Photostimulated Reduction of Nitriles by SmI 2. Supporting information

Σχετικά έγγραφα
Structural Expression of Exo-Anomeric Effect

Supporting Information. DFT Study of Pd(0)-Promoted Intermolecular C H Amination with. O-Benzoyl Hydroxylamines. List of Contents

Electronic Supplementary Information

Ethyl Nitroacetate in Aza-Henry Addition on Trifluoromethyl Aldimines: A Solvent-Free Procedure To Obtain Chiral Trifluoromethyl α,β-diamino Esters

Electronic Supplementary Information

Bifunctional Water Activation for Catalytic Hydration of Organonitriles

Alkyl-functionalization of 3,5-bis(2-pyridyl)-1,2,4,6- thiatriazine

Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2006

Supporting Information. A single probe to sense Al(III) colorimetrically and. Cd(II) by turn-on fluorescence in physiological

Mild Aliphatic and Benzylic hydrocarbon C H Bond Chlorination Using Trichloroisocyanuric Acid (TCCA)

Striking Difference between Succinimidomethyl and Phthalimidomethyl Radicals in Conjugate Addition to Alkylidenemalonate Initiated by Dimethylzinc

Electronic Supplementary Material (ESI) for Chemical Communications This journal is The Royal Society of Chemistry 2013

A Selective, Sensitive, Colorimetric and Fluorescence Probe. for Relay Recognition of Fluoride and Cu (II) ions with

Electronic Supplementary Information (ESI) for

Supporting Information. Identification of Absolute Helical Structures of Aromatic Multi-layered Oligo(m-phenylurea)s in Solution.

Supporting Information

Supporting Information. Fluorinated Thiophene-Based Synthons: Polymerization of 1,4-Dialkoxybenzene

Diels-Alder reaction of acenes with singlet and triplet oxygen - theoretical study of two-state reactivity

Supporting Information for

Syntheses and Characterizations of Molecular Hexagons and Rhomboids and Subsequent Encapsulation of Keggin-Type Polyoxometalates by Molecular Hexagons

Intermolecular Aminocarbonylation of Alkenes using Cycloadditions of Imino-Isocyanates. Supporting Information

Electronic Supplementary Information

Rhodium-Catalyzed Direct Bis-cyanation of. Arylimidazo[1,2-α]pyridine via Double C-H Activation

Nesting Complexation of C 60 with Large, Rigid D 2 Symmetrical Macrocycles

Supporting Information

Asymmetric H/D exchange reaction of fluorinated aromatic ketones

Reaction of Lithium Diethylamide with an Alkyl Bromide and Alkyl Benzenesulfonate: Origins of Alkylation, Elimination, and Sulfonation.

SUPPORTING INFORMATION. Visible Light Excitation of a Molecular Motor with an Extended Aromatic Core

Supporting Information for:

Supporting Information

Figure S12. Kinetic plots for the C(2)-H/D exchange reaction of 2 CB[7] as a function

Supporting Information

Synthesis and spectroscopic properties of chial binaphtyl-linked subphthalocyanines

Accessory Publication

Supporting Information

Bis(perylene diimide) with DACH bridge as nonfullerene. electron acceptor for organic solar cells

Naphthotetrathiophene Based Helicene-like Molecules: Synthesis and Photophysical Properties

Push-Pull Type Porphyrin Based Sensitizers: The Effect of Donor Structure on the Light- Harvesting Ability and Photovoltaic Performance

Supporting Information

Electronic Supplementary Information for

Supporting Information File for. Design of van der Waals Two-Dimensional Heterostructures from

SUPPORTING INFORMATION

Supporting Information. Lithium Cadmate-Mediated Deprotonative Metalation of Anisole: Experimental and Computational Study

Supporting Information

Capture of Benzotriazole-Based Mannich Electrophiles by CH-Acidic Compounds

Disulfide-based metal free sulfanylation of ketones

Electronic Supplementary Information (ESI)

Title N-H versus C-H Activation of a Pyrrole Imine at {Cp*Ir}: A Computational and Experimental Study

Supporting Information

Synthesis, characterization and luminescence studies of

Chemical Communications. Electronic Supporting Information

Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2008

Pt-Ag Clusters and their Neutral Mononuclear Pt(II) Starting Complexes: Structural and Luminescence Studies.

Supplementary Figures

Differentiation of Diastereoisomers of Protected 1,2-Diaminoalkylphosphonic Acids by EI Mass Spectrometry and Density Functional Theory

Electronic Supporting Information. Thermal conversion of a pyridine-bridged bisdithiazolyl radical to a zwitterionic bisdithiazolopyridone

Supporting Information

Amplification of a metallacyclic receptor out of a dynamic combinatorial library. - Supporting Information -

Sculpting the β-peptide foldamer H12 helix via a designed side chain shape

Regioselective and Stereospecific Cu-Catalyzed Deoxygenation of Epoxides to Alkenes

Commiphoratones A and B, Two Sesquiterpene Dimers from Resina Commiphora

Experimental and Theoretical Evidence of the Au(I) Bi(III) Closed-Shell Interaction

Supporting Material. Hydrogen Oxidation and Production Using Nickel-Based Molecular Catalysts with Positioned Proton Relays

Supporting Information. Halogen Photoelimination from Monomeric Ni(III) Complexes Enabled by the Secondary Coordination Sphere

chain transfer polymerization (DET-

A turn-off emission based chemosensor for HSO formation of a hydrogen-bonded complex

DFT Kinetic Study of the Pyrolysis Mechanism of Toluene Used for Carbon Matrix

Zn 2 +, Studies on the Structures and Antihyperglycemic Effects of Zn 2 +, Cu 2 +, Ni 2 + 2Metformin Complexes. ZHU, Miao2Li LU, Li2Ping YANG, Pin Ξ

Supporting Information

Supporting Information. Generation of Pyridyl Coordinated Organosilicon Cation Pool by Oxidative Si-Si Bond Dissociation

SUPPPORTING INFORMATION

Supporting Information

Electronic Supplementary Information (ESI)

Supporting Information for. Department of Chemistry, Vanderbilt University, Nashville, TN 37235

Supplementary Information

Computational Evaluation of Sulfonyl Radical as a Universal Leaving Group for SUPPORTING INFORMATION

Electronic Supplementary Information (ESI)

Sequential Addition of Phosphine to Alkynes for the Selective. Synthesis of 1,2-Diphosphinoethanes under Catalysis. Well-Defined

Gelsekoumidines A and B: Two Pairs of Atropisomeric Bisindole Alkaloids from the Roots of Gelsemium elegans

Supporting Information

Supporting Information

The role of exchange in systematic DFT errors for some organic reactions: Electronic supplementary information

Composed of Thiophene, Pyrrole and Methylthio

The generation and reactivity of aza-oxyallyl cationic intermediates: aza- [4+3] cycloaddition reactions for heterocycle synthesis

Deprotonative Cadmation of Functionalized Aromatics

Supplementary Material (ESI) for Chemical Communications This journal is (c) The Royal Society of Chemistry Supporting Information

Enhancing the Photochemical Stability of N,C-Chelate Polyboryl Compounds: C- C Bond Formation versus C=C Bond cis, trans-isomerization

Diels Alder Exo-Selectivity in Terminal-Substituted Dienes and Dienophiles: Experimental Discoveries and Computational Explanations

Supporting Information

Laccase-catalyzed synthesis of catechol thioethers by reaction of catechols with thiols using air as an oxidant. Electronic Supplementary Information

Chiral α-aminoxy Acid / Achiral Cyclopropane α-aminoxy Acid Unit as a Building Block for Constructing α N O Helix

Electronic Supplementary Information. Catalytic hydroboration of aldehydes, ketones, alkynes and. alkenes initiated by NaOH

Electronic Supplementary Information

Supporting Information

Supporting Information

Supporting Information. Synthesis and Properties of [9]Cyclo-1,4-naphthylene: A π-extended Carbon Nanoring

Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes

SUPPORTING INFORMATION

Supporting Information One-Pot Approach to Chiral Chromenes via Enantioselective Organocatalytic Domino Oxa-Michael-Aldol Reaction

Supporting Information

Transcript:

Photostimulated Reduction of Nitriles by SmI 2 Chintada Nageswara Rao and Shmaryahu Hoz * Department of Chemistry, Bar-Ilan University, Ramat-Gan 52900, Israel E-mail: shoz@mail.biu.ac.il Supporting information Table of contents (1) Complete reference 14 S2 (2) NBO charges S3 (3) Experimental setup for irradiation S4 (4) Spectral data: 1 H, 13 C NMR and HRMS (CI/EI) S5-S14 (5) Archive files S15-S42 S1

(1) Complete reference 14 Gaussian 09, Revision A.02, M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, G. Scalmani, V. Barone, B. Mennucci, G. A. Petersson, H. Nakatsuji, M. Caricato, X. Li, H. P. Hratchian, A. F. Izmaylov, J. Bloino, G. Zheng, J. L. Sonnenberg, M. Hada, M. Ehara, K. Toyota, R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajima, Y. Honda, O. Kitao, H. Nakai, T. Vreven, J. A. Montgomery, Jr., J. E. Peralta, F. Ogliaro, M. Bearpark, J. J. Heyd, E. Brothers, K. N. Kudin, V. N. Staroverov, R. Kobayashi, J. Normand, K. Raghavachari, A. Rendell, J. C. Burant, S. S. Iyengar, J. Tomasi, M. Cossi, N. Rega, J. M. Millam, M. Klene, J. E. Knox, J. B. Cross, V. Bakken, C. Adamo, J. Jaramillo, R. Gomperts, R. E. Stratmann, O. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. Ochterski, R. L. Martin, K. Morokuma, V. G. Zakrzewski, G. A. Voth, P. Salvador, J. J. Dannenberg, S. Dapprich, A. D. Daniels, O. Farkas, J. B. Foresman, J. V. Ortiz, J. Cioslowski, and D. J. Fox, Gaussian, Inc., Wallingford CT, 2009. S2

(2) Table S1: NBO charges for SN; syn, clinal and anti conformations. syn C H H C H H C C N N Gas P. -0.80 0.25 0.21-0.80 0.25 0.21 0.26 0.26-0.42-0.42 THF -0.67 0.23 0.20-0.63 0.26 0.25 0.00 0.31-0.55-0.42 anti C H H C H H C C N N Gas P. -0.69 0.24 0.24-0.69 0.24 0.24 0.17 0.17-0.46-0.46 THF -0.67 0.24 0.24-0.67 0.24 0.24 0.16 0.16-0.47-0.47 S3

(3) Experimental setup for irradiation Figure S1 S4

(4) Spectral data: 1 H, 13 C NMR and HRMS (CI/EI) Crude reaction mixture, 1 H& 13 C (300&75 MHz, CDCl 3 ) NMR and HRMS (CI) of benylamine NH 2 S5

NH 2 calc.mass[m] + =107.0735 obs.mass[m] + =107.0839 S6

Crude reaction mixture, 1 H& 13 C (300&75 MHz, CDCl 3 ) NMR of 2- phenylethylamine NH 2 S7

Crude reaction mixture, 1 H& 13 C (300&75 MHz, CDCl 3 ) NMR and HRMS (CI) of octylamine NH 2 S8

NH 2 calc.mass[m+h] + =130.1596 obs.mass[m+h] + =130.1569 S9

Crude reaction mixture, 1 H& 13 C (300&75 MHz, CDCl 3 ) NMR and HRMS (CI) of isoindolone NH O S10

O NH calc.mass[m] + =133.0528 obs.mass[m] + =133.0745 S11

Crude reaction mixture, 1 H (300 MHz, CDCl 3 ) NMR and MS (EI) of α-amino-mtolunitrile NH 2 CN NH 2 CN calc.mass[m] + =132.0687 obs.mass[m] + =132.0757 S12

Crude reaction mixture, 1 H& 13 C (300&75 MHz, CDCl 3 ) NMR and HRMS (CI) of α-amino-p-tolunitrile NH 2 CN S13

NH 2 CN calc.mass[m] + =132.0687 obs.mass[m] + =132.0651 S14

(5) Archive files Gaussian Archives p-dcn In the gas phase p-dcn-b3lyp 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\22-Dec- 2011\0\\#B3LYP/6-31+G*OPTnosymm\\1,4-Ph-dCN\\0,1\C,0.1919752445,- 0.221071081,0.4026382663\C,1.507441111,- 0.4222131188,0.8575261745\C,2.2867542433,0.6668547379,1.2316744111\C,1.758 1501439,1.9677939364,1.1546948235\C,0.4427111734,2.1689353717,0.6997825992 \C,-0.3366123001,1.0798537319,0.3256338141\H,1.9101456357,- 1.4282321217,0.9150646639\H,0.0399958863,3.1749476331,0.6422014491\H,- 1.3521936769,1.2293496271,- 0.0262042472\C,2.5622413245,3.0918113936,1.5411023862\N,3.213907754,4.0033 506115,1.8544065687\H,3.3023460026,0.5173880145,1.5834947434\C,- 0.6120644868,-1.345116984,0.0162048162\N,-1.2637287455,-2.2565890723,- 0.297299119\\Version=EM64L-G09RevA.02\HF=-416.7472804\RMSD=9.852e- 09\RMSF=1.111e-04\Dipole=-0.0000241,- 0.0000164,0.0000986\Quadrupole=2.4819288,-7.0932894,4.611 3607,-15.5311701,-2.6676573,-6.7298402\PG=C01 [X(C8H4N2)]\\@ In THF p-dcn-b3lyp-thf 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\22-Dec- 2011\0\\#B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph-dcn in THF\\0,1\C,0.1947017728,-0.2171451942,0.4039985285\C,1.5096145564,- 0.4240232196,0.8580828665\C,2.2890422201,0.6649912108,1.2321587647\C,1.755 4469814,1.9638664859,1.1532899691\C,0.4405384663,2.1707439297,0.6992050478 \C,-0.3388912452,1.081726673,0.3251282815\H,1.9130416904,-1.4292199366,0.916377532\H,0.0371071331,3.1759388299,0.6409075067\H,-1.3539475503,1. 2324653108,-0.0263386544\C,2.5594235948,3.0881395033,1.5398397024\N,3. 2112037709,3.9999172151,1.8533578239\H,3.3040993754,0.514257891,1.5836 254198\C,-0.6092575672,-1.3414257414,0.0174347778\N,-1.2610538889,-2.2 53170278,-0.2961462162\\Version=EM64L-G09RevA.02\HF=-16.7579684\RMSD= 3.611e-09\RMSF=6.238e-05\Dipole=0.0000006,-0.0000173,0.0000489\Quadrup ole=2.817342,-8.6225402,5.8051982,-18.4294448,-3.3573346,-8.0422249\pg =C01 [X(C8H4N2)]\\@ Radical anion p-dcn-radical anion-b3lyp 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\22-Dec- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\1,4-ph-dcn radicalanion\\-1,2\c,0.1695 S15

31517,-0.2524584551,0.391955566\C,1.5199353649,-0.4221511424,0.8620726 841\C,2.2900247993,0.6540294458,1.2316007681\C,1.7806118792,1.99919003 97,1.1653141099\C,0.4302091475,2.1688819046,0.6951981983\C,-0.33988070 56,1.0927008011,0.3256701762\H,1.9311977337,-1.4273227326,0.9228946056 \H,0.0189454932,3.1740528203,0.6343745172\H,-1.3569747036,1.2512279947,-0.0258681811\C,2.5678535689,3.0998737745,1.5438414052\N,3.2286510616,4.0237115536,1.8617260571\H,3.3071194915,0.4955042944,1.5831381877\C, -0.6177134552,-1.353142969,0.013437398\N,-1.2784418825,-2.2770346498,- 0.3044341422\\Version=EM64L-G09RevA.02\HF=-416.7930682\S2=0.758675\S2-1=0.\S2A=0.750051\RMSD=9.329e-09\RMSF=6.150e-05\Dipole=-0.0000383,0.00 00309,-0.0000099\Quadrupole=1.5082925,-14.3742486,12.8659561,-28.15880 26,-9.810366,-14.0785204\PG=C01 [X(C8H4N2)]\\@ Radical anion in THF p-dcn-radical anion-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\22-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph-dcn radical anion in THF\\-1,2\C,0.1723802564,-0.2484527138,0.3933394068\C,1.52 25325481,-0.423944315,0.8630076666\C,2.2922099313,0.6517713487,1.23221 95937\C,1.7777627574,1.9951833585,1.1639338006\C,0.4276109024,2.170674 6766,0.6942656627\C,-0.3420665517,1.0949589348,0.3250537302\H,1.934690 8921,-1.4280944878,0.9241768326\H,0.0154526508,3.1748247423,0.63309472 32\H,-1.3585595026,1.2545054918,-0.0259540371\C,2.5632794908,3.0934354 215,1.5416693592\N,3.2244592921,4.017823443,1.859797951\H,3.3087035343,0.4922254859,1.5832258955\C,-0.6131387842,-1.3467025221,0.0156020709\ N,-1.2742481073,-2.2711461846,-0.302511306\\Version=EM64L-G09RevA.02\H F=-416.8568581\S2=0.757997\S2-1=0.\S2A=0.750043\RMSD=3.094e-09\RMSF=3. 189e-05\Dipole=-0.0000502,0.0000399,-0.0000116\Quadrupole=1.9472119,-1 5.3646468,13.4174349,-30.5298141,-10.1345136,-15.0823703\PG=C01 [X(C8H 4N2)]\\@ o-dcn In the gas phase o-dcn-b3lyp 1\1\GINC-ELA\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\30-Nov-2011\0\\# B3LYP/6-31+G* OPT nosymm\\1,2-ph-dcn-am1\\0,1\c,0.3482274133,- 0.1696465006,0.0933377072\C,1.7117458597,- 0.3932354337,0.2810521214\C,2.6277644043,0.6598181675,0.1368651225\C,2.157 9648472,1.9528636525,-0.2007635579\C,0.7830677847,2.1626230336,- 0.3865839845\C,-0.1153805216,1.1063462536,-0.2400519358\H,-0.3511998147,- 0.9925680143,0.2077033657\H,2.079949809,- 1.3807737903,0.5399335236\H,0.4313513054,3.1562572726,-0.6450859878 \H,-1.177265048,1.2809916722,-0.3862962831\C,3.0641846443,3.0533036126,-0.3561884358\C,4.0254941877,0.4072902714,0.3342317708\N,3.7717843763 S16

,3.9668195267,-0.489620546\N,5.1516152623,0.1684403462,0.5010213198\\V ersion=ibm64-g09reva.02\hf=-416.7437658\rmsd=4.554e-09\rmsf=4.798e- 05\ Dipole=-2.7274884,-1.0037061,-0.0495866\Quadrupole=-16.142517,4.932931 1,11.2095859,-11.8581992,-0.204229,0.1868877\PG=C01 [X(C8H4N2)]\\@ In THF o-dcn-b3lyp-scrf-thf 1\1\GINC-NANO02\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\01-Dec- 2011\0\\#B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,2-ph-dcn in THF\\0,1\C,0.3471984368,-0.1700225785,0.093272506\C,1.7110205976,- 0.3965723044,0.2816949441\C,2.6238220728,0.6581264899,0.137023992\C,2.1538 180995,1.9517303289,-0.2008570175\C,0.7802960549,2.1647909409,- 0.3872595344\C,-0.1164239671,1.1059969198,-0.2400667784\H,-0.3521900851,- 0.992177241,0.2073829045\H,2.0763826465,- 1.384705324,0.5401231144\H,0.4255796282,3.1568558386,-0.6456688261\H,- 1.1778026116,1.2800039824,-0.3859844616\C,3.0660957994,3.0464595111,- 0.3546272184\C,4.0225154202,0.4136387981,0.332712134\N,3.7942188145,3.9451 098624,0.4828199835\N,5.1547736035,0.1992948457,0.494628425\\Version=EM64 L-G09RevA.02\HF=-16.7551319\RMSD=4.391e-09\RMSF=1.388e-04\Dipole=- 3.4836943,-1.2818361,-0.0632532\Quadrupole=-0.6177771,6.2682812,14.3494959,- 15.1322161,-0.2668099,0.25843 87\PG=C01 [X(C8H4N2)]\\@ Radical anion o-dcn-radical anion-b3lyp 1\1\GINC-ARMON\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\30-Nov- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\1,2-ph-dcn radicalanion\\-1,2\c,0.35845 35144,-0.1862440854,0.0980571825\C,1.7111153236,-0.3942485952,0.281131 096\C,2.6707797398,0.6471389112,0.1439046074\C,2.1827562796,1.99043225 59,-0.2067734297\C,0.7819589675,2.1629717773,-0.3868034394\C,-0.118175 4394,1.1256526361,-0.2447565392\H,-0.3402288805,-1.0120966975,0.213280 1546\H,2.0759187148,-1.38648373,0.5408478036\H,0.424571337,3.158019096 1,-0.6461003221\H,-1.1814008029,1.3030819965,-0.3915590514\C,3.0352000 984,3.0978054729,-0.369066033\C,4.0318504383,0.3544194457,0.3466942232 \N,3.7155449794,4.0484831642,-0.5135765881\N,5.1609602399,0.0695984223,0.5242745357\\Version=IBM64-G09RevA.02\HF=-416.7827521\S2=0.760808\S2-1=0.\S2A=0.750097\RMSD=9.733e-09\RMSF=2.244e-05\Dipole=-2.5932224,-0. 9544207,-0.0470127\Quadrupole=-31.5131155,4.9856437,26.5274717,-23.181 2342,-0.9763801,2.5156462\PG=C01 [X(C8H4N2)]\\@ Radical anion in THF o-dcn-radical anion-b3lyp-thf 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\01-Dec- 2011 \0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,2-phdcn radical anion in THF\\-1,2\C,0.3560484201,- 0.1867601075,0.0980315968\C,1.7053808193,- 0.4017351322,0.2827999889\C,2.6631403581,0.64552674,0.1438175686\C,2.17544 04982,1.987218322,-0.2063551052\C,0.7723819147,2.1651209401,- 0.3884310394\C,-0.1203531251,1.1241997176,-0.2454440176\H,-0.3454 186552,-1.0089259504,0.212833098\H,2.0666159341,-1.3942770463,0.543189 1615\H,0.4119820508,3.1581283604,-0.6481259133\H,-1.1833752288,1.29694 74342,-0.3916156013\C,3.0435160819,3.0770254506,-0.3627446755\C,4.0251 022026,0.3763962686,0.3402899265\N,3.7694073904,3.9977102307,-0.495435 5843\N,5.1694358489,0.1419548422,0.5067447965\\Version=EM64L-G09RevA.0 S17

2\HF=-416.8502763\S2=0.759226\S2-1=0.\S2A=0.75007\RMSD=3.221e- 09\RMSF=1.920e-05\Dipole=-3.5421116,-1.3029449,-0.0632883\Quadrupole=- 36.7118766,7.1242213,29.5876554,-27.3002126,-0.9004975,2.266414\PG=C01 [X(C8H4N2)]\\@ m-dcn In the gas phase m-dcn-b3lyp 1\1\GINC-ESHEL\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\30-Nov-2011\0\\# B3LYP/6-31+G* OPT nosymm\\1,3-ph-dcn\\0,1\c,0.3342585325,-0.3766611647, 0.0053631898\C,1.7236217855,-0.4648938626,0.0863644278\C,2.504210356,0.702660004,0.0121416504\C,1.8912218505,1.9540513726,-0.1428234855\C,0. 4935429479,2.0308222881,-0.2231401429\C,-0.2861392584,0.8626935602,-0. 1487731452\H,-0.2680438787,-1.2782789316,0.0628894366\H,2.2104899806,- 1.4274973805,0.2065732121\H,-1.3672303198,0.9357853824,-0.2119130491\C,3.9352260799,0.6151575543,0.0953241206\N,5.0938705788,0.5374952457,0. 163377247\H,2.4928838596,2.8547727108,-0.2001321822\C,-0.1423923218,3. 3086305384,-0.3818000629\N,-0.6635149927,4.3406466029,-0.5102309765\\V ersion=ibm64-g09reva.02\hf=-416.7467144\rmsd=5.535e-09\rmsf=1.971e- 05\Dipole=-0.9767833,-1.4622644,0.0929041\Quadrupole=-7.7416332,-1.091615 6,8.8332488,3.5519133,-1.1327748,1.3138638\PG=C01 [X(C8H4N2)]\\@ In THF m-dcn-b3lyp-scrf-thf 1\1\GINC-NANO02\FOpt\RB3LYP\6-31+G(d)\C8H4N2\ROZENTE\01-Dec- 2011\0\\#B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,3-ph- dcn\\0,1\c,0.3335021615,-0.3776657138,0.0053564988\c,1.722645396,-.4656395308,0.0861795329\c,2.5021716815,0.7037162907,0.0119337558\c,1.8932 427002,1.9566591472,-0.1429581699\C,0.495648644,2.0294430455,- 0.2227994147\C,-0.2861606775,0.8617986165,-0.1485757163\H,-0.2686373511,- 1.2785731051,0.0628773923\H,2.2068127957,-1.4293029059,0.2061809908\H,- 1.3670631881,0.9327244637,0.2110885889\C,3.9324638464,0.6169950979,0.09510 50642\N,5.0916860966,0.5421081953,0.1629978448\H,2.4952208774,2.8568886245,-0.2001239914\C,-0.1400182938,3.3064972042,-0.3815675178\N,- 0.6595094889,4.33973449,-0.5102974404\\Version=EM64L-G09RevA.02\HF=- 416.7577091\RMSD=2.785e-09\RMSF=1.603e-04\Dipole=-1.2202419,- 1.828366,0.116644\Quadrupole=-9.5075409,-1.616131,11.1236719,3.931129,- 1.3628875,1.6520755\PG=C01[X(C8H4N2)]\\@ Radical anion m-dcn-radical anion-b3lyp S18

1\1\GINC-ESHEL\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\30-Nov- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\1,3-ph-dcn radical anion\\-1,2\c,0.32997 03081,-0.3830852767,0.0057121278\C,1.7176784152,-0.500269946,0.0891876 076\C,2.5276966392,0.7096652857,0.0124517673\C,1.8877959594,1.94887810 66,-0.1426871945\C,0.4909932756,2.0550882076,-0.2258333216\C,-0.316555 0582,0.8435434202,-0.1485022504\H,-0.2749828582,-1.2886041441,0.063673 0976\H,2.1996317994,-1.4652249721,0.2094508131\H,-1.3979641658,0.91126 32064,-0.2104787065\C,3.9384265863,0.6489313234,0.0923484326\N,5.10986 593,0.5704936256,0.1614945164\H,2.4910386704,2.8519271085,-0.200066870 9\C,-0.1123086148,3.324690802,-0.3818874025\N,-0.6392816866,4.36808717 28,-0.5116423759\\Version=IBM64-G09RevA.02\HF=-416.7818125\S2=0.762386 \S2-1=0.\S2A=0.750099\RMSD=3.242e-09\RMSF=4.506e-05\Dipole=-0.7802423, -1.1683066,0.074297\Quadrupole=-16.9229216,-4.1969449,21.1198665,2.767 6481,-1.9502136,3.0125936\PG=C01 [X(C8H4N2)]\\@ Radical anion in THF m-dcn-radical anion-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H4N2(1-,2)\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,3-ph-dcn radical anion in THF\\-1,2\C,0.3286758493,-0.3851134983,0.0061564586\C,1.71 69317935,-0.5006784716,0.0895742753\C,2.525153519,0.7110930779,0.01186 3581\C,1.8902115576,1.9527579839,-0.1434996732\C,0.4929273585,2.053123 4938,-0.2258086013\C,-0.3169075627,0.8423615339,-0.1487123793\H,-0.275 4831418,-1.2896457925,0.063943626\H,2.1985992581,-1.465419745,0.209982 261\H,-1.3980205261,0.9095470898,-0.2113047477\C,3.9331933548,0.651591 1,0.0916084099\N,5.1051544911,0.5736337829,0.1611499521\H,2.4931785456,2.8555635726,-0.2007444939\C,-0.1080866704,3.32087716,-0.3808118805\N,-0.6335226264,4.3656926326,-0.5101765479\\Version=EM64L-G09RevA.02\HF =-416.8448382\S2=0.762687\S2-1=0.\S2A=0.750097\RMSD=7.054e-09\RMSF=2.0 55e-05\Dipole=-0.9805937,-1.4689834,0.092398\Quadrupole=-17.9201876,-4.3787507,22.2989383,2.8881489,-2.0578523,3.1751979\PG=C01 [X(C8H4N2)]\ \@ In the gas phase BN-B3LYP 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C7H5N1\ROZENTE\30-Nov- 2011\0\\#B3LYP/6-31+G*OPTnosymm\\Ph-CN\\0,1\C,0.261098662,- 0.0670341127,0.3237489129\C,1.6319631862,- 0.3113898307,0.3924540793\C,2.539535897,0.7106776581,0.0617199286\C,2.0645 893551,1.9731203637,-0.3363323289\C,0.6914873425,2.2056871011,- 0.4012682051\C,-0.210611218,1.1887586435,-0.0721944853\H,-0.4389471772,- 0.8573665921,0.579554094\H,2.0063655998,-1.2833 201597,0.6988658585\H,0.3258828898,3.1813128168,-0.7088879391\H,-1.279 9910503,1.3747635127,-0.1239871203\C,3.9521120097,0.4649764531,0.13025 S19

80805\N,5.0975578765,0.265662214,0.1857369884\H,2.7715114567,2.7570544 724,-0.5901326436\\Version=EM64L-G09RevA.02\HF=-24.5051873\RMSD=9.254 e-09\rmsf=9.744e-05\dipole=-1.8468311,0.3212896,-0.0895733\quadrupole= -15.1672716,10.8555449,4.3117267,0.5001477,-1.0936827,-2.0954099\PG=C0 1 [X(C7H5N1)]\\@ In THF BN-B3LYP-SCRF-THF 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C7H5N1\ROZENTE\01-Dec- 2011\0\\#B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\ph-cn in THF\\0,1\C,0.2617058527,-0.0687431402,0.3242338412\C,1.6322074533,- 0.3142162013,0.3932976308\C,2.5374254335,0.7110295146,0.061599046\C,2.0658 665388,1.9756154304,-0.3371562537\C,0.6927050755,2.2070277109,- 0.4017621994\C,-0.2086188714,1.1884023335,-0.0721285841\H,-0.438472549,- 0.8585861092,0.579946743\H,2.0049127879,- 1.2866591842,0.7000109928\H,0.3268297696,3.1823120952,-0.7092219404\H,- 1.2777265374,1.3743855372,- 0.1237868146\C,3.9490777888,0.465625602,0.1300711426\N,5.0951936361,0.2661 198156,0.1856080347\H,2.7714484514,2.7605891358,- 0.591176419\\Version=EM64L-G09RevA.02\HF=-324.5120681\RMSD=7.442e- 09\RMSF=1.270e-04\Dipole=-2.2906742,0.3985049,-0.1109005\Quadrupole=- 18.5379608,12.9227517,5.6152091,0.4601542,-1.3045974,-2.3112775\PG=C01 [X(C7H5N1)]\\@ Radical anion BN-radical anion-b3lyp 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C7H5N1(1-,2)\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\ph-cn radical anion\\-1,2\c,0.264747692,-0.0739475682,0.3258931717\c,1.6206274076,-0.3248656639,0.3968022542\ C,2.5895011418,0.7019470123,0.0640860893\C,2.0589453778,1.9895340851,- 0.3414898118\C,0.6974614937,2.210900804,-0.4029626972\C,-0.2442693107, 1.1945727088,-0.0739714545\H,-0.4320418645,-0.8729098404,0.5844377193\ H,1.9808196057,-1.3043784768,0.7058836809\H,0.3380936236,3.1935230117, -0.7128644624\H,-1.3142846267,1.3807456967,-0.1255778948\C,3.965033295 5,0.4627412693,0.1308199968\N,5.1325537204,0.2596258593,0.1873875356\H,2.7553672737,2.7854136424,-0.5989089073\\Version=EM64L-G09RevA.02\HF= -324.5086506\S2=0.760391\S2-1=0.\S2A=0.750075\RMSD=4.830e-09\RMSF=6.90 6e-05\Dipole=-1.8249684,0.3176022,-0.0882365\Quadrupole=-32.1332164,16.476284,15.6569325,-3.0999899,-1.8588904,-1.0204514\PG=C01 [X(C7H5N1)] \\@ Radical anion in THF BN-radical anion-b3lyp-thf 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C7H5N1(1-,2)\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\ph-cn radical anion in THF\\-1,2\C,0.2651761504,- 0.0744081643,0.3263942293\C,1.621324477,- 0.3278487214,0.3970578393\C,2.5889614644,0.7022859214,0.0629929142 \C,2.060322001,1.9925169617,-0.3434025101\C,0.6975960904,2.2113812198, -0.4031402735\C,-0.2396796177,1.1941146128,-0.0724775406\H,-0.43190627 S20

31,-0.8716622533,0.5840345435\H,1.9797952934,-1.3077978909,0.705473345 4\H,0.3367551002,3.192256048,-0.7123741035\H,-1.308961122,1.379910085, -0.1244866435\C,3.958903105,0.4643735883,0.1308297857\N,5.1294814489,0.2583758455,0.1900300605\H,2.7547867121,2.7894052876,-0.6013964269\\Ve rsion=em64l-g09reva.02\hf=-324.5782705\s2=0.761681\s2-1=0.\s2a=0.75009 7\RMSD=4.245e-09\RMSF=4.448e-05\Dipole=-2.540684,0.4436137,-0.1260197\ Quadrupole=-36.63883,19.4738908,17.1649392,-3.3680825,-2.1664817,-1.45 7315\PG=C01 [X(C7H5N1)]\\@ In the gas phase SN-B3LYP 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C4H4N2\ROZENTE\25-Dec- 2011\0\\#B3LYP/6-31+G*OPT\\CN-CH2-CH2-CN\\0,1\C,- 3.5030305484,0.2429624716,-0.1876658944\H,-3.1552657414,-0.7560743643,- 0.4729029275\H,-3.0369495533,0.4891618576,0.7734666115\C,- 3.0487404797,1.2879390721,-1.2383370172\H,-3.4472268185,2.2766529167,- 0.9852980943\H,-1.955252298,1.3591480917,-1.2094537202\C,- 4.9569416922,0.2071199275,-0.0000783387\C,-3.4532219201,0.9455551963,- 2.6056333915\N,-6.1064964854,0.1933925574,0.1599822563\N,- 3.7585898832,0.6631747432,-3.6892826639\\Version=EM64L-G09RevA.0 2\State=1-A\HF=-264.3114353\RMSD=2.952e-09\RMSF=1.243e-05\Dipole=1.877 8678,0.3821884,1.1920732\Quadrupole=-0.3820974,4.8843212,-4.5022238,-0.497684,4.2945447,-0.0628931\PG=C01 [X(C4H4N2)]\\@ In THF SN-B3LYP-THF 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C4H4N2\ROZENTE\25-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\cn-ch2- CH2-CN in THF\\0,1\C,-3.4984987228,0.251557827,-0.1780058019\H,- 3.1348866557,-0.7492703269,-0.4327912172\H,- 3.056447359,0.5250586467,0.7858609502\C,-3.0360019352,1.2830678265,- 1.2369631288\H,-3.4019005376,2.283656126,-0.9842420725\H,- 1.9416742214,1.321842871,-1.2256364207\C,-4.9550475552,0.196 820658,-0.0199812677\C,-3.4725985047,0.9520135244,-2.5967634455\N,-6.1 087397045,0.1591897044,0.1068375579\N,-3.8159202241,0.6850956128,-3.67 35183335\\Version=EM64L-G09RevA.02\HF=-264.3252367\RMSD=5.537e- 09\RMSF=2.356e-05\Dipole=2.3606644,0.481087,1.4983298\Quadrupole=- 22.6907801,20.6441155,2.0466647,-1.6729514,-12.1480593,0.6880513\PG=C01 [X(C4H4N2)]\\@ Radical anion SN-radical anion-b3lyp 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C4H4N2(1-,2)\ROZENTE\25-Dec- 2011\0\\#B3LYP/6-31+G* OPT\\CN-CH2-CH2-CN radical anion\\-1,2\c,- 3.5488091083,0.2678209621,-0.1933047518\H,-3.1906520378,-0.7457238717,- S21

0.4246309778\H,-3.0789812398,0.5754932324,0.7674123365\C,- 3.0643005838,1.2505969144,-1.2716362085\H,-3.4154909659,2.2655596301,- 1.0358875223\H,-1.9524125496,1.2648400957,-1.2282783425\C,- 5.0070184522,0.2229204706,-0.0151235874\C,-3.4812555603,0.9138584737,- 2.6401736952\N,-6.0954202271,0.0703455909,0.3893729911\N,- 3.5873746954,0.8233209716,-3.8029534221\\Version=EM64L- G09RevA.02\State=2-A\HF=-264.3022037\S2=0.750516\S2-1=0.\S 2A=0.75\RMSD=5.352e-09\RMSF=2.234e-05\Dipole=-0.1017824,-0.0207151,-0. 0646116\Quadrupole=-2.9391929,9.6071776,-6.6679847,-2.5083576,3.274725 5,0.4317364\PG=C01 [X(C4H4N2)]\\@ Radical anion in THF SN-radical anion-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C4H4N2(1-,2)\ROZENTE\25-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\cn-ch2- CH2-CNradical anion in THF\\-1,2\C,-3.609783852,0.2671389551,- 0.2486656838\H,-3.265245429,-0.7441078334,-0.5044727944\H,- 3.1951159808,0.5182455083,0.7443955992\C,-3.0367382004,1.2744341083,- 1.2656241063\H,-3.4157757654,2.2800904253,-1.0447470814\H,- 1.9422526932,1.309862019,-1.1876070507\C,-5.1452924983,0.2638802094,- 0.2106370979\C,-3.3688335803,0.963797752 6,-2.6612308379\N,-5.9060459371,0.0298321956,0.7163954304\N,-3.5366314 838,0.7458591295,-3.7930095572\\Version=EM64L-G09RevA.02\HF=-264.37285 58\S2=0.753324\S2-1=0.\S2A=0.750006\RMSD=4.955e-09\RMSF=1.653e-04\Dipo le=3.4537705,1.0795433,-0.6623598\quadrupole=-73.2991734,49.4228844,23.8762889,2.0072603,-8.6776364,2.646802\pg=c01 [X(C4H4N2)]\\@ In the gas phase trans-sn-b3lyp 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C4H4N2\ROZENTE\25-Dec- 2011\0\\#B3LYP/6-31+G*OPT\\trans-CN-CH2-CH2-CN\\0,1\C,- 3.4027363999,0.0679542875,-0.5252437027\H,-3.2312220371,-0.8917860151,- 1.0249649813\H,-2.8493233828,0.0440130766,0.4199552699\C,- 2.8916590745,1.2312004866,-1.4136943253\H,-3.4450890772,1.255160811,- 2.3588827225\H,-3.0631499166,2.1909377472,-0.9139588061\C,- 4.8329734566,0.2071429222,-0.2373700471\C,-1.4614289742,1.091994671,- 1.7015943581\N,-5.9662171815,0.3325434345,-0.0190649554\N,- 0.3281913596,0.9665805785,-1.9199234513\\Version=EM64L-G09 RevA.02\State=1-A\HF=-264.3132942\RMSD=6.290e-09\RMSF=1.020e-04\Dipole =0.0000075,0.0000179,0.0000293\Quadrupole=-13.1416884,7.6427901,5.4988 983,-1.2232636,6.144648,-0.0228756\PG=C01 [X(C4H4N2)]\\@ In THF S22

trans-sn-b3lyp-thf 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C4H4N2\ROZENTE\26-Dec- 2011\0\\#B3LYP/6-31+G*OPT SCRF=(PCM, Solvent=THF) nosymm\\trans-cn- CH2-CH2-CN in THF\\0,1\C,-3.4025977894,0.0674903982,-0.5249774276\H,- 3.2400412846,-0.8939017407,-1.0234220735\H,- 2.8574189057,0.0437693276,0.4243870354\C,-2.89180055,1.2316574703,- 1.4139715825\H,-3.4369781653,1.2553779188,-2.3633367684\H,- 3.054358663,2.1930495464,-0.9155272957\C,-4.832158109,0.2075837451,-0.238034124\C,-1.462239772,1.0915652701,-1.7009132319\N,-5.9656039637,0.3260417199,-0.014857933\N,-0.3287936572,0.9731083443, -1.9240886787\\Version=EM64L-G09RevA.02\HF=-264.3256591\RMSD=8.497e- 09\RMSF=9.916e-05\Dipole=-0.0000007,-0.0000015,-0.0000016\Quadrupole=-15.5145039,9.0370213,6.4774826,-1.5246544,7.3098885,-0.0053602\PG=C01 [X (C4H4N2)]\\@ Radical anion trans-sn-radical anion-b3lyp 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C4H4N2(1-,2)\ROZENTE\26-Dec- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\trans-cn-ch2-ch2-cn radical anion\\- 1,2 \C,-3.4814094451,0.1141581194,-0.5343835191\H,-3.3583011861,-0.8757145 403,-1.0064045731\H,-2.9747364961,0.06407652,0.4447023187\C,-2.8129888 552,1.184989447,-1.4045654709\H,-3.3196600838,1.235068705,-2.383652403 6\H,-2.9360994928,2.1748625855,-0.9325461845\C,-4.931577224,0.34699142 62,-0.3018723242\C,-1.3628201049,0.9521580477,-1.637073467\N,-6.003381 1759,0.1162675997,0.1308570361\N,-0.2910167962,1.1828840897,-2.0698034 924\\Version=EM64L-G09RevA.02\HF=-264.2996497\S2=0.751118\S2-1=0.\S2A= 0.750001\RMSD=3.899e-09\RMSF=1.985e-04\Dipole=-0.0000056,-0.0000028,0. 0000005\Quadrupole=-40.65423,22.169849,18.484381,3.3343471,0.1273666,5.257255\PG=C01 [X(C4H4N2)]\\@ Radical anion in THF trans-sn-radicalanion-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C4H4N2(1-,2)\ROZENTE\26-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\trans-cn- CH2-CH2-CN radical anion in THF\\-1,2\C,-3.4780990178,0.1139693276,- 0.5350616553\H,-3.3643766832,-0.8759443943,-1.0072393811\H,- 2.9797475005,0.0660939754,0.4473349648\C,-2.816298337,1.185176679,- 1.4038852414\H,-3.3146502682,1.2330521228,-2.3862818419\H,- 2.9300207032,2.1750904603,-0.9317072468\C,-4.9341764495,0.3728093777,- 0.3177032483\C,-1.3602196393,0.9263349523,-1.6212432858\N,- 5.9923301218,0.0984716808,0.1392680472\N,-0.3020721396,1.2006878183,- 2.0782231913\\Version=EM64L-G09RevA.02\HF=-264.3653729\S2=0.751579\S2-1=0.\S2A=0.750002\RMSD=5.142e-09\RMSF=6.848e-05\Dipole=-0.0001222,- 0.0000225,0.0000475\Quadrupole=-43.6565963,24.09 79759,19.5586204,2.6937024,1.6949709,5.0478287\PG=C01 [X(C4H4N2)]\\@ In the gas phase PN-B3LYP S23

1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C8H7N1\ROZENTE\30-Nov- 2011\0\\#B3LYP/6-31+G* OPT nosymm\\ph-ch2-cn\\0,1\c,0.2903727055,- 0.06575867,0.6527294825\C,1.6154379172,- 0.4286891646,0.3988994934\C,2.4887876342,0.4680173854,- 0.2282768804\C,2.0182896099,1.7330346669,-0.6004063935\C,0.6935663272,2.0977599888,-0.3472911678\C,-0.173342077,1.1988699745,0.2 801278468\H,-0.3780432241,-0.7710588059,1.1396068331\H,1.9719583808,-1.4134863135,0.6933545458\H,0.3398902987,3.0824437323,-0.6415993163\H,- 1.2042507624,1.4816906794,0.4761607037\C,3.9370825201,0.0747192266,-0. 4945664041\H,2.6893544058,2.4376135751,-1.0870370639\H,4.3099178129,0. 5701558602,-1.3993373021\H,4.0160046055,-1.005103694,-0.6702074991\C,4.8385298719,0.4203791626,0.6154764201\N,5.5491289337,0.6938091162,1.49 25650216\\Version=EM64L-G09RevA.02\HF=-363.8164455\RMSD=8.730e- 09\RMSF=1.251e-05\Dipole=-1.1722241,-0.2978881,-1.1159401\Quadrupole=- 10.3951787,8.6590321,1.7361466,-4.7995048,-13.6004234,-3.4493905\PG=C01 [X(C8H7N1)]\\@ In THF PN-B3LYP-SCRF-THF 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C8H7N1\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\ph-ch2-cn inthf\\0,1\c,0.2850965803,-0.069860768,0.645170176\c,1.6099270883,- 0.4372928863,0.3910534637\C,2.4883536353,0.4623155537,- 0.2260874153\C,2.0253870146,1.7336494137,- 0.5893475417\C,0.7010840248,2.1020341854,-0.3354554338\C,- 0.1717459049,1.2011425518,0.28311585\H,-0.3880863753,-0.7770160356,1.1225152937\H,1.9599650896,-1.4277065304,0.6730913089\H,0.3519629582,3.0901006814,-0.6235176943\H,-1.201879818,1.4868737658,0.4787444355\C,3.9355687159,0.0636499313,-0.4946261257\H,2.6994762212,2.4375321529,-1. 0722216006\H,4.3065146529,0.5369700899,-1.4112066805\H,4.0202680383,-1.0196871049,-0.6377207416\C,4.8369139663,0.4438744194,0.60292099\N,5.5 438790723,0.7478172998,1.4737700355\\Version=EM64L-G09RevA.02\HF=-363. 8248745\RMSD=4.844e-09\RMSF=2.468e-06\Dipole=-1.3353976,-0.43213,-1.36 65668\Quadrupole=-12.0137174,9.7781175,2.2355999,-6.1834164,-16.012061 7,-4.013502\PG=C01 [X(C8H7N1)]\\@ Radical anion PN-radical anion-b3lyp 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C8H7N1(1-,2)\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\ph-ch2-cn radical anion\\-1,2\c,0.27680 10906,-0.0762898197,0.6355640786\C,1.6001292528,-0.4332768959,0.400777 9311\C,2.5118756074,0.491363683,-0.1694153985\C,2.0050077547,1.7420005 36,-0.6054396991\C,0.6809722818,2.0952592725,-0.368991033\C,-0.1904914 372,1.2169946287,0.3125994722\H,-0.4001444484,-0.8043812143,1.08400688 S24

74\H,1.9467264965,-1.4352937302,0.6580062191\H,0.320353585,3.067449358,-0.7070881593\H,-1.21379345,1.5121094231,0.5385573394\C,3.9401292069, 0.0957669031,-0.4485823208\H,2.6661567755,2.4323119488,-1.1313533823\H,4.3101016905,0.5946996408,-1.3708125644\H,4.0121808874,-0.9980505493, -0.6352871172\C,4.8750127081,0.4187590683,0.6290022455\N,5.6616669583, 0.6549744671,1.4586538211\\Version=EM64L-G09RevA.02\HF=-363.7966741\S2 =0.752498\S2-1=0.\S2A=0.750004\RMSD=4.152e-09\RMSF=1.095e-05\Dipole=-1.3610824,0.301317,0.0994206\Quadrupole=-30.3191212,16.59284,13.7262812,-5.4609578,-6.7925828,-1.2007634\PG=C01 [X(C8H7N1)]\\@ Radical anion in THF PN-radical anion-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H7N1(1-,2)\ROZENTE\01-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\ph-ch2-cn radical anion in THF\\-1,2\C,0.3461664909,-0.0602706454,0.6890508728\C,1.643 2248736,-0.4551787925,0.3546662828\C,2.5204501836,0.41136795,-0.332095 2103\C,2.0496682861,1.7068815247,-0.6364059535\C,0.753315323,2.1049027 124,-0.3030478992\C,-0.1136374907,1.2219446181,0.3563785088\H,-0.31220 64784,-0.7566029855,1.2050478745\H,1.9841650747,-1.4555630572,0.616839 0109\H,0.4137520119,3.105388296,-0.5645825523\H,-1.1246073973,1.529486 369,0.6127153284\C,3.9454462299,0.0281926609,-0.5865075502\H,2.7091870 734,2.4028660418,-1.1522622592\H,4.3355975529,0.5204580534,-1.48451792 88\H,4.0445848878,-1.0514612368,-0.7458127503\C,4.9653191297,0.3912337 295,0.5847448527\N,4.8422592088,0.9307514814,1.6659876927\\Version=EM6 4L-G09RevA.02\HF=-363.8669778\S2=0.754371\S2-1=0.\S2A=0.750014\RMSD=3.201e-09\RMSF=2.320e-05\Dipole=-4.2081485,- 0.199239,-2.0656963\Quadrupole=-50.9329301,30.0733354,20.8595947,- 12.3623526,-23.9346197,-6.2849519\PG=C01 [X(C8H7N1)]\\@ In the gas phase HC-B3LYP 1\1\GINC-NANO01\FOpt\RB3LYP\6-31+G(d)\C8H15N1\ROZENTE\05-Dec- 2011\0\\#B3LYP/6-31+G* OPT nosymm\\c7- CN\\0,1\C,0.001575893,0.0004440343,-0.06 70164992\H,1.0983623657,0.0175621464,-0.1083516296\H,-0.3476707074,1.0 401762416,-0.1111352719\H,-0.3574031863,-0.509509369,-0.9690792443\C,- 0.4943978722,-0.6977720254,1.2046694093\H,-1.5937185979,-0.7294163056, 1.1996886481\H,-0.1589608266,-1.7451711731,1.2013265129\C,-0.014440245,-0.0184084228,2.4947791058\H,1.0858472134,0.0145878537,2.4981409648\H,-0.3509735548,1.0296766626,2.49851359\C,-0.5050280446,-0.7132092847,3.7725197984\H,-0.1684197312,-1.7608011849,3.7686019583\H,-1.604878526, -0.7455604599,3.7693210723\C,-0.0229546324,-0.0320996846,5.0609463535\ H,-0.3605069614,1.0153467889,5.0666738634\H,1.0770695245,-0.0005634618,5.0658660099\C,-0.517613194,-0.7328863502,6.3325980818\H,-0.177398189 4,-1.7762457603,6.3429823197\H,-1.6146665981,-0.7606973616,6.343524220 8\C,-0.0196367268,-0.0286570776,7.6132969291\H,-0.360721651,1.01469770 81,7.6309003386\H,1.0777192083,-0.0024316682,7.6311218053\C,-0.4834244 S25

685,-0.6842855404,8.8406228871\N,-0.8599637511,-1.2164831055,9.8021929 661\\Version=EM64L-G09RevA.02\HF=-368.6505896\RMSD=5.171e- 09\RMSF=3.404e-05\Dipole=0.4637751,0.6557062,- 1.5768132\Quadrupole=17.1594156,15.7706391,-32.9300548,- 1.9621612,9.7410498,13.772346\PG=C01 [X(C8H15N1)]\\@ In THF HC-B3LYP-SCRF-THF 1\1\GINC-NANO02\FOpt\RB3LYP\6-31+G(d)\C8H15N1\ROZENTE\06-Dec- 2011\0\\#B3LYP/6-31+G* OPT SCRF=(PCM,Solvent=THF) nosymm\\c7-cn in THF\\0,1\C,0.0004573013,0.0025677538,0.0658438059\H,1.0973786508,0.0195886 055,-0.1067273513\H,-0.3494528746,1.0423066067,-0.1074275441\H,- 0.3591218236,-0.5066238835,-0.968323901\C,-0.4946438309,- 0.6972739876,1.2056855366\H,-1.5939951705,-0.7282229775,1.2013556867\H,- 0.1582854706,-1.7443770853,1.2009288536\C,-0.0139682871,- 0.0191322432,2.4961074214\H,1.0862790794,0.01305359,2.4991535694\H,- 0.3518028719,1.0284632339,2.5014278593\C,-0.5039470082,- 0.715660257,3.7731207916\H,-0.1652042921,-1.7625054312,3.7684810242\H,- 1.603759928,-0.7475840031,3.7701257244\C,-0.021791662,- 0.0340649355,5.0611236645\H,-0.3611083251,1.0122867545,5.068820025 \H,1.0777752817,-0.0041265161,5.0683899024\C,-0.5184146543,-0.73706330 51,6.3306302351\H,-0.1745777557,-1.7789182038,6.3410769846\H,-1.615219 2429,-0.7624927657,6.3399239651\C,-0.0188533177,-0.0274219874,7.608819 5063\H,-0.3602788295,1.0150490443,7.6269763969\H,1.0777635217,-0.00491 91013,7.6314607797\C,-0.4845954737,-0.6782664333,8.8366239905\N,-0.862 8362763,-1.206369272,9.8007948752\\Version=EM64L-G09RevA.02\HF=-368.65 7598\RMSD=9.560e-09\RMSF=6.034e-06\Dipole=0.5780144,0.8064279,-1.79863 5\Quadrupole=19.9641239,18.395802,-38.3599259,-2.2734087,11.8276037,16.5186812\PG=C01 [X(C8H15N1)]\\@ Radical anion HC-radical anion-b3lyp 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C8H15N1(1-,2)\ROZENTE\05-Dec- 2011\0\\# B3LYP/6-31+G* OPT nosymm\\c7-cn radical anion\\-1,2\c,0.01682761 58,0.0207764778,-0.0740211019\H,1.1146449493,0.0394703351,-0.109693282 \H,-0.3244443342,1.0643060028,-0.1123464409\H,-0.3312654948,-0.4703121 845,-0.9934391902\C,-0.4905529464,-0.6892532951,1.1861484608\H,-1.5907 699275,-0.7195074902,1.1731098487\H,-0.1599786998,-1.7391001416,1.1742 561228\C,-0.0180689838,-0.0253244119,2.4875949557\H,1.0817477263,0.009 3345306,2.4967860212\H,-0.3481525839,1.0243721805,2.4983790277\C,-0.51 49638384,-0.7271366229,3.7581845213\H,-0.1813754968,-1.7768005217,3.74 87207656\H,-1.6158025398,-0.7614344967,3.7487856389\C,-0.0365195652,-0.0511216855,5.0519138633\H,-0.3671302519,0.9974917319,5.0630377518\H,1.0622368905,-0.0109965275,5.0614697248\C,-0.5349321941,-0.7596956752,6.3187992794\H,-0.1961537606,-1.8049785989,6.3196192854\H,-1.6331481266,-0.7956107441,6.3190290855\C,-0.0583610061,-0.0798474124,7.6174673713 \H,-0.3985236713,0.9718682171,7.6424736819\H,1.0462754452,-0.039709625 9,7.6426249524\C,-0.506288279,-0.7196091853,8.8670620467\N,-0.68750418 69,-0.9788876562,9.9967417999\\Version=EM64L-G09RevA.02\HF=-368.614007 2\S2=0.750285\S2-1=0.\S2A=0.75\RMSD=6.425e-09\RMSF=9.973e-06\Dipole=-0.5433035,-0.7661345,-1.9044442\Quadrupole=71.2739681,68.4817094,-139.7 556775,-3.9235422,5.7062343,8.0547835\PG=C01 [X(C8H15N1)]\\@ S26

Radical anion in THF HC-radical anion-b3lyp-scrf-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H15N1(1-,2)\ROZENTE\06-Dec- 2011\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\c7-cn radical anion in THF\\-1,2\C,0.0179051679,0.0319034097,- 0.077372306\H,1.1153783638,0.0457308609,-0.106365347\H,- 0.3276284717,1.0733755331,-0.1149037952\H,-0.3334654352,-0.4691321252,- 0.9879486331\C,-0.4922863968,-0.6750682888,1.1844748668\H,-1.59178779,- 0.7025796411,1.1686828207\H,-0.159880644,-1.72358196,1.1745962009\C,- 0.0221692266,-0.0103844636,2.4858280 302\H,1.0784103097,0.0211471559,2.4965799939\H,-0.3579950028,1.0381382 061,2.4978085847\C,-0.519881379,-0.7169879253,3.7543848505\H,-0.189615 4356,-1.7670088793,3.7356583282\H,-1.6204416346,-0.7429573285,3.746800 589\C,-0.0377813618,-0.0613051075,5.0567169112\H,-0.373290417,0.986763 4202,5.0810516161\H,1.0629144869,-0.0288692379,5.0577259588\C,-0.52061 94568,-0.7853257803,6.3212731574\H,-0.1977957433,-1.8361417647,6.28794 67516\H,-1.621206773,-0.8057378033,6.3339907214\C,-0.0147483645,-0.158 8893768,7.6280145283\H,-0.3816738445,0.8823645462,7.7147689399\H,1.085 0396917,-0.1110982304,7.5980592126\C,-0.4064728313,-0.9527722331,8.889 9083493\N,-0.8631110716,-0.5532897861,9.9550238599\\Version=EM64L-G09R eva.02\hf=-368.6928857\s2=0.75327\s2-1=0.\s2a=0.750006\rmsd=8.882e-09\ RMSF=8.839e-06\Dipole=0.7912121,0.9542987,-9.2712234\Quadrupole=113.47 23114,109.3630958,-222.8354071,-2.15447,25.8775603,30.4122864\PG=C01 [ X(C8H15N1)]\\@ Radical in THF α-amino-p-tolunitrile-radical-b3lyp-thf 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H7N2(2)\ROZENTE\11-Jan- 2012\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph- CNCH-NH2-radical in THF\\0,2\C,0.1736243972,- 0.2662306059,0.8984459565\C,1.3817383039,- 0.0913492668,1.6491977255\C,2.2573241329,0.9378188481,1.380611881 4\C,1.9807846296,1.8619628634,0.3364568503\C,0.793647282,1.7044166256, -0.4225387877\C,-0.0838108884,0.6730894765,-0.1535276454\H,1.607307867 9,-0.7895049173,2.4516551354\H,0.5772834075,2.4032884535,-1.2253884314 \H,-0.9772019714,0.5831628575,-0.764540057\C,2.8802495147,2.9254042908,0.0549399583\N,3.6216265933,3.8000852608,-0.1748841632\H,3.1652133134,1.0480283914,1.9662430233\C,-0.689752815,-1.3282841078,1.2232442944\N,-1.8552054441,-1.6307058584,0.5836485392\H,-2.3016137889,-0.962955278,-0.0314142387\H,-0.4130465315,-2.0143207811,2.0173049328\H,-2.4789035 S27

631,-2.3079730622,1.0002650562\\Version=EM64L-G09RevA.02\HF=-418.55316 56\S2=0.768332\S2-1=0.\S2A=0.750233\RMSD=8.049e-09\RMSF=2.989e-05\Dipo le=-3.1575008,-2.9618859,0.7085771\quadrupole=-1.8009497,-8.2415004,10.0424501,-13.3195323,2.919283,-3.9142129\pg=c01 [X(C8H7N2)]\\@ Radical in THF α-amino-p-tolunitrile-radical-b3lyp-thf 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C8H7N2(2)\ROZENTE\11-Jan- 2012\0\\#B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph- CNCH2-NH-radical in THF\\0,2\C,0.2195440598,- 0.3482004976,0.5609901257\C,1.0935102246,- 0.0201395023,1.6089282411\C,1.957008722,1.0677355713,1.5053775715 \C,1.9537448834,1.8481601347,0.3352032103\C,1.0829246079,1.5292869471, -0.7221153346\C,0.2259304646,0.4379649884,-0.6019947328\H,1.1044612887,-0.6230678247,2.5134884956\H,1.0839593368,2.1307932272,-1.6256069348\ H,-0.4429934185,0.1915711395,-1.4222441171\C,2.8437610552,2.9664396612,0.2180392157\N,3.5667863842,3.874615581,0.1231147842\H,2.6345133734,1.3112182484,2.3176791268\C,-0.7547086978,-1.506971353,0.6856021039\N,- 2.0736083711,-1.1136181542,1.1551899241\H,-1.9331613653,-0.4589423614, 1.9391078747\H,-0.3548605509,-2.2455592588,1.4035368208\H,-0.866670127 2,-2.0239947267,-0.2735873552\\Version=EM64L-G09RevA.02\HF=-418.513644 3\S2=0.753834\S2-1=0.\S2A=0.750011\RMSD=9.418e-09\RMSF=1.234e-05\Dipol e=-0.5525578,-1.5948027,0.4554917\quadrupole=-9.4269121,-6.5167749,15. 943687,-16.1822922,2.8461253,-1.3454539\PG=C01 [X(C8H7N2)]\\@ Radical in THF α-amino-p-tolunitrile--radical-b3lyp-thf 1\1\GINC-NANO02\FOpt\UB3LYP\6-31+G(d)\C8H7N2(2)\ROZENTE\11-Jan- 2012\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph- CNHCH-NH-radical\\0,2\C,0.0600420982,- 0.292912674,0.5835170087\C,0.3662862429,0.5494844509,1.6847602458\C,1.2173 788251,1.6236504475,1.556193045\C,1.8348761318,1.9123664058,0.2896449607\C S28

,1.5219549567,1.0675536167,-0.8286710891\C,0.6639059351,-0.000268067,- 0.6645188136\H,- 0.0720170664,0.3528045071,2.6600106621\H,1.970802604,1.2730375625,- 1.7952935918\H,0.4457010944,-0.6384733795,- 1.5179604634\C,2.6371801899,3.0166794281,0.1383815456\N,3.6336990574,3.728 8815413,0.1012833636\H,1.4365854135,2.2573041978,2.4098448648\C,- 0.8391323617,-1.4438724137,0.6778020713\N,-1.4936682738,- 1.8988963902,1.6920557502\H,-1.3243191929,-1.3334710393,2.531503 0145\H,-0.9671592108,-1.9945365818,-0.2600037049\H,3.5266168964,4.7211 759378,-0.1411796496\\Version=EM64L-G09RevA.02\HF=-418.5057945\S2=0.77 9124\S2-1=0.\S2A=0.750604\RMSD=6.016e-09\RMSF=7.405e-06\Dipole=0.92811 41,2.0102344,-0.5666168\Quadrupole=-8.5524494,4.5462202,4.0062292,0.32 23267,0.4389079,4.3174544\PG=C01 [X(C8H7N2)]\\@ Radical in THF 1,4-Ph-CH=NCH-NH-radical-B3LYP-THF 1\1\GINC-NANO01\FOpt\UB3LYP\6-31+G(d)\C8H7N2(2)\ROZENTE\11-Jan- 2012\0\\# B3LYP/6-31+G* OPT SCRF=(PCM, Solvent=THF) nosymm\\1,4-ph- CH=NCH-NH-radical in THF\\0,2\C,0.0273403723,- 0.2771268292,0.6029669455\C,0.3713291032,0.5034288785,1.7191416007\C,1.255 9212895,1.5698141625,1.5881165757\C,1.817375491,1.8806772489,0.3381890888\ C,1.4780371741,1.1048404727,-0.7826177703\C,0.5930958271,0.0403135631,- 0.6458454775\H,- 0.0472480547,0.2854973193,2.6980562013\H,1.9070724337,1.3378262272,- 1.7524097271\H,0.3334344933,-0.5571809678,- 1.5163227138\C,2.7570060606,3.024984633,0.2386178452\N,3.3407537814,3.4298 797963,-0.8008200858\H,1.5144391375,2.1663046997,2.4590227406\C,- 0.907352608,-1.425972001,0.675959777\N,-1.5336620513,- 1.8987655351,1.6879170742\H,-1.3256733147,-1.3731443698,2.5444936091\H,- 1.0743805756,-1.9320338888,-0.2799924799\H,2.956215622, 3.5681983806,1.1778825921\\Version=EM64L-G09RevA.02\HF=-418.5146223\S2 =0.762707\S2-1=0.\S2A=0.750088\RMSD=6.259e-09\RMSF=1.647e-05\Dipole=0. 0827947,0.3351968,0.732384\Quadrupole=-5.8754144,-4.5666462,10.4420606,-8.2378939,7.6104319,11.3047684\PG=C01 [X(C8H7N2)]\\@ S29