. SBA-15 NH2-SBA-15 / / Si-OH (MCM-50) B (B010 EO16 ), P123,.[ ] (P85, P65, Brij97(C18 H35 EO10 SBA MDA-SBA-15
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1 - - a_shahbazi@sbu.ac.ir() - ( ) - (// // ) SBA-15.. (MDA-SBA-15) (NH2-SBA-15) FT-IR XRD. MDA-SBA-15. BET SEM. SBA-15 NH2-SBA-15 / /. -. MDA-SBA-15 MDA-SBA-15. MDA-SBA-15. MDA-SBA-15 NH2-SBA-15 SBA-15 : Si-OH...[].[].[] -. /. (MCM-48) (SBA-15 MCM-41) (MCM-50) SBA-15. B (B010 EO16 ), P123,.[] (P85, P65, Brij97(C18 H35 EO10. 19
2 ...[].[]..[ ]..[].. ( ).[] SBA-15.[] SBA-15 SBA-. 15.[] MDA-SBA-15. MDA.[] : ) SBA-15 (. MDA- NH2-SBA-15 SBA SBA-15 SBA-15 P123 /.[ ] / /... ) /.. (... SBA-15 SBA-15 (NH2-SBA-15) ).(.[] NH2-SBA-15.[ ] SBA-15 MDA-SBA-15) 30). NH2-SBA-15.. SBA
![-- NH2-SBA-SBA-15 MDA-SBA-15 15...[]. (λmax).() / / ph. λmax (q).](/docs-images/72/67308870/images/3-0.jpg "-- (XRD) SBA-15. SEM LEO SBA-15. (BET) FT-IR.")
3 -- NH2-SBA-SBA-15 MDA-SBA []. (λmax).() / / ph. λmax (q). -- (XRD) SBA-15. SEM LEO SBA-15. (BET) FT-IR.. - Mthyln Blu / - ( ) (Å) λ () SBA-15-1 Philips X'prt MPD Diffractomtr, Holland - 2 SEM, LEO 1455VP, Cambridg, U.K 3 BELsorp-mini II Volumtric Adsorption Analyzr, Japan 4 Brukr Vctor 22 Infrard Spctrophotomtr 21
4 nf 1/nF K F ( ). RT RT q = ln AT + bt bt LnC BT(RT/bT () AT.[] :D-R 2 ln q = ln qm kε () q m k ε ε=rtln(1+ 1 ) ) C R ( T. (/J/mol K) SBA 15 SBA 15 SEM. SBA 15 q (C0 C)V = W C C R% = C 0 * 100 () () R q C C o W V MDA-SBA-15. q qmklc = 1+ K C L () q m q C K L. R L R L 1 = () 1+ BC 0 SEM - SBA 15 (RL>1) RL (RL = 0) (RL<1> ) (RL= 1). q = K C () F 1/ nf 22
5 ) (- ) (. SBA 15.. MDA MDA SBA 15 XRD MDA.[] SBA SBA 15 IV.[] SBA 15 ( P/P0= -/) ( ).(-). SBA 15 BET. P/P0= /-/. SBA 15 P/P0 >/.. P/P0= / SBA 15 BET SBA 15 BJH.[ ]. / XRD. / SBA 15 () -. SBA 15. SBA 15 SBA 15.[] --- XRD - MDA SBA 15 ( : (2 APTES (CC ) ( CC-SBA-15 XRD.. SBA 15 SBA 15 () :- - MDA SBA 15 () CC SBA 15 () NH2 SBA 15() 23
6 . MDA SBA 15.[] FTIR --- SBA 15 FTIR SBA SBA 15 - MDA SBA 15 (cm 3 /g) / / / / 2000 (nm) / / / / ѵ(nh 2 ) ѵ(c=n) (cm -1 ) (m 2 /g) ѵ(si O Si) 950 SBA 15 NH 2 SBA 15 CC SBA 15 MDA SBA Transmittanc (a.u) NH 2 () SBA 15 () :FTIR - MDA SBA 15() SBA 15 (cm 3 /g STP) Adsorption Dsorption (p/p 0 ) SBA 15 () : - - () CC SBA 15 () NH 2 SBA 15() MDA SBA 15.[] BET - MDA SBA 15 IV SBA 15. H1.[] SBA 15. SBA 15.[]. SBA 15. MDA SBA 15 SBA 15 MDA SBA 15 24
7 MDA-SBA-15. R q MDA-SBA ( R 2 >/).(- ). MDA-SBA-15. MDA-SBA RL. MDA-SBA-15 nf - / K L (l/mg) / R L / R 2 / K F ((mg/g)(l/mg)) / n F / R 2 q m (mg/g) / β - E / R 2 / A T (l/mg) / b T / R 2 SBA 15 ( Si O Si ). NH2 N H.(- ) MDA SBA 15 C=N FTIR.( - ).[ ] -- MDA-SBA-15 NH2-SBA-15 SBA-15. (SBA-15) SBA-15./. SBA-15. / SBA / / ph) ( 25
8 . BT. RL MDA-SBA [] β (E). E = 1 2B (). E E E.[]. / ].[ () - - ( ( ( SBA-15 - ph Dos(g/l) T C o (mg/l) q (mg/g) [] / / / [] - [] - - / [] / [] - - / / / / / / / / MCM-48 MCM-41 MCM-41 SBA-15 SBA-15 NH 2 -SBA-15 MDA-SBA-15 26
9 MDA- NH2-SBA-15) / (SBA-15.. MDA-SBA-15. BT.. MDA-SBA " ". -. MDA-SBA / ) MCM-41 ( /) MCM-48 ( /) (. / SBA-15 MDA. -.. SEM BET XRD FT-IR SBA Chw, T. L., Ahmad, A. L., and Bhatia, S. (2010). Ordrd msoporous silica (OMS) as an adsorbnt and mmbran for sparation of carbon dioxid (CO 2 ). Advancs in Colloid and Intrfac Scinc, 153(1-2), Karim, A. H., Jalil, A. A., Triwahyono, S., Sidik, S. M., Kamarudin, N. H. N., Jusoh, R., t al. (2012). Amino modifid msostructurd silica nanoparticls for fficint adsorption of mthyln blu. J. of Colloid and Intrfac Scinc, 386(1), Dbnath, S., Kitinya, J., and Onyango, M. S. (2014). Rmoval of Congo rd from aquous solution by two variants of calcium and iron basd mixd oxid nano-particl agglomrats. J. of Industrial and Enginring Chmistry, 20(4), Nayab, S., Farrukh, A., Oluz, Z., Tuncl, E., Tariq, S. R., Rahman, H. U., t al. (2014). Dsign and fabrication of branchd polyamin functionalizd msoporous silica: An fficint absorbnt for watr rmdiation. ACS Applid Matrials and Intrfacs, 6(6), Chn, Z., Zhou, L., Zhang, F., Yu, C., and Wi, Z. (2012). Multicarboxylic hyprbranchd polyglycrol modifid SBA-15 for th adsorption of cationic dys and coppr ions from aquous mdia. Applid Surfac Scinc, 258(13), Huang, C. H., Chang, K. P., Ou, H. D., Chiang, Y. C., and Wang, C. F. (2011). Adsorption of cationic dys onto msoporous silica. Microporous and Msoporous Matrials, 141(1-3),
10 7. Shahbazi, A., Younsi, H., and Badii, A. (2011). Functionalizd SBA-15 msoporous silica by mlaminbasd dndrimr amins for adsorptiv charactristics of Pb(II), Cu(II) and Cd(II) havy mtal ions in batch and fixd bd column. Chmical Enginring Journal, 168(2), Zhao, D., Fng, J., Huo, Q., Mlosh, N., Frdrickson, G. H., Chmlka, B. F., t al. (1998). Triblock copolymr synthss of msoporous silica with priodic 50 to 300 angstrom pors. Scinc, 279(5350), Mahmoodi, N. M., Khorramfar, S., and Najafi, F. (2011). Amin-functionalizd silica nanoparticl: Prparation, charactrization and anionic dy rmoval ability. Dsalination, 279(1-3), Ho, K. Y., McKay, G., and Yung, K. L. (2003). Slctiv adsorbnts from ordrd msoporous silica. Langmuir, 19(7), Graham, N., Chn, X., and Jayaslan, S. (2001). Th potntial application of activatd carbon from swag sludg to organicdys rmoval. Watr Scinc and Tchnology, 43(2), Liang, Z., Fadhl, B., Schnidr, C. J., and Chaff, A. L. (2008). Stpwis growth of mlamin-basd dndrimrs into msopors and thir CO 2 adsorption proprtis. Microporous and Msoporous Matrials, 111(1), Huang, C.-H., Chang, K.-P., Ou, H.-D., Chiang, Y.-C., Chang, E.-E., and Wang, C.-F. (2011). Charactrization and application of Ti-containing msoporous silica for dy rmoval with synrgistic ffct of coupld adsorption and photocatalytic oxidation. J. of Hazardous Matrials, 186(2-3), Acosta, E. J., Carr, C. S., Simank, E. E., and Shantz, D. F. (2004). Enginring nanospacs: Itrativ synthsis of mlamin basd dndrimrs on amin functionalizd SBA 15 lading to complx hybrids with controllabl chmistry and porosity. Advancd Matrials, 16(12), Wang, L., and Yang, R. T. (2011). Incrasing slctiv CO 2 adsorption on amin-graftd SBA-15 by incrasing silanol dnsity. Th Journal of Physical Chmistry C, 115(43), Da na, E., and Sayari, A. (2011). Adsorption of coppr on amin-functionalizd SBA-15 prpard by cocondnsation: Equilibrium proprtis. Chmical Enginring Journal, 166(1), Albadarin, A. B., Mangwandi, C., Al-Muhtasb, A. A. H., Walkr, G. M., Alln, S. J., and Ahmad, M. N.(2012). Kintic and thrmodynamics of chromium ions adsorption onto low-cost dolomit adsorbnt. Chmical Enginring Journal, 179, Yang, Y., Wang, G., Wang, B., Li, Z., Jia, X., Zhou, Q., t al. (2011). Biosorption of acid black 172 and Congo Rd from aquous solution by nonviabl Pnicillium YW 01: Kintic study, quilibrium isothrm and artificial nural ntwork modling. Biorsourc Tchnology, 102(2), Doğan, M., Abak, H., and Alkan, M. (2008). Biosorption of mthyln blu from aquous solutions by hazlnut shlls: Equilibrium, paramtrs and isothrms. Watr, Air, and Soil Pollution, 192(1-4), Liu, Y., Zhng, Y., and Wang, A. (2010). Enhancd adsorption of Mthyln Blu from aquous solution by chitosan-g-poly (acrylic acid)/vrmiculit hydrogl composits. J. of Environmntal Scincs, 22(4), Vargas, A. M., Caztta, A. L., Kunita, M. H., Silva, T. L., and Almida, V. C. (2011). Adsorption of mthyln blu on activatd carbon producd from flamboyant pods (Dlonix rgia): Study of adsorption isothrms and kintic modls. Chmical Enginring Journal, 168(2), Wang, S., and Li, H. (2006). Structur dirctd rvrsibl adsorption of organic dy on msoporous silica in aquous solution. Microporous and Msoporous Matrials, 97(1-3), Monash, P., and Pugazhnthi, G. (2010). Invstigation of quilibrium and kintic paramtrs of mthyln blu adsorption onto MCM-41. Koran Journal of Chmical Enginring, 27(4), Karagöz, S., Tay, T., Ucar, S., and Erdm, M. (2008). Activatd carbons from wast biomass by sulfuric acid activation and thir us on mthyln blu adsorption. Biorsourc Tchnology, 99(14),
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Supporting Information Wiley-VCH 27 69451 Weinheim, Germany Supplementary Figure 1. Synthetic results as detected by XRD (Cu-Kα). Simulation pattern of MCM-68 Relative Intensity / a.u. YNU-2P Conventional
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