-nitrophenyl)propan--ol (3p) 0
11 O 2 N 3p Reddish liquid, H NMR (CDCl 3, 400 MHz): δ (.5H, dd, J=6 Hz), δ (.5H, dd, J=6 Hz), δ (H, m), δ 5.22 (H, d, J= 8.4 Hz), δ (H, dd, J= 8.4 Hz), δ 7.78 (H, d, J=7.6 Hz), δ 8.50 (H, d, J=7.6 Hz) 8.69 (H, s); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 6., 74.97, 88.0, 2.95, 23.84, 33.2, 35.00, 40.83, 48.38; IR (KBr, pellet, ν max /cm - ): 3445, 330, 3055, 289, 2779,536, 44, 327, 282, 242, 58. -(4-Chlorophenyl)-2-nitropropan--ol (3q) Cl 3q Colorless oil, H NMR (CDCl 3, 400 MHz): δ.47 (3H, d, J=6.8 Hz), δ (H, m), δ 5.0 (H, d, J= 8.8 Hz), δ7.52 (2H, d, J= 7.6 Hz), δ 7.8 (2H, d, J=7.6 Hz); 3 C-NMR (00 MHz, CDCl3, TMS): δ 6.33, 3.77, 88.25, 27.40, 28.32, 3.47, 36.87; IR (KBr pellet, ν max /cm - ): 340, 3025, 2949, 2889, 2786, 546, 438, 38, 323, 28, 79, 2, 845, (-Hydroxy-2-nitropropyl)benzonitrile (3r) NC 3r Light green liquid, H NMR (CDCl 3, 400 MHz): δ (.5 H, d, J=6.8 Hz), δ (.5 H, dd, J=6.8 Hz), δ (H, m), δ 5.2 (H, d, J= 8.8 Hz), δ7.86 (2H, d, J= 8 Hz), δ 8.0
12 (2H, d, J=8 Hz); 3 C-NMR (00 MHz, CDCl3, TMS): δ 5.95, 73.3, 87.93, 2.07, 8.32, 26.97, 32.57, 43.87; IR (KBr pellet, ν max /cm - ): 3555, 3059, 294, 2055, 976, 528, 448, 280, (2-Bromophenyl)-2-nitropropan--ol (3s) Br 3s Yellow liquid, H NMR (CDCl 3, 400 MHz): δ (.5 H, dd, J=4 Hz), δ (.5 H, dd, J=6.8 Hz), δ (H, m), δ 5.55 (H, d, J= 6.8 Hz), δ 5.75 (H, s), δ7.2 (H, t, J= 5.2 Hz), δ 7.45 (H, d, J=6.8 Hz), δ 7.55 (H, t, J=7.2 Hz), δ 7.59 (H, d, J=7.6 Hz); 3 C-NMR (00 MHz, CDCl3, TMS): δ 6.0, 73.9, 88.33, 2.53, 29.94, 30.32, 32.32, 37.98; IR (KBr pellet, ν max /cm - ): 335, 2957, 2863, 2756, 527, 379, Nitro--(p-tolyl)propan--ol (3t) 3t Colorless liquid, H NMR (CDCl 3, 400 MHz): δ (.5 H, dd, J=6 Hz), δ (.5 H, dd, J=6 Hz), δ (H, m), δ 5.22 (H, d, J= 8.4 Hz), δ 5.56 (H, s), δ (H, dd, J= 8.4 Hz), δ 7.78 (H, d, J=7.6 Hz), δ 8.69 (H,s); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 6., 74.97, 88.0, 2.53, 29.95, 23.84, 33.2, 35.00, 40.38, 48.83; IR (KBr pellet, pellet, ν max /cm - ): ν 3445, 330, 3055, 289, 2779, 536, 44, 327, 282, 242, 58. 2
13 2-nitrohexan-3-ol (3u) 3u Light yellow liquid, H NMR (CDCl 3, 400 MHz): δ (3H, m), δ (4H, m), δ (3H, d, J=4.4), δ 2.69 (H, s), δ (H, m), δ (H, m); 3 C NMR (CDCl 3, 25 MHz): δ 3.74, 6.2, 8.35, 34.9, 7.8, 86.4; IR (KBr pellet, ν max /cm - ): 3306, 2946, 2830, 608, 536, 206, 48, 035, 838, ,9-Dimethyl-2-nitrodec-8-en-3-ol (3v) 3v Colorless liquid, H NMR (CDCl 3, 400 MHz): δ 0.93 (3H, d, J=6.8 Hz), δ 0.96 (3H, dd, J=6.4 Hz), δ.54 (6H, t, J=6.4 Hz), δ (8H, m), δ.60 (6H,s), δ.68 (6H,s), δ (2H, m), δ (4H, m), δ (H, m), δ (H, m), δ (H, m), δ (H, m), δ (2H, m), δ (2H, m); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 0., 0.2, 7.6, 8.6, 8.7, 20.0, 20.3, 25.4, 25.9, 25.3, 25.7, 28.4, 25.7, 28.6, 28.8, 29., 35.7, 36., 37.6, 37.8, 40., 40.4, , 70.8, 7., 86.8, 87.9, 88.4, 24.3, 3.5, 3.6; IR (KBr pellet, ν max /cm - ): 3540, 3025, 2925, 620, 553, 454, 38, nitro-7-((tetrahydro-2H-pyran-2-yl)oxy)heptan-3-ol (3w) THPO 3w 3
14 Light yellow liquid, H NMR (CDCl 3, 400 MHz): δ (3H, m), δ 2.5 (H, s), δ (2H, m), δ (H, m),δ (2H,m), δ (H, m), δ (H, m); 3 C-NMR (00 MHz, CDCl 3, TMS): δ 0., 0.2, 7.6, 8.6, 8.7, 20.0, 20.3, 25.4, 25.9, 25.3, 25.7, 28.4, 25.7, 28.6, 28.8, 29., 35.7, 36., 37.6, 37.8, 40., 40.4, , 70.8, 7., 86.8, 87.9, 88.4, 24.3, 3.5, 3.6; IR (KBr pellet, ν max /cm - ): 330, 306, 2940, 656, 530, 403, 350, 80, 875, 76. 4
15 O 2 N O 2 N 3a Fig: S4 : H NMR and 3 C NMR Spectra of 2-nitro--(4-nitrophenyl)ethanol (Table 3, Entry 3a) 5
16 3c 3c Fig S5: H NMR and 3 C NMR Spectra of 2-Nitro--(2-nitrophenyl)ethan--ol (Table 3, Entry 3c) 6
17 O 2 N 3d O 2 N Fig S6: H NMR and 3 C NMR Spectra of 2-nitro--(3-nitrophenyl)ethanol (Table 3, Entry 3d) 7
18 F 3e F 3e Fig S7: H NMR and 3 C NMR Spectra of -(4-Fluorophenyl)-2-nitroethan--ol (Table 3, Entry 3e) 8
19 Cl 3f Cl Fig S8:- H NMR and 3 C NMR Spectra of -(4-Chlorophenyl)-2-nitroethan--ol (Table 3, Entry 3f) 9
20 Br 3g Br 3g Fig S9: H NMR and 3 C NMR Spectra of -(4-Bromophenyl)-2-nitroethan--ol (Table 3, Entry 3g) 20
21 MeO 3h MeO 3h Fig S0: H NMR and 3 C NMR Spectra of -(4-methoxyphenyl)-2-nitroethan--ol (Table 3, Entry 3h) 2
22 MeO MeO OMe 3j MeO MeO OMe 3j Fig S: H NMR and 3 C NMR Spectra of -(3, 4-Dimethoxyphenyl)-2-nitroethanol (Table 3, Entry 3j) 22
23 3k 3k Fig S2: H NMR and 3 C NMR Spectra of 2-Nitro--(p-tolyl)ethan--ol (Table 3, Entry 3k) 23
24 3l 3l Fig S3: H NMR and 3 C NMR Spectra of -Nitropentan-2-ol (Table 3, Entry 3l) 24
25 TBSO 3m TBSO 3m Fig S4: H NMR and 3 C NMR Spectra of 6-((tert-butyldimethylsilyl)oxy)--nitrohexan-2-ol (Table 3, Entry 3m) 25
26 O 2 N 3o O 2 N 3o Fig S5 : H NMR and 3 C NMR Spectra of 2-Nitro--(4-nitrophenyl)propan--ol (Table 3, Entry 3o) 26
27 O 2 N 3p O 2 N 3p Fig S6 : H NMR and 3 C NMR Spectra of 2-Nitro--(3-nitrophenyl)propan--ol (Table 3, Entry 3p) 27
28 Cl 3q Cl 3q Fig S7 : H NMR and 3 C NMR Spectra of -(4-Chlorophenyl)-2-nitropropan--ol (Table 3, Entry 3q) 28
29 NC 3r NC 3r Fig S 8: H NMR and 3 C NMR Spectra of 4-(-Hydroxy-2-nitropropyl)benzonitrile (Table 3, Entry 3r) 29
30 Br Br Fig S9 : H NMR and 3 C NMR Spectra of -(2-Bromophenyl)-2-nitropropan--ol (Table 3, Entry) 30
31 3t 3t Fig S20 : H NMR and 3 C NMR Spectra of 2-Nitro--(p-tolyl)propan--ol (Table 3, Entry 3t) 3
32 3u 3u Fig S 2 : H NMR and 3 C NMR Spectra of 2-nitrohexan-3-ol (Table 3, Entry 3u) 32
33 3v 3v Fig S 22 : H NMR and 3 C NMR Spectra of 5,9-Dimethyl-2-nitrodec-8-en-3-ol (Table 3, Entry) 33
34 THPO 3w THPO 3w Fig S 23 : H NMR and 3 C NMR Spectra of 2-nitro-7-((tetrahydro-2H-pyran-2-yl)oxy)heptan-3-ol (Table 3, Entry 3w) 34
Supporting information
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 204 Supporting information Palladium nanoparticles supported on triazine functionalised mesoporous
Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via double C(sp 2 )-H thiolation
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via
A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Novel electroluminescent donor-acceptors based on dibenzo[a,c]phenazine as
![Novel electroluminescent donor-acceptors based on dibenzo[a,c]phenazine as](/thumbs/92/107849210.jpg "Novel electroluminescent donor-acceptors based on dibenzo[a,c]phenazine as")
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2016 Novel electroluminescent donor-acceptors
Supporting Information
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2017 Supporting Information Palladium
SUPPLEMENTARY MATERIAL
10.1071/CH16014_AC The Authors 2016 Australian Journal of Chemistry 2016, 69(9), 1049-1053 SUPPLEMENTARY MATERIAL A Green Approach for the Synthesis of Novel 7,11-Dihydro-6H-chromeno[3,4- e]isoxazolo[5,4-b]pyridin-6-one
Copper-Catalyzed Oxidative Dehydrogenative N-N Bond. Formation for the Synthesis of N,N -Diarylindazol-3-ones
Electronic Supplementary Material (ESI) for Organic Chemistry Frontiers. This journal is the Partner Organisations 2016 Supporting information Copper-Catalyzed Oxidative Dehydrogenative - Bond Formation
D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical and experimental study
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical
The Free Internet Journal for Organic Chemistry
The Free Internet Journal for Organic Chemistry Paper Archive for Organic Chemistry Arkivoc 2018, part iii, S1-S6 Synthesis of dihydropyranones and dihydropyrano[2,3- d][1,3]dioxine-diones by cyclization
Supporting Information
Supporting Information for AgOTf-catalyzed one-pot reactions of 2-alkynylbenzaldoximes with α,β-unsaturated carbonyl compounds Qiuping Ding 1, Dan Wang 1, Puying Luo* 2, Meiling Liu 1, Shouzhi Pu* 3 and
SUPPORTING INFORMATION. Polystyrene-immobilized DABCO as a highly efficient and recyclable organocatalyst for Knoevenagel condensation
Electronic Supplementary Material (ESI) for RSC Advances This journal is The Royal Society of Chemistry 213 SUPPORTING INFORMATION Polystyrene-immobilized DABCO as a highly efficient and recyclable organocatalyst
Available online at shd.org.rs/jscs/
J. Serb. Chem. Soc. 78 (1) S1 S8 (2013) Supplementary material SUPPLEMENTARY MATERIAL TO Metal complexes of N'-[2-hydroxy-5-(phenyldiazenyl)- benzylidene]isonicotinohydrazide. Synthesis, spectroscopic
Electronic Supplementary information
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Electronic Supplementary information Sulfonic acid-functionalized MIL-101(Cr) as a highly efficient
Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic acids with the assistance of isocyanide
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic
SUPPLEMENTARY MATERIAL. A Facile and Convenient Approach for the Synthesis of Novel Sesamol-Oxazine and Quinoline- Oxazine Hybrids
10.1071/CH17272_AC CSIRO 2017 Australian Journal of Chemistry 2017, 70(12), 1285-1290 SUPPLEMENTARY MATERIAL A Facile and Convenient Approach for the Synthesis of Novel Sesamol-Oxazine and Quinoline- Oxazine
College of Life Science, Dalian Nationalities University, Dalian , PR China.
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2018 Postsynthetic modification
Enantioselective Organocatalytic Michael Addition of Isorhodanines. to α, β-unsaturated Aldehydes
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2016 Enantioselective Organocatalytic Michael Addition of Isorhodanines to α,
9-amino-(9-deoxy)cinchona alkaloids-derived novel chiral phase-transfer catalysts
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 9-amino-(9-deoxy)cinchona alkaloids-derived novel chiral phase-transfer
Supporting Information
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2016 Supporting Information Abnormal N-Heterocyclic Carbene Based Nickel Complex for Catalytic
Supporting Information
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2015 Synthesis of 3-omosubstituted Pyrroles via Palladium- Catalyzed Intermolecular Oxidative Cyclization
using metal-organic framework Cu-MOF-74 as an efficient heterogeneous catalyst Hanh T. H. Nguyen, Oanh T. K. Nguyen, Thanh Truong *, Nam T. S.
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Synthesis of imidazo[1,5-a]pyridines via oxidative amination of C(sp 3 )-H bond under air using
Divergent synthesis of various iminocyclitols from D-ribose
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 205 Divergent synthesis of various iminocyclitols from D-ribose Ramu Petakamsetty,
Eco-friendly synthesis of diverse and valuable 2-pyridones by catalyst- and solvent-free thermal multicomponent domino reaction
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2015 SUPPRTIG IFRMATI Eco-friendly synthesis of diverse and valuable 2-pyridones by catalyst-
Metal-free Oxidative Coupling of Amines with Sodium Sulfinates: A Mild Access to Sulfonamides
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting information for Metal-free Oxidative Coupling of Amines with Sodium Sulfinates:
Supporting Information
Supporting Information Nano WO3-supported sulfonic acid: New, efficient and high recyclable heterogeneous nano catalyst Ali Amoozadeh* and Salman Rahmani* Department of Chemistry, Semnan University, Semnan,
Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes
Supporting Information for Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes Changkun Li and Jianbo Wang* Beijing National Laboratory
National d Histoire Naturelle, 57 rue Cuvier (C.P. 54), Paris, France. Contents:
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Supporting Information Synthesis and Biological Evaluation of the Ascidian
Supplementary material
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2015 Supplementary material Recyclable
Supporting Information
Supporting Information Ceric Ammonium Nitrate (CAN) catalyzed efficient one-pot three component aza-diels-alder reactions for a facile synthesis of tetrahydropyranoquinoline derivatives Ravinder Goud Puligoundla
Supporting Information for
Supporting Information for An atom-economic route to densely functionalized thiophenes via base-catalyzed rearrangement of 5-propargyl-2H-thiopyran-4(3H)-ones Chunlin Tang a, Jian Qin b, Xingqi Li *a a
New Cytotoxic Constituents from the Red Sea Soft Coral Nephthea sp.
SUPPLEMENTARY MATERIAL New Cytotoxic Constituents from the Red Sea Soft Coral Nephthea sp. Mohamed-Elamir F. Hegazy a,*, Amira M. Gamal-Eldeen b, Tarik A. Mohamed a, Montaser A. Alhammady c, Abuzeid A.
Aluminium triflate as a Lewis acid catalyst for the ring opening of epoxides in alcohols
Aluminium triflate as a Lewis acid catalyst for the ring opening of epoxides in alcohols D. Bradley G. Williams* and Michelle Lawton a Department of Chemistry, University of Johannesburg, P.O. Box 524,
Supporting Information
Supporting Information Copper/Silver Cocatalyzed Oxidative Coupling of Vinylarenes with ICH 2 CF 3 or ICH 2 CHF 2 Leading to β-cf 3 /CHF 2 -Substituted Ketones Niannian Yi, Hao Zhang, Chonghui Xu, Wei
phase: synthesis of biaryls, terphenyls and polyaryls
Supporting Information for Studies on Pd/NiFe 2 O 4 catalyzed ligand-free Suzuki reaction in aqueous phase: synthesis of biaryls, terphenyls and polyaryls Sanjay R. Borhade and Suresh B. Waghmode* Address:
Electronic Supplementary Information
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2014 Electronic Supplementary Information Syntheses and structures of copper complexes of
Available online at
J. Serb. Chem. Soc. 76 (12) S1 S5 (2011) Supplementary material SUPPLEMENTARY MATERIAL TO Synthesis of quinoline-attached furan-2(3h)-ones having anti-inflammatory and antibacterial properties with reduced
Electronic Supplementary Information
Electronic Supplementary Information Unprecedented Carbon-Carbon Bond Cleavage in Nucleophilic Aziridine Ring Opening Reaction, Efficient Ring Transformation of Aziridines to Imidazolidin-4-ones Jin-Yuan
A straightforward metal-free synthesis of 2-substituted thiazolines in air
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2015 Supporting Information for A straightforward metal-free synthesis of 2-substituted thiazolines
Supporting Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2018 Supporting Information Silver or Cerium-Promoted Free Radical Cascade Difunctionalization
Facile construction of the functionalized 4H-chromene via tandem. benzylation and cyclization. Jinmin Fan and Zhiyong Wang*
Facile construction of the functionalized 4H-chromene via tandem benzylation and cyclization Jinmin Fan and Zhiyong Wang* Hefei National Laboratory for Physical Science at Microscale, Joint- Lab of Green
Synthesis of novel 1,2,3-triazolyl derivatives of pregnane, androstane and D-homoandrostane. Tandem Click reaction/cu-catalyzed D-homo rearrangement
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information Synthesis of novel 1,2,3-triazolyl derivatives of
Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/ bromides in water using oxone-kx(x= Cl or Br)
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2014 Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/ bromides in water using
Supporting information
Supporting information Spectroscopic data of compounds 1a-f Benzyl bromide (1a) Yield: 81%. Colorless oil. b.p. 79-82 o C/15 mmhg (Lit. 83.5 84 o C/13 mmhg). 1 1 H NMR (CDCl 3 ): δ 4.45 (2H, s, PhCH 2
Supporting Information
Supporting Information Montmorillonite KSF-Catalyzed One-pot, Three-component, Aza-Diels- Alder Reactions of Methylenecyclopropanes With Arylaldehydes and Aromatic Amines Li-Xiong Shao and Min Shi* General
Supporting Information. Experimental section
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting Information Experimental section General. Proton nuclear magnetic resonance ( 1
Sulfonated graphene as highly efficient and reusable acid carbocatalyst for the synthesis of ester plasticizers
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 204 Supporting information for publication Sulfonated graphene as highly efficient and reusable
Supporting Information. Introduction of a α,β-unsaturated carbonyl conjugated pyrene-lactose hybrid
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 16 Supporting Information Introduction of a α,β-unsaturated carbonyl conjugated pyrene-lactose hybrid
Nitric oxide (NO) reactivity studies on mononuclear Iron(II) complexes supported by a tetradentate Schiff base Ligand
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Nitric oxide (NO) reactivity studies on mononuclear Iron(II) complexes supported by a tetradentate
SUPPORTING INFORMATION. 1. General... S1. 2. General procedure for the synthesis of compounds 3 and 4 in the absence of AgOAc...
SUPPORTING INFORMATION Table of contents 1. General.... S1 2. General procedure for the synthesis of compounds 3 and 4 in the absence of AgOAc... S2 3. General procedure for the synthesis of compounds
Available online at shd.org.rs/jscs/
J. Serb. Chem. Soc. 78 (12) S131 S136 (2013) Supplementary material SUPPLEMENTARY MATERIAL TO New 9-aminoacridine derivatives as inhibitors of botulinum neurotoxins and P. falciparum malaria MIKLOŠ TOT
Extended dissolution studies of cellulose in imidazolium based ionic liquids
Electronic Supplementary Information Extended dissolution studies of cellulose in imidazolium based ionic liquids Jürgen Vitz, a,b Tina Erdmenger, a,b Claudia Haensch, a,b Stephanie Hornig # and Ulrich
Heavier chalcogenone complexes of bismuth(iii)trihalides: Potential catalysts for acylative cleavage of cyclic ethers. Supporting Information
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 Heavier chalcogenone complexes of bismuth(iii)trihalides: Potential catalysts for acylative
Supporting Information
Supporting Information Gold-catalyzed Cycloisomerization of 1,6-Diyne-4-en-3-ols to form Naphthyl Ketone Derivatives. Jian-Jou Lian and Rai-Shung Liu* Department of Chemistry, National Tsing-Hua University,
Supporting Information. for. A novel application of 2-silylated 1,3-dithiolanes for the. synthesis of aryl/hetaryl-substituted ethenes and
Supporting Information for A novel application of 2-silylated 1,3-dithiolanes for the synthesis of aryl/hetaryl-substituted ethenes and dibenzofulvenes Grzegorz Mlostoń *1, Paulina Pipiak 1, Róża Hamera-Fałdyga
Supporting Information
Supporting Information Molecular Cage Impregnated Palladium Nanoparticles: Efficient, Additive-Free Heterogeneous Catalysts for Cyanation of Aryl Halides. Bijnaneswar Mondal, Koushik Acharyya, Prodip Howlader
Supporting Information One-Pot Approach to Chiral Chromenes via Enantioselective Organocatalytic Domino Oxa-Michael-Aldol Reaction
Supporting Information ne-pot Approach to Chiral Chromenes via Enantioselective rganocatalytic Domino xa-michael-aldol Reaction Hao Li, Jian Wang, Timiyin E-Nunu, Liansuo Zu, Wei Jiang, Shaohua Wei, *
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2008
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2008 Rhodium-Catalyzed Cyclopropanation of Alkenes with Diazomalonates Francisco González-Bobes, a * Michaël D. B. Fenster,
Chiral Brønsted Acid Catalyzed Enantioselective Intermolecular Allylic Aminations. Minyang Zhuang and Haifeng Du*
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Chiral Brønsted Acid Catalyzed Enantioselective Intermolecular Allylic
Supporting information for
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting information for Mesoporous silica KIT-6 supported superparamagnetic CuFe 2 O
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2006
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2006 1 A Facile Way to Synthesize 2H-Chromenes: Reconsideration of the Reaction Mechanism between Salicylic Aldehyde and
Supporting Information
Supporting Information Lewis acid catalyzed ring-opening reactions of methylenecyclopropanes with diphenylphosphine oxide in the presence of sulfur or selenium Min Shi,* Min Jiang and Le-Ping Liu State
Synthesis and Biological Evaluation of Novel Acyclic and Cyclic Glyoxamide derivatives as Bacterial Quorum Sensing and Biofilm Inhibitors
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Synthesis and Biological Evaluation of Novel Acyclic and Cyclic Glyoxamide
Supporting information
Electronic upplementary Material (EI) for New Journal of Chemistry. This journal is The Royal ociety of Chemistry and the Centre National de la Recherche cientifique 7 upporting information Lipase catalyzed,-addition
Chemical Constituents and Antioxidant Activity of Teucrium barbeyanum Aschers.
Supporting Information Rec. Nat. Prod. 9:1 (2015) 159-163 Chemical Constituents and Antioxidant Activity of Teucrium barbeyanum Aschers. Mohamed Ali A. Alwahsh, Melati Khairuddean * and Wong Keng Chong
Modular Synthesis of Cyclic cis- and trans-1,2-diamine Derivatives
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 4 Modular Synthesis of Cyclic cis- and trans-,-diamine Derivatives Anna K. Weber,
Supplementary Materials
Supplementary Materials Figure S1. Chemical structures of phloracetophenone intermediates (2a, 2c 2g). 2a 2c 2d 2e 2f 2g Figure S2. Chemical structures of geranylacetophenone analogues (3a, 3c, 3e g).
Heterobimetallic Pd-Sn Catalysis: Michael Addition. Reaction with C-, N-, O-, S- Nucleophiles and In-situ. Diagnostics
Supporting Information (SI) Heterobimetallic Pd-Sn Catalysis: Michael Addition Reaction with C-, N-, -, S- Nucleophiles and In-situ Diagnostics Debjit Das, a Sanjay Pratihar a,b and Sujit Roy c * a rganometallics
Supplementary Information for
Supplementary Information for Organocatalytic Asymmetric Intramolecular [3+2] Cycloaddition: A Straightforward Approach to Access Multiply Substituted Hexahydrochromeno[4,3-b]pyrrolidine Derivatives in
Fischer Indole Synthesis in Low Melting Mixtures
Fischer Indole Synthesis in Low Melting Mixtures Sangram Gore, a,b Sundarababu Baskaran* a and Burkhard König* b Supporting Information Table of Contents: General Information General Procedure for the
Highly enantioselective cascade synthesis of spiropyrazolones. Supporting Information. NMR spectra and HPLC traces
Highly enantioselective cascade synthesis of spiropyrazolones Alex Zea a, Andrea-Nekane R. Alba a, Andrea Mazzanti b, Albert Moyano a and Ramon Rios a,c * Supporting Information NMR spectra and HPLC traces
First DMAP-mediated direct conversion of Morita Baylis. Hillman alcohols into γ-ketoallylphosphonates: Synthesis of
Supporting Information File 1 for First DMAP-mediated direct conversion of Morita Baylis Hillman alcohols into γ-ketoallylphosphonates: Synthesis of γ-aminoallylphosphonates Marwa Ayadi 1,2, Haitham Elleuch
Vilsmeier Haack reagent-promoted formyloxylation of α-chloro-narylacetamides
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 205 Vilsmeier aack reagent-promoted formyloxylation of α-chloro-arylacetamides by formamide Jiann-Jyh
Supporting information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting information Copper-catalysed intramolecular O-arylation: a simple
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%.
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%. S1 Supplementary Figure S2. Single X-ray structure 5a at probability ellipsoids of 20%. S2 H 15 Ph Ac Ac I AcH Ph Ac
Supporting Information. Experimental section
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting Information Experimental section General. Anhydrous solvents were transferred by
Pd Catalyzed Carbonylation for the Construction of Tertiary and
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Pd Catalyzed Carbonylation for the Construction of Tertiary and Quaternary
SUPPLEMENTAL INFORMATION. Fully Automated Total Metals and Chromium Speciation Single Platform Introduction System for ICP-MS
Electronic Supplementary Material (ESI) for Journal of Analytical Atomic Spectrometry. This journal is The Royal Society of Chemistry 2018 SUPPLEMENTAL INFORMATION Fully Automated Total Metals and Chromium
Supporting information. An unusual bifunctional Tb-MOF for highly sensing of Ba 2+ ions and remarkable selectivities of CO 2 /N 2 and CO 2 /CH 4
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2015 Supporting information An unusual bifunctional Tb-MOF for highly sensing
Supporting Information for
Supporting Information for A ovel Synthesis of luorinated Pyrazoles via Gold(I)-Catalyzed Tandem Aminofluorination of Alkynes in the Presence of Selectfluor Jianqiang Qian, Yunkui Liu,* Jie Zhu, Bo Jiang,
Selective mono reduction of bisphosphine
Griffith Research Online https://research-repository.griffith.edu.au Selective mono reduction of bisphosphine oxides under mild conditions Author etersson, Maria, Loughlin, Wendy, Jenkins, Ian ublished
Supporting Information
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2010 A Highly Effective Bis(sulfonamide) Diamine Ligand: A Unique Chiral Skeleton for the Enantioselective Cu-Catalyzed
Supporting Information. Partial thioamide scan on the lipopeptaibiotic trichogin GA IV. Effects on
Supporting Information for Partial thioamide scan on the lipopeptaibiotic trichogin GA IV. Effects on folding and bioactivity Marta De Zotti 1, Barbara Biondi 1, Cristina Peggion 1, Matteo De Poli 1, Haleh
Supplementary Data. Engineering, Nanjing University, Nanjing , P. R. China;
Supplementary Data Synthesis, Chemo-selective Properties of Substituted 9-Aryl-9H-fluorenes from Triarylcarbinols and Enantiomerical Kinetics of Chiral 9-Methoxy-11-(naphthalen-1-yl)-11H-benzo[a]fluorene
Structure-Metabolism-Relationships in the microsomal clearance of. piperazin-1-ylpyridazines
Electronic Supplementary Material (ESI) for MedChemComm. This journal is The Royal Society of Chemistry 2017 Structure-Metabolism-Relationships in the microsomal clearance of piperazin-1-ylpyridazines
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2006
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2006 A new route to enantiopure b-aryl-substituted b-amino acids and 4-aryl-substituted b-lactams through lipase-catalyzed
Mandelamide-Zinc Catalyzed Alkyne Addition to Heteroaromatic Aldehydes
1 Mandelamide-Zinc Catalyzed Alkyne Addition to Heteroaromatic Aldehydes Gonzalo Blay, Isabel Fernández, Alícia Marco-Aleixandre, and José R. Pedro Departament de Química Orgànica, Facultat de Química,
Tributylphosphine-Catalyzed Cycloaddition of Aziridines with Carbon Disulfide and Isothiocyanate
upporting Information Tributylphosphine-Catalyzed Cycloaddition of Aziridines with Carbon Disulfide and Isothiocyanate Jing-Yu Wu, Zhi-Bin Luo, Li-Xin Dai and Xue-Long Hou* a tate Key Laboratory of Organometallic
Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information
![Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information](/thumbs/64/50937700.jpg "Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information")
Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans Liang Yun, Shi Tang, Xu-Dong Zhang, Li-Qiu Mao, Ye-Xiang Xie and Jin-Heng Li* Key Laboratory
Synthesis of Imines from Amines in Aliphatic Alcohols on Pd/ZrO 2 Catalyst at Ambient Conditions
This journal is The Royal Society of Chemistry 213 Synthesis of Imines from Amines in Aliphatic Alcohols on Pd/ZrO 2 Catalyst at Ambient Conditions Wenjing Cui, a Bao Zhaorigetu,* a Meilin Jia, a and Wulan
Supplementary Information
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2017 Supplementary Information Immobilization of Pseudomonas fluorescens lipase on silk fibroin
Supporting Information
Supporting Information Regioselective Reversal in the Cyclization of 2-Diazo-3,5-dioxo-6-ynoates (ynones, ynamide): Construction of -Pyrones and 3(2H)-Furanones Starting from Identical Materials Feng Wang,
Supplementary Material for Synthesis of Compact Multidentate Ligands to Prepare Stable Hydrophilic Quantum Dot Fluorophores
Supplementary Material for Synthesis of Compact Multidentate Ligands to Prepare Stable Hydrophilic Quantum Dot Fluorophores 5-[1,2]-Dithiolan-3-yl-pentanoic acid 2-[2-(2-{2-[2-(2-hydroxy-ethoxy)-ethoxy]-ethoxy}-
Site-Selective Suzuki-Miyaura Cross-Coupling Reactions of 2,3,4,5-Tetrabromofuran
1 Site-Selective Suzuki-Miyaura Cross-Coupling Reactions of 2,3,4,5-Tetrabromofuran Munawar Hussain, a Rasheed Ahmad Khera, a Nguyen Thai Hung, a Peter Langer* a,b a Institut für Chemie, Universität Rostock,
SUPPORTING INFORMATION
SUPPRTING INFRMATIN Per(-guanidino--deoxy)cyclodextrins: Synthesis, characterisation and binding behaviour toward selected small molecules and DNA. Nikolaos Mourtzis, a Kyriaki Eliadou, a Chrysie Aggelidou,
Supporting Information. Consecutive hydrazino-ugi-azide reactions: synthesis of acylhydrazines bearing 1,5- disubstituted tetrazoles
Supporting Information for Consecutive hydrazino-ugi-azide reactions: synthesis of acylhydrazines bearing 1,5- disubstituted tetrazoles Angélica de Fátima S. Barreto*, Veronica Alves dos Santos, and Carlos
Room Temperature Highly Diastereoselective Zn-Mediated. Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled
Supporting Information for: Room Temperature Highly Diastereoselective Zn-Mediated Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled Stereoselectivity Reversal
Electronic Supplementary Information (ESI)
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Electronic Supplementary Information (ESI) Cyclopentadienyl iron dicarbonyl (CpFe(CO) 2 ) derivatives
Supporting Information
Supporting Information Biomimetic total syntheses of borreverine and flinderole alkaloids. Dattatraya. Dethe,* Rohan D. Erande and Alok Ranjan Department of Chemistry, Indian Institute of Technology-Kanpur,
Free Radical Initiated Coupling Reaction of Alcohols and. Alkynes: not C-O but C-C Bond Formation. Context. General information 2. Typical procedure 2
Free Radical Initiated Coupling Reaction of Alcohols and Alkynes: not C-O but C-C Bond Formation Zhongquan Liu,* Liang Sun, Jianguo Wang, Jie Han, Yankai Zhao, Bo Zhou Institute of Organic Chemistry, Gannan
Protease-catalysed Direct Asymmetric Mannich Reaction in Organic Solvent
Supplementary information for the paper Protease-catalysed Direct Asymmetric Mannich Reaction in Organic Solvent Yang Xue, Ling-Po Li, Yan-Hong He * & Zhi Guan * School of Chemistry and Chemical Engineering,