PHMG PET 93. 7%. TEM PHMG. PET-g-PHMG. PET PET PET PHMG. PET-g-PHMG PET PET 99%

Μέγεθος: px
Εμφάνιση ξεκινά από τη σελίδα:

Download "PHMG PET 93. 7%. TEM PHMG. PET-g-PHMG. PET PET PET PHMG. PET-g-PHMG PET PET 99%"

Transcript

1 Vol 35 No CHEMICAL JOURNAL OF CHINESE UNIVERSITIES 873 ~ 880 doi /cjcu PHMG PET 15% PET PET-g-PHMG PHMG PET 93 7% TEM PHMG PET PHMG PET-g-PHMG PET PET-g-PHMG PET-g-PHMG PET PET PET 99% PET PET PET O631 A 1 2 ~ ~ ATRP PET PET 16 PHMG PHMG PHMG 24 PHMG PET ZR ZR zan@ ecust edu cn lsz@ ecust edu cn

2 874 Vol 35 PET PET PET PET PET PET PET 0 81 dl /g PHMG M n = 1000 DMF 8099 ATCC6538 Magna-IR550 FTIR Nicolet KBr 500 ~ 4000 cm - 1 JSM-6360LV SEM JEM-2100F200 kv TEM AVANCE Ⅲ 500 MHz 1 H NMR Spectrospin D 2 O 1 2 PHMG- PHMG-e PHMG Scheme ml 34 g PHMG 28 g 150 ml DMF PHMG 0 45 g 60 4 h 20 5 g 25 8 h Scheme 1 Chemical structure of PHMG DMF PHMG-e 1 3 PET-g-PHMG PET h 51 g PET 9 g PHMG-e PHMG-e 15% Haake Haake min PET PET-g-PHMG Haake 1 4 PET PET PET-g-PHMG h PET PET-g- PHMG Haake 0 5% 0 8% 1% PET PET-0 5 PET-0 8 PET-1 Haake min 1 5 PET PET-g-PHMG PET h MATE-Ⅴ Tokyo m /min 0 13 tex 1 6 GB /T g PET 75 ml cfu /ml h cfu /ml 0 1 ml h 5 Y Y = A - B /A 100% A B

3 No PHMG PHMG-e PHMG PHMG-e 1 H NMR 1 1 A δ 1 28 ~ 1 51 t CH 2 δ 2 61 ~ 2 66 PHMG m NH 2 δ 3 1 m CH 2 NH δ 4 7 t NH 1 B δ 2 61 ~ 2 66 m NH 2 δ 2 8 ~ 2 9 t CH CH 2 δ 3 2 s CH CH 2 δ 3 5 m CH 2 CH CH 2 PHMG-e Fig 1 1 H NMR spectra of PHMG A and PHMG-e B 2 2 PET PHMG-e Haake PET PHMG-e PHMG-e PET Scheme 2 Scheme 2 Reaction scheme of producing PET-g-PHMG 2 PET PHMG-e 2 PET 1 PET PHMG-e 1 1 min 1 PET PHMG-e Haake 2 PET PHMG-e PET-g-PHMG PET PET Fig 2 Torque variations with time in Haake PET PET-g-PHMG FTIR PET FTIR 3 a 1720 cm - 1 PET PET 3 b PET-g-PHMG 1640 cm PHMG C N PHMG PET-

4 876 Vol 35 g-phmg h PHMG PET PHMG 3 c PET-g-PHMG 1640 cm - 1 C N PHMG PET PHMG PET P P = 1 - m - m / m 15% 100% m Fig 3 FTIR spectra of PET / antibacterial masterbatch before and after extraction m a PET b PET-g-PHMG before extraction P = 93 7% c PET-g-PHMG after extraction 2 4 PET PHMG PET PET SEM 4 4 A PET /PHMG PET PHMG PET /PHMG PHMG PET PHMG PET 4 A 4 B PET-g-PHMG PHMG PET PHMG PET Fig 4 SEM images of fracture surface of PET /PHMG A and antibacterial PET with 1%PHMG B PHMG PET PET-g-PHMG TEM 5 PET /PHMG PET-g-PHMG OsO 4 TEM 5 A PET /PHMG PHMG PET 5 B PHMG PET PHMG PET PHMG PET PHMG Fig 5 TEM images of ultrathin section of PET /PHMG A and PET-g-PHMG B

5 No PET PET PET-g-PHMG PET PET-g-PHMG PET Haake 5 min PHMG 0 5% 0 8% 1 0% PET 1 PET /PHMG 1% PHMG PET 5 min Processed PET PET min Sample Content of antibacterial master batch % Table 1 PHMG content % intrinsic viscosity test of PET samples Processing temperature / viscosity * Intrinsic / dl g - 1 Antibacterial rate % E coli S aureus PET processed PET PET-g-PHMG 15 PET PET PET PET /PHMG * Test solution filtered 1 PHMG PET PHMG PET PET /PHMG 0 57 dl /g PET-1 PHMG 1% 0 75 dl /g PET PET PET-g-PHMG PHMG PET PET PET-1 PET Processed PET PET-g-PHMG PET PET-1 Processed PET PET PET-g-PHMG PET PET dl /g PET PET-g-PHMG PET PET PET 300 PET min PET dl /g 2 6 PET PET /PHMG PET-0 5 PET-0 8 PET-1 E coli S aureus 1 1 PET PET % PET-g-PHMG PET % PHMG PET PET /PHMG 61 59% 25 PHMG PP PE 99% PET PHMG PET PET

6 878 Vol 35 PHMG PHMG PHMG PET PET PET-0 5 PET /PHMG h 6 A B C PET PET /PHMG PET PET /PHMG 20% PET PET /PHMG PET % PHMG PET PET Fig 6 Antibacterial performance of PET A PET /PHMG washed by water B and PET-0 5 washed by water C against Gram-Negative E coli 2 7 PET PET-0 5 PET 10 d PET 7 PET PET 7 A 7 B PET % PET PET 8 PET cfu /ml 2 GB /T % 8 70% Fig 7 Antibacterial performance against Gram-Negative E coli of PET fibre A and antibcterial PET fibre B Fig 8 Antimicrobial kinetics test of antimicrobial PET fibers against E coli a and S aureus b

7 No min 22 PET PET PET-1 PET PET-1 10 min 90% 8 36 min PET 90% 94% PHMG PET 15% PET-g-PHMG PHMG 93 7% PET PET-g-PHMG PHMG PET PHMG PET PET-g- PHMG PET 3 PET PET-g- PHMG PET PET 99% PET PET 100% 1 Tang Z R Textile Auxiliaries Braydich-Stolle L Hussain S Schlage J J Hofmann M C Toxicol Sci Wen H C Lin Y N Jian S R Tseng S C Weng M X Liu Y P Lee P T Chen P Y Hsu R Q Wu W F Chou C P J Phys Conf Ser Gopinath P Gogoi S K Chattopadhyay A Gosh S S Nanobiotechnol Hussain S M Javorina M K Schrand A M Duhart H M Ali S F Schlager J J Toxicol Sci Hussain S M Hess K L Gearhart J M Geiss K T Schlager J J Toxicol in Vitro Buche ska J J Appl J Polym Sci Park J S Kim J H Nho Y C Kwon O H J Appl Polym Sci Chu C L Bi S M Bao J Y New Chemical Material Xiang Z H Application of Silver Loading Multi-walled Carbon Nanotubes Antibacterial Agents in Fiber Taiyuan University of Technology Taiyuan 2011 PET Kerkeni A Behary N Dhulster P Chihib N E Perwuelz A J Appl Polym Sci Holl nder A Thome J Keusgen M Degener I Klein W Appl Surf Sci / Ping X Irradiation Grafting and Induced Compatibilized Modification of PET University of Science and Technology of China Hefei 2011 PET Kurt P Wood L Ohman D E Wynne K J Langmuir Cerkez I Worley S D Broughton R M Huang T S Prog Org Coat / SalIe A J Fundamental Principles of Bacteriology McGraw-Hili Book Company New York Sideridou I Tserki V Papanastasiou G Biomaterials Pereira S G Nunes T G Kalachandra S Biomaterials Wei D F Ma Q X Guan Y Hu F Z Zheng A N Zhang X Teng Z Jiang H Mater Sci Eng C Qian L Y Guan Y He B H Xiao H N Polymer Zhou Z X Wei D F Guan Y Zheng A N Zhong J J J Appl Microbiol Guan Y Qian L Xiao H Zheng A Cellulose Guan Y Xiao H Sullivan H Zheng A Carbohydr Polym Zheng A N Guan Y Zhou Q Cheng Y Plastics Packaging Ma Q X Wei D F Hu F Z Zheng A N Journal of Functional Polymers / /

8 880 Vol 35 Preparation and Characterization of Long-acting Antimicrobial Polyethylene Terephthalate via Covalent Bonding Method ZHANG Qi LU Suhui ZHENG Anna * GUAN Yong WEI Dafu HUANG Tianhua LI Shuzhao * School of Materials Science and Engineering Shanghai Key Laboratory of Advanced Polymeric Materials Key Laboratory for Ultrafine Materials of Ministry of Education East China University of Science and Technology Shanghai China Abstract Polyhexamethylene guanidine hydrochloride PHMG was uesd to produce a long-acting antimicrobial polyethylene terephthalate PET masterbatch PET-g-PHMG which was obtained by covalently bonding 15% PHMG based on total weight onto PET matrix Attributed to the higher grafting efficiency 93 7% the hydrophilic PHGH is uniformly dispersed in PET matrix without any aggregate which potentially enhances its antimicrobial activity Several antimicrobial PET samples can be prepared by adding specific amount of PET-g- PHMG into the PET matrix It was found that the addition of PET-g-PHMG did not cause the degradation of PET matrix instead increased the intrinsic viscosity because of the presence of some un-reactive functional groups in the PET-g-PHMG The antimicrobial PET samples showed quickly and efficiently antimicrobial activity against both Gram-positive and Gram-negative bacteria Furthermore antimicrobial activity of the antimicrobial PET fibers prepared by a spun-bonded method remained even after constant water washing for 10 d indicating its long-acting antimicrobial ability via a contact activity rather than a release mechanism Keywords Polyethylene terephthalate Covalent bonding Long-acting antibacterial Graft modification Guanidine-based antimicrobial polymers polyhexamethylene guanidine hydrochloride Ed W Z Supported by the Natural Science Foundation of Shanghai China No 13ZR ZR

Antibacterial property of fabric treated with a fiber-reactive chitosan derivative

Antibacterial property of fabric treated with a fiber-reactive chitosan derivative 32 2 2011 2 Journal of Textile Research Vol. 32 No. 2 Fen. 2011 0253-9721 2011 02-0096-06 1 1 2 1. 201620 2. 201620 85% CTS N- HDCC HDCC N- NMA O- -N- NMA-HDCC HDCC NMA-HDCC 95% HDCC 100% 30 NMA-HDCC 85%

Διαβάστε περισσότερα

Comparison of carbon-sulfur and carbon-amine bond in therapeutic drug: -S-aromatic heterocyclic podophyllum derivatives display antitumor activity

Comparison of carbon-sulfur and carbon-amine bond in therapeutic drug: -S-aromatic heterocyclic podophyllum derivatives display antitumor activity Comparison of carbon-sulfur and carbon-amine bond in therapeutic drug: -S-aromatic heterocyclic podophyllum derivatives display antitumor activity Jian-Long Li 1,a, Wei Zhao 1,a, Chen Zhou 1,a, Ya-Xuan

Διαβάστε περισσότερα

College of Life Science, Dalian Nationalities University, Dalian , PR China.

College of Life Science, Dalian Nationalities University, Dalian , PR China. Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2018 Postsynthetic modification

Διαβάστε περισσότερα

Gro wth Properties of Typical Water Bloom Algae in Reclaimed Water

Gro wth Properties of Typical Water Bloom Algae in Reclaimed Water 31 1 2010 1 ENVIRONMENTAL SCIENCE Vol. 31,No. 1 Jan.,2010, 3, (,, 100084) :,.,, ( Microcystis aeruginosa),3 (A 2 O ) 10 6 ml - 1,> 0139 d - 1. A 2 O222,. TP ( K max ) ( R max ), Monod. :; ; ; ; :X173 :A

Διαβάστε περισσότερα

ER-Tree (Extended R*-Tree)

ER-Tree (Extended R*-Tree) 1-9825/22/13(4)768-6 22 Journal of Software Vol13, No4 1, 1, 2, 1 1, 1 (, 2327) 2 (, 3127) E-mail xhzhou@ustceducn,,,,,,, 1, TP311 A,,,, Elias s Rivest,Cleary Arya Mount [1] O(2 d ) Arya Mount [1] Friedman,Bentley

Διαβάστε περισσότερα

Study on the Strengthen Method of Masonry Structure by Steel Truss for Collapse Prevention

Study on the Strengthen Method of Masonry Structure by Steel Truss for Collapse Prevention 33 2 2011 4 Vol. 33 No. 2 Apr. 2011 1002-8412 2011 02-0096-08 1 1 1 2 3 1. 361005 3. 361004 361005 2. 30 TU746. 3 A Study on the Strengthen Method of Masonry Structure by Steel Truss for Collapse Prevention

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information for AgOTf-catalyzed one-pot reactions of 2-alkynylbenzaldoximes with α,β-unsaturated carbonyl compounds Qiuping Ding 1, Dan Wang 1, Puying Luo* 2, Meiling Liu 1, Shouzhi Pu* 3 and

Διαβάστε περισσότερα

Electronic Supplementary Information

Electronic Supplementary Information Electronic Supplementary Information Unprecedented Carbon-Carbon Bond Cleavage in Nucleophilic Aziridine Ring Opening Reaction, Efficient Ring Transformation of Aziridines to Imidazolidin-4-ones Jin-Yuan

Διαβάστε περισσότερα

Antimicrobial Ability of Limonene, a Natural and Active Monoterpene

Antimicrobial Ability of Limonene, a Natural and Active Monoterpene 2010,32 (1) :24 28 http :/ / xuebao. jlau. edu. cn Journal of Jilin Agricultural University E2mail : jlndxb @vip. sina. com Ξ,,,, ΞΞ, 200062 : : 320 mg/ L,; ph 4 9, ; 80, 100,121 : : ; ; : TS20213 : A

Διαβάστε περισσότερα

JOURNAL OF THE CHINESE CERAMIC SOCIETY. TiO 2 X

JOURNAL OF THE CHINESE CERAMIC SOCIETY. TiO 2 X 40 8 2012 8 Ni-YSZ Sm 0.5 Sr 0.5 Fe 0.8 Cu 0.2 O 3 δ 1215 JOURNAL OF THE CHINESE CERAMIC SOCIETY Vol. 40 No. 8 August 2012 TiO 2 ( 710048) TiO 2 20 30 nm TiO 2 (PVP) TiO 2 X TiO 2 TiO 2 TiO 2 150 250 nm

Διαβάστε περισσότερα

D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical and experimental study

D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical and experimental study Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical

Διαβάστε περισσότερα

Studies on the Binding Mechanism of Several Antibiotics and Human Serum Albumin

Studies on the Binding Mechanism of Several Antibiotics and Human Serum Albumin 2005 63 Vol. 63, 2005 23, 2169 2173 ACTA CHIMICA SINICA No. 23, 2169 2173 a,b a a a *,a ( a 130012) ( b 133002), 26 K A 1.98 10 4, 1.01 10 3, 1.38 10 3, 5.97 10 4 7.15 10 4 L mol 1, n 1.16, 0.86, 1.19,

Διαβάστε περισσότερα

Νανοσύνθετα πολυαιθυλενίου υψηλής πυκνότητας (HDPE) / νανοϊνών χαλκού (Cu-nanofibers) με βελτιωμένη σταθερότητα στην υπεριώδη ακτινοβολία

Νανοσύνθετα πολυαιθυλενίου υψηλής πυκνότητας (HDPE) / νανοϊνών χαλκού (Cu-nanofibers) με βελτιωμένη σταθερότητα στην υπεριώδη ακτινοβολία ΑΡΙΣΤΟΤΕΛΕΙΟ ΠΑΝΕΠΙΣΤΗΜΙΟ ΘΕΣΣΑΛΟΝΙΚΗΣ ΣΧΟΛΗ ΘΕΤΙΚΩΝ ΕΠΙΣΤΗΜΩΝ ΤΜΗΜΑ ΦΥΣΙΚΗΣ Πρόγραμμα Μεταπτυχιακών Σπουδών ΦΥΣΙΚΗΣ ΚΑΙ ΤΕΧΝΟΛΟΓΙΑΣ ΥΛΙΚΩΝ Νανοσύνθετα πολυαιθυλενίου υψηλής πυκνότητας (HDPE) / νανοϊνών

Διαβάστε περισσότερα

Synthesis Characterization and Application of Phosphorus-Containing Derivatives of Chitosan

Synthesis Characterization and Application of Phosphorus-Containing Derivatives of Chitosan 22 5 2010 5 PROGRESS IN CHEMISTRY Vol. 22 No. 5 May 2010 * 450001 / O636. 1 A 1005-281X 2010 05-0938-10 Synthesis Characterization and Application of Phosphorus-Containing Derivatives of Chitosan Ma li

Διαβάστε περισσότερα

Optimizing Microwave-assisted Extraction Process for Paprika Red Pigments Using Response Surface Methodology

Optimizing Microwave-assisted Extraction Process for Paprika Red Pigments Using Response Surface Methodology 2012 34 2 382-387 http / /xuebao. jxau. edu. cn Acta Agriculturae Universitatis Jiangxiensis E - mail ndxb7775@ sina. com 212018 105 W 42 2 min 0. 631 TS202. 3 A 1000-2286 2012 02-0382 - 06 Optimizing

Διαβάστε περισσότερα

FENXI HUAXUE Chinese Journal of Analytical Chemistry. Savitzky-Golay. n = SG SG. Savitzky-Golay mmol /L 5700.

FENXI HUAXUE Chinese Journal of Analytical Chemistry. Savitzky-Golay. n = SG SG. Savitzky-Golay mmol /L 5700. 38 2010 3 FENXI HUAXUE Chinese Journal of Analytical Chemistry 3 342 ~ 346 DOI 10. 3724 /SP. J. 1096. 2010. 00342 Savitzky-Golay 1 * 1 2 1 3 1 1 510632 2 510632 3 200444 PLS Savitzky-Golay SG 10000 ~ 5300

Διαβάστε περισσότερα

Electronic Supplementary Information

Electronic Supplementary Information Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2014 Electronic Supplementary Information Syntheses and structures of copper complexes of

Διαβάστε περισσότερα

Quantum dot sensitized solar cells with efficiency over 12% based on tetraethyl orthosilicate additive in polysulfide electrolyte

Quantum dot sensitized solar cells with efficiency over 12% based on tetraethyl orthosilicate additive in polysulfide electrolyte Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2017 Supplementary Information (SI) Quantum dot sensitized solar cells with

Διαβάστε περισσότερα

Preparation and performance of drug-loaded nano-hydroxyapatite/chitosan microspheres

Preparation and performance of drug-loaded nano-hydroxyapatite/chitosan microspheres 42 5 ( ) Vol.42 No.5 2011 5 Journal of Central South University (Science and Technology) May 2011 / 1, 2 1 1 1 (1. 430070 2. 430070) ph=11 W/O / / 1~10 µm 38.23% 54.21% 3 d 82% / R318 A 1672 7207(2011)05

Διαβάστε περισσότερα

Preparation of Hydroxyapatite Coatings on Enamel by Electrochemical Technique

Preparation of Hydroxyapatite Coatings on Enamel by Electrochemical Technique 25 7 2009 7 CHINESE JOURNAL OF INORGANIC CHEMISTRY Vol.25 No.7 1187~1193 1,2 *,1 1 ( 1, 361005) ( 2, 363105) : Ca(NO 3 ) 2 NH 4 H 2 PO 4 NaNO 3, (HA) X (XRD) (SEM) (EDS), ph (HA), HA c ph 6 0.5 ma cm -2

Διαβάστε περισσότερα

Recent advances in coal to chemicals technology developed by SINOPEC

Recent advances in coal to chemicals technology developed by SINOPEC 2013 Chinese Journal of Catalysis Vol. 34 No. 1 DOI: 10.3724/SP.J.1088.2013.21056 : 217 224 *,,, 201208 : : S-MTO ; ;. : ; ; ; ; ; : 2012-10-31. : 2012-12-03. : 2013-01-20. *. : (021)68463382; : (021)68462283;

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information Synthesis and Electroactive Properties of Poly(amidoamine) Dendrimers with an Aniline Pentamer Shell Wei-I Hung a, Chih-Bing Hung a, Ya-Han Chang a, Jiun-Kuang Dai a, Yan Li b, Hai

Διαβάστε περισσότερα

Fenton. COD ρ NH N TP ENVIRONMENTAL PROTECTION OF CHEMICAL INDUSTRY

Fenton. COD ρ NH N TP ENVIRONMENTAL PROTECTION OF CHEMICAL INDUSTRY COD TP DB32/ 939 6 Fenton ph 3.~3.5 H 2 O 2 3.8 ml/l FeSO 4 H 2 O.8 g/l1 min Fenton ph 7. 2 1 km 3 /d Fenton H 2 O 2 15 L/h FeSO 4 7H 2 O 7 L/h COD TP mg/l.4 mg/l.9 X73 A 6 1878 15 6 9 5 Research Institute

Διαβάστε περισσότερα

Stress Relaxation Test and Constitutive Equation of Saturated Soft Soil

Stress Relaxation Test and Constitutive Equation of Saturated Soft Soil 8 7 011 7 Journal of Highway and Transportation Research and Development Vol. 8 No. 7 Jul. 011 100-068 011 07-0014 - 05 1 1. 0009. 710064 k 0 Merchant 4 Merchant U416. 1 + 6 A Stress Relaxation Test and

Διαβάστε περισσότερα

Mean bond enthalpy Standard enthalpy of formation Bond N H N N N N H O O O

Mean bond enthalpy Standard enthalpy of formation Bond N H N N N N H O O O Q1. (a) Explain the meaning of the terms mean bond enthalpy and standard enthalpy of formation. Mean bond enthalpy... Standard enthalpy of formation... (5) (b) Some mean bond enthalpies are given below.

Διαβάστε περισσότερα

Studies on Synthesis and Biological Activities of 2( 1 H21,2,42 Triazol212yl)2 2Arylthioethyl Substituted Phenyl Ketones

Studies on Synthesis and Biological Activities of 2( 1 H21,2,42 Triazol212yl)2 2Arylthioethyl Substituted Phenyl Ketones 2002 60 7, 1303 1310 ACTA CHIMICA SINICA Vol. 60, 2002 No. 7, 1303 1310 2( 1 H21,2,42 212 )2 2 ( 300071) Ξ Ξ 22(1 H21,2,42 212 )222 212 (2) 1,42, 3,,. R 1, R 1 = (CH 3 ) 3 C, R 1 = Ar, Ar., 1,42,, Studies

Διαβάστε περισσότερα

Polymer-Based Composites with High Dielectric Constant and Low Dielectric Loss

Polymer-Based Composites with High Dielectric Constant and Low Dielectric Loss 22 8 2010 8 PROGRESS IN CHEMISTRY Vol. 22 No. 8 Aug. 2010 * 430070 TB33 TM215. 92 A 1005-281X 2010 08-1619-07 Polymer-Based Composites with High Dielectric Constant and Low Dielectric Loss Lu Pengjian

Διαβάστε περισσότερα

Approximation Expressions for the Temperature Integral

Approximation Expressions for the Temperature Integral 20 7Π8 2008 8 PROGRSS IN CHMISRY Vol. 20 No. 7Π8 Aug., 2008 3 3 3 3 3 ( 230026),,,, : O64311 ; O64213 : A : 10052281X(2008) 07Π821015206 Approimation pressions for the emperature Integral Chen Haiiang

Διαβάστε περισσότερα

- A. A Biphenol A BPA BPA BPA LLE 5 SPE Electrospinning Kang. Packed-fiber solid-phase extraction PFSPE 1 ml

- A. A Biphenol A BPA BPA BPA LLE 5 SPE Electrospinning Kang. Packed-fiber solid-phase extraction PFSPE 1 ml 38 200 4 FENXI HUAXUE Chinese Journal of Analytical Chemistry 4 503 ~ 507 DOI 0. 3724 /SP. J. 096. 200. 00503 6 - A * 2 2 * 2 20009 2 20096 6 - A ph 6 0 ml ph 8. 0 3 ml /min. 5 mg 6 300 μl A 6 0. 20 ~

Διαβάστε περισσότερα

LUO, Hong2Qun LIU, Shao2Pu Ξ LI, Nian2Bing

LUO, Hong2Qun LIU, Shao2Pu Ξ LI, Nian2Bing 2003 61 3, 435 439 ACTA CHIMICA SINICA Vol 61, 2003 No 3, 435 439 2 ΞΞ ( 400715), 2, 2, 2, 3/ 2 2,, 2,, Ne w Methods for the Determination of the Inclusion Constant between Procaine Hydrochloride and 2Cyclodextrin

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information Mitochondria-Targeting Polydopamine Nanocomposites as Chemophotothermal Therapeutics for Cancer Zhuo Wang *,, Yuzhi Chen, Hui Zhang, Yawen Li, Yufan Ma, Jia Huang, Xiaolei Liu, Fang

Διαβάστε περισσότερα

Reaction of a Platinum Electrode for the Measurement of Redox Potential of Paddy Soil

Reaction of a Platinum Electrode for the Measurement of Redox Potential of Paddy Soil J. Jpn. Soc. Soil Phys. No. +*0, p.- +*,**1 Eh * ** Reaction of a Platinum Electrode for the Measurement of Redox Potential of Paddy Soil Daisuke MURAKAMI* and Tatsuaki KASUBUCHI** * The United Graduate

Διαβάστε περισσότερα

Supplementary Data. Engineering, Nanjing University, Nanjing , P. R. China;

Supplementary Data. Engineering, Nanjing University, Nanjing , P. R. China; Supplementary Data Synthesis, Chemo-selective Properties of Substituted 9-Aryl-9H-fluorenes from Triarylcarbinols and Enantiomerical Kinetics of Chiral 9-Methoxy-11-(naphthalen-1-yl)-11H-benzo[a]fluorene

Διαβάστε περισσότερα

Rapid determination of soluble reactive silicate in seawater by flow injection analysis with spectrophotometric detection and its application

Rapid determination of soluble reactive silicate in seawater by flow injection analysis with spectrophotometric detection and its application 31 5 2011 5 Acta Scientiae Circumstantiae Vol 31 No 5 May 2011 2011 - J 31 5 935-940 Huang Y M Yuan D X Peng Y Z et al 2011 Rapid determination of soluble reactive silicate in seawater by flow injection

Διαβάστε περισσότερα

1 h, , CaCl 2. pelamis) 58.1%, (Headspace solid -phase microextraction and gas chromatography -mass spectrometry,hs -SPME - Vol. 15 No.

1 h, , CaCl 2. pelamis) 58.1%, (Headspace solid -phase microextraction and gas chromatography -mass spectrometry,hs -SPME - Vol. 15 No. 2 0 1 5 7 Journal of Chinese Institute of Food Science and Technology Vol. 15 No. 7 Jul. 2 0 1 5 1,2 1 1 1 1* ( 1 315211 2 315502) : ( ) : (E-Nose), - : GC-MS, 20.98% 2.5%, 53.15% 11.2%, 0. 51% 71.86%

Διαβάστε περισσότερα

Supporting Information. Enhanced energy storage density and high efficiency of lead-free

Supporting Information. Enhanced energy storage density and high efficiency of lead-free Supporting Information Enhanced energy storage density and high efficiency of lead-free CaTiO 3 -BiScO 3 dielectric ceramics Bingcheng Luo 1, Xiaohui Wang 1*, Enke Tian 2, Hongzhou Song 3, Hongxian Wang

Διαβάστε περισσότερα

Rapid Raman spectra identification and determination of levofloxacin hydrochloride injection *

Rapid Raman spectra identification and determination of levofloxacin hydrochloride injection * DOI:0.655/j.0254-793.20.09.039 75 * 2 2 3. 200435 2. 20203 3. 20000 ph R97 A 0254-793 20 09-75 - 05 Rapid Raman spectra identification and determination of levofloxacin hydrochloride injection * CHEN Bin

Διαβάστε περισσότερα

Supporting Information One-Pot Approach to Chiral Chromenes via Enantioselective Organocatalytic Domino Oxa-Michael-Aldol Reaction

Supporting Information One-Pot Approach to Chiral Chromenes via Enantioselective Organocatalytic Domino Oxa-Michael-Aldol Reaction Supporting Information ne-pot Approach to Chiral Chromenes via Enantioselective rganocatalytic Domino xa-michael-aldol Reaction Hao Li, Jian Wang, Timiyin E-Nunu, Liansuo Zu, Wei Jiang, Shaohua Wei, *

Διαβάστε περισσότερα

Supplementary Information

Supplementary Information Electronic upplementary Material (EI) for Photochemical & Photobiological ciences. This journal is The Royal ociety of Chemistry and wner ocieties 214 upplementary Information elective and sensitive fluorescence-shift

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information for Lewis acid-catalyzed redox-neutral amination of 2-(3-pyrroline-1-yl)benzaldehydes via intramolecular [1,5]-hydride shift/isomerization reaction Chun-Huan Jiang, Xiantao Lei,

Διαβάστε περισσότερα

Research on explaining porosity in carbonate reservoir by capture cross section method

Research on explaining porosity in carbonate reservoir by capture cross section method 33 4 2014 12 GLOBAL GEOLOGY Vol. 33 No. 4 Dec. 2014 1004-5589 2014 04-0875 - 05 1 2 1 2 1. 130026 2. 830011 PND SIGMA CATO SIGMA CNL 0. 91 SIGMA CATO P631. 325 A doi 10. 3969 /j. issn. 1004-5589. 2014.

Διαβάστε περισσότερα

c Key words: cultivation of blood, two-sets blood culture, detection rate of germ Vol. 18 No

c Key words: cultivation of blood, two-sets blood culture, detection rate of germ Vol. 18 No 2008 245 2 1) 1) 2) 3) 4) 1) 1) 1) 1) 1), 2) 1) 2) 3) / 4) 20 3 24 20 8 18 2001 2 2 2004 2 59.0 2002 1 2004 12 3 2 22.1 1 14.0 (CNS), Bacillus c 2 p 0.01 2 1 31.3 41.9 21.4 1 2 80 CNS 2 1 74.3 2 Key words:

Διαβάστε περισσότερα

8Q5SAC) 8Q5SAC UV2Vis 8500 ( ) ; PHS23C ) ;721 ( ) :1 4. ;8Q5SAC : molπl ;Britton2Robinson Q5SAC BSA Britton2Robinson,

8Q5SAC) 8Q5SAC UV2Vis 8500 ( ) ; PHS23C ) ;721 ( ) :1 4. ;8Q5SAC : molπl ;Britton2Robinson Q5SAC BSA Britton2Robinson, 31 2003 8 (FENXI HUAXUE) 8 Chinese Journal of Analytical Chemistry 976 980 22( 82 252 272 )21,82 23,62 3 (, 510631) 22(82 252 272 )21,82 23,62 (BSA), 8Q5SAC BSA 298K, 35 40 6. 1 10 5 LΠmol 8Q5SAC, ph =

Διαβάστε περισσότερα

Resurvey of Possible Seismic Fissures in the Old-Edo River in Tokyo

Resurvey of Possible Seismic Fissures in the Old-Edo River in Tokyo Bull. Earthq. Res. Inst. Univ. Tokyo Vol. 2.,**3 pp.,,3,.* * +, -. +, -. Resurvey of Possible Seismic Fissures in the Old-Edo River in Tokyo Kunihiko Shimazaki *, Tsuyoshi Haraguchi, Takeo Ishibe +, -.

Διαβάστε περισσότερα

Supporting information

Supporting information Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting information Copper-catalysed intramolecular O-arylation: a simple

Διαβάστε περισσότερα

Journal of Central South University (Science and Technology) May Bragg TU443 A (2011)

Journal of Central South University (Science and Technology) May Bragg TU443 A (2011) 42 5 ( ) Vol.42 No.5 2011 5 Journal of Central South University (Science and Technology) May 2011 Bragg 1 1 1 2 2 (1. 330099 2. 330038) ( ) D10 Bragg TU443 A 1672 7207(2011)05 1442 05 Fiber Bragg grating

Διαβάστε περισσότερα

ΜΕΛΕΤΗ ΤΗΣ ΠΛΑΣΤΙΚΟΤΗΤΑΣ ΑΡΓΙΛΟΥΧΩΝ ΜΙΓΜΑΤΩΝ ΜΕ ΠΡΟΣΘΗΚΗ ΣΙΔΗΡΑΛΟΥΜΙΝΑΣ ΑΠΟ ΤΗ ΔΙΕΡΓΑΣΙΑ BAYER

ΜΕΛΕΤΗ ΤΗΣ ΠΛΑΣΤΙΚΟΤΗΤΑΣ ΑΡΓΙΛΟΥΧΩΝ ΜΙΓΜΑΤΩΝ ΜΕ ΠΡΟΣΘΗΚΗ ΣΙΔΗΡΑΛΟΥΜΙΝΑΣ ΑΠΟ ΤΗ ΔΙΕΡΓΑΣΙΑ BAYER Πρακτικά 1ου Πανελληνίου Συνεδρίου για την Αξιοποίηση των Βιομηχανικών Παραπροϊόντων στη Δόμηση, ΕΒΙΠΑΡ, Θεσσαλονίκη, 24-26 Νοεμβρίου 2005 ΜΕΛΕΤΗ ΤΗΣ ΠΛΑΣΤΙΚΟΤΗΤΑΣ ΑΡΓΙΛΟΥΧΩΝ ΜΙΓΜΑΤΩΝ ΜΕ ΠΡΟΣΘΗΚΗ ΣΙΔΗΡΑΛΟΥΜΙΝΑΣ

Διαβάστε περισσότερα

Emulsifying Properties of Egg Yolk as a Function of Diacylglycerol Oil

Emulsifying Properties of Egg Yolk as a Function of Diacylglycerol Oil 354 Nippon Shokuhin Kagaku Kogaku Kaishi Vol. /-, No.0, -/.-0* (,**0) 38 * * Emulsifying Properties of Egg Yolk as a Function of Diacylglycerol Oil Tomoko Kawakami, Kyoko Ohashi* and Atsuko Shimada Graduate

Διαβάστε περισσότερα

*,* + -+ on Bedrock Bath. Hideyuki O, Shoichi O, Takao O, Kumiko Y, Yoshinao K and Tsuneaki G

*,* + -+ on Bedrock Bath. Hideyuki O, Shoichi O, Takao O, Kumiko Y, Yoshinao K and Tsuneaki G J. Hot Spring Sci. /2 +.,.,**2 + + + +, - +3 ++ -*,* + -+ Evaluation of the E# ect of Hyperthermia on Bedrock Bath Hideyuki O, Shoichi O, Takao O, Kumiko Y, Yoshinao K and Tsuneaki G + + + HNAMI KOUCHI

Διαβάστε περισσότερα

Protease-catalysed Direct Asymmetric Mannich Reaction in Organic Solvent

Protease-catalysed Direct Asymmetric Mannich Reaction in Organic Solvent Supplementary information for the paper Protease-catalysed Direct Asymmetric Mannich Reaction in Organic Solvent Yang Xue, Ling-Po Li, Yan-Hong He * & Zhi Guan * School of Chemistry and Chemical Engineering,

Διαβάστε περισσότερα

PACS: Pj, Gg

PACS: Pj, Gg * 1)2) 2) 3) 2) 1) 1) (, 310023 ) 2) (, 315211 ) 3) (, 510006 ) ( 2011 6 16 ; 2011 10 31 ),..,,.,.,. :,,, PACS: 07.05.Pj, 05.45.Gg 1,.,, [1,2].,,, [3,4].,, [5,6].,. [7 9]., [10 17].,.,, [10]., [18 20],

Διαβάστε περισσότερα

9-amino-(9-deoxy)cinchona alkaloids-derived novel chiral phase-transfer catalysts

9-amino-(9-deoxy)cinchona alkaloids-derived novel chiral phase-transfer catalysts Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 9-amino-(9-deoxy)cinchona alkaloids-derived novel chiral phase-transfer

Διαβάστε περισσότερα

Supporting Information. Asymmetric Binary-acid Catalysis with Chiral. Phosphoric Acid and MgF 2 : Catalytic

Supporting Information. Asymmetric Binary-acid Catalysis with Chiral. Phosphoric Acid and MgF 2 : Catalytic Supporting Information Asymmetric Binary-acid Catalysis with Chiral Phosphoric Acid and MgF 2 : Catalytic Enantioselective Friedel-Crafts Reactions of β,γ- Unsaturated-α-Ketoesters Jian Lv, Xin Li, Long

Διαβάστε περισσότερα

2 PbO 2. Pb 3 O 4 Sn. Ti/SnO 2 -Sb 2 O 4 -CF/PbO x SnO 2 -Sb PbO 2. Sn-Sb 1:1. 1 h. Sn:Sb=10:1. PbO 2 - CeO 2 PbO 2. [8] SnO 2 +Sb 2 O 4 _

2 PbO 2. Pb 3 O 4 Sn. Ti/SnO 2 -Sb 2 O 4 -CF/PbO x SnO 2 -Sb PbO 2. Sn-Sb 1:1. 1 h. Sn:Sb=10:1. PbO 2 - CeO 2 PbO 2. [8] SnO 2 +Sb 2 O 4 _ 41 Vol.41, No. 01 RARE METAL MATERIALS AND ENGINEERING March 01 Pb O 4 PbO ( 710049) SnO -Sb Pb O 4 Pb O 4 100.5 h 970 h XRF XRD SEM Pb O 4 PbO PbO TG146.1 + A 100-185X(01)0-046-05 [1,] 1 PbO PbO Sn-Sb

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information 2017 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim Convenient and General Zinc-Catalyzed Borylation of Aryl Diazonium Salts and Aryltriazenes under Mild Conditions

Διαβάστε περισσότερα

J. of Math. (PRC) 6 n (nt ) + n V = 0, (1.1) n t + div. div(n T ) = n τ (T L(x) T ), (1.2) n)xx (nt ) x + nv x = J 0, (1.4) n. 6 n

J. of Math. (PRC) 6 n (nt ) + n V = 0, (1.1) n t + div. div(n T ) = n τ (T L(x) T ), (1.2) n)xx (nt ) x + nv x = J 0, (1.4) n. 6 n Vol. 35 ( 215 ) No. 5 J. of Math. (PRC) a, b, a ( a. ; b., 4515) :., [3]. : ; ; MR(21) : 35Q4 : O175. : A : 255-7797(215)5-15-7 1 [1] : [ ( ) ] ε 2 n n t + div 6 n (nt ) + n V =, (1.1) n div(n T ) = n

Διαβάστε περισσότερα

Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes

Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes Supporting Information for Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes Changkun Li and Jianbo Wang* Beijing National Laboratory

Διαβάστε περισσότερα

Supporting Information. Microwave-assisted construction of triazole-linked amino acid - glucoside conjugates as novel PTP1B inhibitors

Supporting Information. Microwave-assisted construction of triazole-linked amino acid - glucoside conjugates as novel PTP1B inhibitors Supporting Information Microwave-assisted construction of triazole-linked amino acid - glucoside conjugates as novel PTP1B inhibitors Xiao-Peng He, abd Cui Li, d Xiao-Ping Jin, b Zhuo Song, b Hai-Lin Zhang,

Διαβάστε περισσότερα

Sulfonic acid-functionalized ionic liquid catalyzed hydrolysis of cellulose under microwave irradiation

Sulfonic acid-functionalized ionic liquid catalyzed hydrolysis of cellulose under microwave irradiation 34 3 Vol 34No 3 2011 8 Journal of Zhejiang Normal UniversityNat Sci Aug 2011 1001-5051201103-0311-06 * 1 2 1 1 1 3210042 361005 1- -3-1- -3-640 W 0 05 g 0 04 g 0 6 g 60 s O636 1 A Sulfonic acid-functionalized

Διαβάστε περισσότερα

1 (forward modeling) 2 (data-driven modeling) e- Quest EnergyPlus DeST 1.1. {X t } ARMA. S.Sp. Pappas [4]

1 (forward modeling) 2 (data-driven modeling) e- Quest EnergyPlus DeST 1.1. {X t } ARMA. S.Sp. Pappas [4] 212 2 ( 4 252 ) No.2 in 212 (Total No.252 Vol.4) doi 1.3969/j.issn.1673-7237.212.2.16 STANDARD & TESTING 1 2 2 (1. 2184 2. 2184) CensusX12 ARMA ARMA TU111.19 A 1673-7237(212)2-55-5 Time Series Analysis

Διαβάστε περισσότερα

21 2 No.2 Vol Journal of Chemical Engineering of Chinese Universities Apr PET/ATO

21 2 No.2 Vol Journal of Chemical Engineering of Chinese Universities Apr PET/ATO 21 2 No.2 Vol.21 2007 4 Journal of Chemical Engineering of Chinese Universities Apr. 2007 1003-9015(2007)02-0334-07 PET/ATO,, (, 200237) (ATO) (EG) EG (TPA) (PET)/ATO SEM DSC XRD FTIR TGA ATO PET PET/ATO

Διαβάστε περισσότερα

A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes

A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes

Διαβάστε περισσότερα

Supporting information. An unusual bifunctional Tb-MOF for highly sensing of Ba 2+ ions and remarkable selectivities of CO 2 /N 2 and CO 2 /CH 4

Supporting information. An unusual bifunctional Tb-MOF for highly sensing of Ba 2+ ions and remarkable selectivities of CO 2 /N 2 and CO 2 /CH 4 Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2015 Supporting information An unusual bifunctional Tb-MOF for highly sensing

Διαβάστε περισσότερα

,,, (, 100875) 1989 12 25 1990 2 23, - 2-4 ;,,, ; -

,,, (, 100875) 1989 12 25 1990 2 23, - 2-4 ;,,, ; - 25 3 2003 5 RESOURCES SCIENCE Vol. 25 No. 3 May 2003 ( 100875) : 500L - 2-4 - 6-8 - 10 114h - 120h 6h 1989 12 25 1990 2 23-2 - 4 : ; ; - 4 1186cm d - 1 10cm 514d ; : 714 13 317 714 119 317 : ; ; ; :P731

Διαβάστε περισσότερα

Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via double C(sp 2 )-H thiolation

Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via double C(sp 2 )-H thiolation Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via

Διαβάστε περισσότερα

1010 C 73 H 108 O 12. FENXI HUAXUE Chinese Journal of Analytical Chemistry 399 ~ HPLC. PDA 282 nm PP 1010 Weibull PP PP.

1010 C 73 H 108 O 12. FENXI HUAXUE Chinese Journal of Analytical Chemistry 399 ~ HPLC. PDA 282 nm PP 1010 Weibull PP PP. 43 2015 3 FENXI HUAXUE Chinese Journal of Analytical Chemistry 3 399 ~ 403 DOI 10. 11895 /j. issn. 0253-3820. 140659 1 2 1 2 2 2 * 1 1 100081 2 100089 PP 2 6- BHT 3 5- -4-1010 190 PP 0. 1 mm HPLC PDA 282

Διαβάστε περισσότερα

Rh(III)-Catalyzed C-H Amidation with N-hydroxycarbamates: A. new Entry to N-Carbamate Protected Arylamines

Rh(III)-Catalyzed C-H Amidation with N-hydroxycarbamates: A. new Entry to N-Carbamate Protected Arylamines Rh(III)-Catalyzed C-H Amidation with N-hydroxycarbamates: A new Entry to N-Carbamate Protected Arylamines Bing Zhou,* Juanjuan Du, Yaxi Yang,* Huijin Feng, Yuanchao Li Shanghai Institute of Materia Medica,

Διαβάστε περισσότερα

PNS mg kg - 1. Rb 1

PNS mg kg - 1. Rb 1 94 2 3 3. 53002 2. 53000 3. 543000 86. 2 mg kg -. 8 mg kg - R Rg Rb 3P97 AUC 0 - R Rg Rb R 0. 8 ± 0. 09 vs 0. 6 ± 0. 06 h Rg 2. 03 ± 0. 76 vs. 74 ± 0. 27 h Rb 0. 76 ± 0. 39 vs 0. 74 ± 0. 7 h R 0. 96 ±

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information Lewis acid catalyzed ring-opening reactions of methylenecyclopropanes with diphenylphosphine oxide in the presence of sulfur or selenium Min Shi,* Min Jiang and Le-Ping Liu State

Διαβάστε περισσότερα

Supplementary material

Supplementary material Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2015 Supplementary material Recyclable

Διαβάστε περισσότερα

and Selective Allylic Reduction of Allylic Alcohols and Their Derivatives with Benzyl Alcohol

and Selective Allylic Reduction of Allylic Alcohols and Their Derivatives with Benzyl Alcohol FeCl 3 6H 2 O-Catalyzed Disproportionation of Allylic Alcohols and Selective Allylic Reduction of Allylic Alcohols and Their Derivatives with Benzyl Alcohol Jialiang Wang, Wen Huang, Zhengxing Zhang, Xu

Διαβάστε περισσότερα

Comparison of HPLC fingerprint between enzymatic Calculus bovis and natural Calculus bovis

Comparison of HPLC fingerprint between enzymatic Calculus bovis and natural Calculus bovis HPLC * 271016 HPLC - DAD DiamonsilC 18 250 mm 4. 6 mm 5 μm - -1% 370 nm 1. 0 ml /min 40 R282. 7 A 1001-1528 2011 01-0001-05 Comparison of HPLC fingerprint between enzymatic Calculus bovis and natural Calculus

Διαβάστε περισσότερα

Screening of Respiration-deficient Saccharomyces cerevisiae Strains with Sugar-and Thermo-tolerances

Screening of Respiration-deficient Saccharomyces cerevisiae Strains with Sugar-and Thermo-tolerances 3 3 Vol3 No3 3 9 Life Science Research June 9 *,,, 535 :, 3, 5- (TTC), 3,, T,, ; (5~5 μ 375~5 μ),, 5% (W/V), 55,, 55% 9% : ; ; ; ; :Q39 + :A :7-77(9)3-99-5 Screening of Respiration-deficient Saccharomyces

Διαβάστε περισσότερα

Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic acids with the assistance of isocyanide

Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic acids with the assistance of isocyanide Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic

Διαβάστε περισσότερα

Preparation and Application of Amorphous Alloy Catalyst

Preparation and Application of Amorphous Alloy Catalyst 17 4 2005 7 PROGRESS IN CHEMISTRY Vol. 17 No. 4 Jul., 2005 3 ( 300072), XRD EXAFS DSC SEM TEM XPS : O643136 ; TQ42618 : A : 10052281X(2005) 0420614208 Preparation and Application of Amorphous Alloy Catalyst

Διαβάστε περισσότερα

Computational study of the structure, UV-vis absorption spectra and conductivity of biphenylene-based polymers and their boron nitride analogues

Computational study of the structure, UV-vis absorption spectra and conductivity of biphenylene-based polymers and their boron nitride analogues Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Computational study of the structure, UV-vis absorption spectra and conductivity of biphenylene-based

Διαβάστε περισσότερα

Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3

Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3 Supporting Information Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3 Shohei Shimokawa, Yuhsuke Kawagoe, Katsuhiko Moriyama, Hideo Togo* Graduate

Διαβάστε περισσότερα

Nguyen Hien Trang* **

Nguyen Hien Trang* ** 152 Nippon Shokuhin Kagaku Kogaku Kaishi Vol.., No.., +,+3 (,**1) 10 Nguyen Hien Trang* ** * Department of Food Science and Technology, Hue University of Agriculture and Forestry ** Properties of "Shishibishio

Διαβάστε περισσότερα

ΜΕΤΑΠΤΥΧΙΑΚΗ ΕΡΕΥΝΗΤΙΚΗ ΔΙΑΤΡΙΒΗ

ΜΕΤΑΠΤΥΧΙΑΚΗ ΕΡΕΥΝΗΤΙΚΗ ΔΙΑΤΡΙΒΗ ΓΕΩΠΟΝΙΚΟ ΠΑΝΕΠΙΣΤΗΜΙΟ ΑΘΗΝΩΝ ΤΜΗΜΑ ΕΠΙΣΤΗΜΗΣ & ΤΕΧΝΟΛΟΓΙΑΣ ΤΡΟΦΙΜΩΝ ΕΡΓΑΣΤΗΡΙΟ ΠΟΙΟΤΙΚΟΥ ΕΛΕΓΧΟΥ & ΥΓΙΕΙΝΗΣ ΤΡΟΦΙΜΩΝ ΚΑΙ ΠΟΤΩΝ Π.Μ.Σ. «ΕΠΙΣΤΗΜΗ & ΤΕΧΝΟΛΟΓΙΑ ΤΡΟΦΙΜΩΝ & ΔΙΑΤΡΟΦΗ ΤΟΥ ΑΝΘΡΩΠΟΥ» Η ΕΠΙΔΡΑΣΗ

Διαβάστε περισσότερα

Supplementary Information. Living Ring-Opening Polymerization of Lactones by N-Heterocyclic Olefin/Al(C 6 F 5 ) 3

Supplementary Information. Living Ring-Opening Polymerization of Lactones by N-Heterocyclic Olefin/Al(C 6 F 5 ) 3 Supplementary Information Living Ring-Opening Polymerization of Lactones by N-Heterocyclic Olefin/Al(C 6 F 5 ) 3 Lewis Pairs: Structures of Intermediates, Kinetics, and Mechanism Qianyi Wang, Wuchao Zhao,

Διαβάστε περισσότερα

Application of Wavelet Transform in Fundamental Study of Measurement of Blood Glucose Concentration with Near2Infrared Spectroscopy

Application of Wavelet Transform in Fundamental Study of Measurement of Blood Glucose Concentration with Near2Infrared Spectroscopy 37 6 2004 6 Journal of Tianjin University Vol. 37 No. 6 Jun. 2004 Ξ 1,2, 1,2, 3 (1., 300072 ; 2. 2, 300072 ; 3., 300072) :,,,.,,(RMSEP) 53 %58 %.. : ; ; : O657. 33 : A : 04932 2137 (2004) 062 05352 05

Διαβάστε περισσότερα

Preparation and Characterization of Solid Dispersion of Total Flavonols from Resina Draconis

Preparation and Characterization of Solid Dispersion of Total Flavonols from Resina Draconis 37 1 Vol37 No1 2018 3 Journal of South-Central University for NationalitiesNatSciEdition Mar2018 * 430074 RDF K30PVP K30 188F68 X XRD IR DSC SEM TFDB PVP K30 F68 181 F68 K30 188 TQ461 A 1672-4321201801-0061-05

Διαβάστε περισσότερα

CorV CVAC. CorV TU317. 1

CorV CVAC. CorV TU317. 1 30 8 JOURNAL OF VIBRATION AND SHOCK Vol. 30 No. 8 2011 1 2 1 2 2 1. 100044 2. 361005 TU317. 1 A Structural damage detection method based on correlation function analysis of vibration measurement data LEI

Διαβάστε περισσότερα

Vol. 31,No JOURNAL OF CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY Feb

Vol. 31,No JOURNAL OF CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY Feb Ξ 31 Vol 31,No 1 2 0 0 1 2 JOURNAL OF CHINA UNIVERSITY OF SCIENCE AND TECHNOLOGY Feb 2 0 0 1 :025322778 (2001) 0120016205 (, 230026) : Q ( m 1, m 2,, m n ) k = m 1 + m 2 + + m n - n : Q ( m 1, m 2,, m

Διαβάστε περισσότερα

Supporting Information

Supporting Information Supporting Information Copper/Silver Cocatalyzed Oxidative Coupling of Vinylarenes with ICH 2 CF 3 or ICH 2 CHF 2 Leading to β-cf 3 /CHF 2 -Substituted Ketones Niannian Yi, Hao Zhang, Chonghui Xu, Wei

Διαβάστε περισσότερα

No. 7 Modular Machine Tool & Automatic Manufacturing Technique. Jul TH166 TG659 A

No. 7 Modular Machine Tool & Automatic Manufacturing Technique. Jul TH166 TG659 A 7 2016 7 No. 7 Modular Machine Tool & Automatic Manufacturing Technique Jul. 2016 1001-2265 2016 07-0122 - 05 DOI 10. 13462 /j. cnki. mmtamt. 2016. 07. 035 * 100124 TH166 TG659 A Precision Modeling and

Διαβάστε περισσότερα

Nuclear Physics 5. Name: Date: 8 (1)

Nuclear Physics 5. Name: Date: 8 (1) Name: Date: Nuclear Physics 5. A sample of radioactive carbon-4 decays into a stable isotope of nitrogen. As the carbon-4 decays, the rate at which the amount of nitrogen is produced A. decreases linearly

Διαβάστε περισσότερα

2 1, 2 A 2F 10 : : 00 1A01 C 4F B 5F 10 : : 40 1B01 1C01 1A02 1C02 BC2N 1B02 1B04. 1A03 C/N Fe 1C03. 1C04 DNA Somlak Ittisanronnnachai

2 1, 2 A 2F 10 : : 00 1A01 C 4F B 5F 10 : : 40 1B01 1C01 1A02 1C02 BC2N 1B02 1B04. 1A03 C/N Fe 1C03. 1C04 DNA Somlak Ittisanronnnachai A 2F 10 : 0012 : 00 1A01 1A02 1 2 1 1 1 2 2 2 2 1A03 C/N Fe 1A04 1A05 EDL 1 2 1 2 2 1 1 1 1A06 12 1 B 10 : 0011 : 40 1B01 1B02 / 1B04 1 2 1 2 1 1 1 1 1, 2 1B05 1 2 1 2 1 1B06 N- 1 2 1, 2 1 CHA IN OH 1

Διαβάστε περισσότερα

Comparison of Evapotranspiration between Indigenous Vegetation and Invading Vegetation in a Bog

Comparison of Evapotranspiration between Indigenous Vegetation and Invading Vegetation in a Bog J. Jpn. Soc. Soil Phys. No. +*-, p.-3.1,**0 ** * *** Comparison of Evapotranspiration between Indigenous Vegetation and Invading Vegetation in a Bog Toshiki FUJIMOTO*, Ippei IIYAMA*, Mai SAKAI*, Osamu

Διαβάστε περισσότερα

) ; GSP ) ;PXD g, 100 ml

) ; GSP ) ;PXD g, 100 ml 30 (FENXI HUAXUE) 10 2002 10 Chinese Journal of Analytical Chemistry 1163 1167 3 3 3 (, 225002) PVC, 1. 0 10-4 1. 0 10-8 molπl, 58. 6 mvπdecade ; 2. 5 10-9 molπl, 2 3,,,,, 1, PVC Pretsch 1, EDTA,, 5 10-12

Διαβάστε περισσότερα

Polyvinyl Chloride PVC, The effects of organotin thermal stabilizers on the dehydrochlorination of TPUΠPVC blends

Polyvinyl Chloride PVC, The effects of organotin thermal stabilizers on the dehydrochlorination of TPUΠPVC blends No. 4 J ul.,2004 Polyvinyl Chloride 4 2004 7 TPUΠPVC Ξ,, (, 210009) [ ] [ ] Π,, :,, 395A T - 137 DB TL CaSt 2, [ ] TQ325. 3 TQ328. 3 [ ] A [ ] 1009-7937 (2004) 04-0028 - 06 The effects of organotin thermal

Διαβάστε περισσότερα

Room Temperature Highly Diastereoselective Zn-Mediated. Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled

Room Temperature Highly Diastereoselective Zn-Mediated. Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled Supporting Information for: Room Temperature Highly Diastereoselective Zn-Mediated Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled Stereoselectivity Reversal

Διαβάστε περισσότερα

ΦΙΛΙΚΗ ΠΡΟΣ ΤΟ ΠΕΡΙΒΑΛΛΟΝ ΧΗΜΙΚΗ ΑΝΑΚΥΚΛΩΣΗ ΦΙΑΛΩΝ ΑΠΟ ΡΕΤ ΜΕ ΧΡΗΣΗ ΜΙΚΡΟΚΥΜΑΤΩΝ

ΦΙΛΙΚΗ ΠΡΟΣ ΤΟ ΠΕΡΙΒΑΛΛΟΝ ΧΗΜΙΚΗ ΑΝΑΚΥΚΛΩΣΗ ΦΙΑΛΩΝ ΑΠΟ ΡΕΤ ΜΕ ΧΡΗΣΗ ΜΙΚΡΟΚΥΜΑΤΩΝ ΦΙΛΙΚΗ ΠΡΟΣ ΤΟ ΠΕΡΙΒΑΛΛΟΝ ΧΗΜΙΚΗ ΑΝΑΚΥΚΛΩΣΗ ΦΙΑΛΩΝ ΑΠΟ ΡΕΤ ΜΕ ΧΡΗΣΗ ΜΙΚΡΟΚΥΜΑΤΩΝ ηµήτρης Σ. Αχιλιάς*, Γεωργία Π. Τσίντζου, Αλέξανδρος Κ. Νικολαϊδης, Γιώργος Π. Καραγιαννίδης Εργαστήριο Οργανικής Χηµικής

Διαβάστε περισσότερα

ΠΑΡΑΣΚΕΥΗ ΝΑΝΟΣΥΝΘΕΤΩΝ ΒΙΟΔΡΑΣΤΙΚΟΥ ΓΥΑΛΙΟΥ/ΠΟΛΥ(D,L-ΓΑΛΑΚΤΙΚΟΥ ΟΞΕΟΣ) ΚΑΙ IN- VITRO ΜΕΛΕΤΗ ΤΗΣ ΒΙΟΣΥΜΒΑΤΟΤΗΤΑΣ

ΠΑΡΑΣΚΕΥΗ ΝΑΝΟΣΥΝΘΕΤΩΝ ΒΙΟΔΡΑΣΤΙΚΟΥ ΓΥΑΛΙΟΥ/ΠΟΛΥ(D,L-ΓΑΛΑΚΤΙΚΟΥ ΟΞΕΟΣ) ΚΑΙ IN- VITRO ΜΕΛΕΤΗ ΤΗΣ ΒΙΟΣΥΜΒΑΤΟΤΗΤΑΣ ΕΘΝΙΚΟ ΜΕΤΣΟΒΙΟ ΠΟΛΥΤΕΧΝΕΙΟ ΣΧΟΛΗ ΧΗΜΙΚΩΝ ΜΗΧΑΝΙΚΩΝ ΤΟΜΕΑΣ IV: ΣΥΝΘΕΣΗ ΚΑΙ ΑΝΑΠΤΥΞΗ ΒΙΟΜΗΧΑΝΙΚΩΝ ΔΙΑΔΙΚΑΣΙΩΝ ΕΡΓΑΣΤΗΡΙΟ ΤΕΧΝΟΛΟΓΙΑΣ ΠΟΛΥΜΕΡΩΝ Διπλωματική Εργασία ΠΑΡΑΣΚΕΥΗ ΝΑΝΟΣΥΝΘΕΤΩΝ ΒΙΟΔΡΑΣΤΙΚΟΥ ΓΥΑΛΙΟΥ/ΠΟΛΥ(D,L-ΓΑΛΑΚΤΙΚΟΥ

Διαβάστε περισσότερα

Enantioselective Organocatalytic Michael Addition of Isorhodanines. to α, β-unsaturated Aldehydes

Enantioselective Organocatalytic Michael Addition of Isorhodanines. to α, β-unsaturated Aldehydes Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2016 Enantioselective Organocatalytic Michael Addition of Isorhodanines to α,

Διαβάστε περισσότερα

Advance in Nanorealgar Studies

Advance in Nanorealgar Studies 21 5 2009 5 PROGRESS IN CHEMISTRY Vol. 21 No. 5 May, 2009 1 1 2 3 (1. 430074 ; 2. 430074),,, ;,, : O61316 ; R284 : A : 10052281X(2009) 0520934206 Advance in Nanorealgar Studies Ye Xiaochuan 1 Yang Xiangliang

Διαβάστε περισσότερα

ect of Modified Wheat Starches on the Textural Properties of Baked Products, such as Cookies

ect of Modified Wheat Starches on the Textural Properties of Baked Products, such as Cookies 224 Nippon Shokuhin Kagaku Kogaku Kaishi Vol. // No. /. - (**2) 22 * * E# ect of Modified Wheat Starches on the Textural Properties of Baked Products such as Cookies Atsuko Higo and Yoshiko Wada* Bunkyo

Διαβάστε περισσότερα

Apr Vol.26 No.2. Pure and Applied Mathematics O157.5 A (2010) (d(u)d(v)) α, 1, (1969-),,.

Apr Vol.26 No.2. Pure and Applied Mathematics O157.5 A (2010) (d(u)d(v)) α, 1, (1969-),,. 2010 4 26 2 Pure and Applied Matheatics Apr. 2010 Vol.26 No.2 Randić 1, 2 (1., 352100; 2., 361005) G Randić 0 R α (G) = v V (G) d(v)α, d(v) G v,α. R α,, R α. ; Randić ; O157.5 A 1008-5513(2010)02-0339-06

Διαβάστε περισσότερα

Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information

Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans Liang Yun, Shi Tang, Xu-Dong Zhang, Li-Qiu Mao, Ye-Xiang Xie and Jin-Heng Li* Key Laboratory

Διαβάστε περισσότερα

ACTA POLYMERICA SINICA

ACTA POLYMERICA SINICA 12 2010 12 ACTA POLYMERICA SINICA No 12 Dec 2010 * 1 1 1 2 2 1 200433 2 200032 SF 3- -co-3- PHBHHx PHBHHx 90 51 37 9 mj / m 2 57 4 mj / m 2 PHBHHx HUVECs MTT 3 5 7 SF PHBHHx PHBHHx 5 PHBHHx HUVECs ECM

Διαβάστε περισσότερα