Experimental. Crystal data. C 37 H 38 N 4 O 6 M r = Monoclinic, P2 1 a = (2) Å b = (7) Å c = (2) Å = 112.
|
|
|
- Αλκιππη Κουταλιανός
- 6 χρόνια πριν
- Προβολές:
Transcript
1 organic compounds Acta Crystallographica Section E Structure Reports Online ISSN Pheophorbide b ethyl ester from a chlorella vulgaris dietary supplement Experimental Crystal data C 37 H 38 N 4 O 6 M r = Monoclinic, P2 1 a = (2) Å b = (7) Å c = (2) Å = (2) V = (7) Å 3 Z =2 Mo K radiation = 0.09 mm 1 T = 100 (2) K mm Chin Fei Chee, Noorsaadah Abdul Rahman, Sharifuddin M. Zain and Seik Weng Ng* Department of Chemistry, University of Malaya, Kuala Lumpur, Malaysia Correspondence seikweng@um.edu.my Received 10 September 2008; accepted 16 September 2008 Key indicators: single-crystal X-ray study; T = 100 K; mean (C C) = Å; R factor = 0.064; wr factor = 0.178; data-to-parameter ratio = 8.3. In the title compound, C 37 H 38 N 4 O 6, four five-membered nitrogen-bearing rings are nearly coplanar. Two N atoms in two these five-membered rings have attached H atoms, which contribute to the formation of intramolecular N HN hydrogen bonds [NN = (5) (6) Å]. Related literature For the crystal structure of pheophorbide a methyl ester, see: Fischer et al. (1972). For another example of a chlorin, see: Senge & Smith (1997). Data collection Bruker SMART APEX diffractometer Absorption correction: none measured reflections Refinement R[F 2 >2(F 2 )] = wr(f 2 ) = S = reflections 438 parameters 3 restraints Table 1 Hydrogen-bond geometry (Å, ) independent reflections 3100 reflections with I > 2(I) R int = H atoms treated by a mixture of independent and constrained refinement max = 0.55 e Å 3 min = 0.38 e Å 3 D HA D H HA DA D HA N1 H1NN (3) 2.48 (9) (6) 111 (7) N1 H1NN (3) 2.42 (8) (6) 127 (8) N3 H3NN (3) 1.99 (4) (5) 139 (5) Data collection: APEX2 (Bruker, 2007); cell refinement: SAINT (Bruker, 2007); data reduction: SAINT; program(s) used to solve structure: SHELXS97 (Sheldrick, 2008); program(s) used to refine structure: SHELXL97 (Sheldrick, 2008); molecular graphics: X-SEED (Barbour, 2001); software used to prepare material for publication: publcif (Westrip, 2008). We thank the University of Malaya (grant No. PS149/ 2007B) for supporting this study. Supplementary data and figures for this paper are available from the IUCr electronic archives (Reference: CV2447). References Barbour, L. J. (2001). J. Supramol. Chem. 1, Bruker (2007). APEX2 and SAINT. Bruker AXS Inc., Madison, Wisconsin, USA. Fischer, M. S., Templeton, D. H., Zalkin, A. & Calvin, M. (1972). J. Am. Chem. Soc. 94, Senge, M. O. & Smith, K. M. (1997). Acta Cryst. C53, Sheldrick, G. M. (2008). Acta Cryst. A64, Westrip, S. P. (2008). publcif. In preparation. o1986 Chee et al. doi: /s x Acta Cryst. (2008). E64, o1986
2
3 Acta Cryst. (2008). E64, o1986 [ doi: /s x ] Pheophorbide b ethyl ester from a chlorella vulgaris dietary supplement C. F. Chee, N. A. Rahman, S. M. Zain and S. W. Ng Experimental A sample of the dietary supplement Chlorenergy (C'est Si Bon Co., USA) (20 g) was dissolved in 100 ml e thanol and 10 ml dilute sulfuric acid (10%, v/v). The mixture was heated at 323 K for 2 h. The solution was cooled and then stirred at room temperature for 3 days under normal day light (light intensity not measured), during which the solution turned green yellowish. The solvent was evaporated to dryness at reduced pressure. The crude product was purified by HPLC on an RP18e semi-preparative column (Merck Chromolith mm) with acetonitrile-water (90:10, v/v) as the eluent. Pheophorbide b ethyl ester was isolated as brownish plates. Single crystals were grown by slow evaporation of a mixture of acetone and chloroform solution. Refinement C-bound H-atoms were placed in calculated positions (C H 0.95 to 0.99 Å) and were included in the refinement in the riding model approximation, with U iso (H) set to U eq (C). The amino H-atoms were located on a difference Fourier map, and were isotropically refined with a distance restraint N H=0.88 (2) Å). In the absence of heavy scatterers, 3452 Friedel pairs were merged in the refinement. Figures Fig. 1. The molecular structure of the title compound showing the atomic numbering and 70% probability displacement ellipsoids. (I) Crystal data C 37 H 38 N 4 O 6 F 000 = 672 M r = Monoclinic, P2 1 Hall symbol: P 2yb D x = Mg m 3 Mo Kα radiation λ = Å a = (2) Å θ = º b = (7) Å c = (2) Å β = (2)º Cell parameters from 3714 reflections µ = 0.09 mm 1 T = 100 (2) K Plate, brown sup-1
4 V = (7) Å 3 Z = mm Data collection Bruker SMART APEX diffractometer Radiation source: fine-focus sealed tube R int = Monochromator: graphite θ max = 27.5º T = 100(2) K θ min = 1.3º ω scans Absorption correction: None 3100 reflections with I > 2σ(I) h = 9 9 k = measured reflections l = independent reflections Refinement Refinement on F 2 Least-squares matrix: full R[F 2 > 2σ(F 2 )] = Secondary atom site location: difference Fourier map Hydrogen site location: inferred from neighbouring sites H atoms treated by a mixture of independent and constrained refinement wr(f 2 ) = w = 1/[σ 2 (F o 2 ) + (0.0986P) P] where P = (F o 2 + 2F c 2 )/3 S = 1.17 (Δ/σ) max = reflections Δρ max = 0.55 e Å parameters Δρ min = 0.38 e Å 3 3 restraints Extinction correction: none Primary atom site location: structure-invariant direct methods Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å 2 ) x y z U iso */U eq O (6) (12) (5) (8) O (6) (13) (6) (9) O (6) (11) (5) (8) O (5) (12) (5) (7) O (5) (12) (4) (7) O (7) (13) (5) (9) N (7) (14) (6) (8) H1N (11) (3) (3) 0.06 (3)* N (6) (13) (5) (8) N (6) (13) (5) (8) H3N (8) (19) (3) (15)* N (6) (13) (5) (8) C (7) (16) (6) (9) C (7) (17) (6) (9) sup-2
5 C (9) (19) (7) (12) H * C (11) (2) (8) (16) H4A * H4B * C (7) (16) (6) (9) C (8) (17) (6) (10) H6A * H6B * H6C * C (7) (16) (6) (9) C (7) (16) (6) (9) H * C (7) (16) (6) (9) C (7) (15) (6) (9) H * C (9) (16) (7) (10) H11A * H11B * H11C * C (7) (16) (6) (9) H * C (7) (15) (6) (9) H13A * H13B * C (8) (16) (7) (10) H14A * H14B * C (8) (16) (7) (10) C (9) (19) (7) (11) H16A * H16B * C (9) (2) (9) (12) H17A * H17B * H17C * C (7) (15) (6) (9) C (7) (15) (6) (9) C (7) (15) (6) (9) H * C (7) (15) (6) (9) C (8) (16) (7) (10) H22A * H22B * H22C * C (7) (16) (7) (9) C (7) (15) (6) (9) C (7) (16) (7) (9) C (7) (16) (6) (9) sup-3
6 C (8) (17) (7) (10) H27A * H27B * H27C * C (7) (16) (6) (9) C (7) (16) (7) (9) H * C (7) (16) (7) (9) C (7) (16) (7) (10) C (8) (17) (7) (10) H32A * H32B * C (9) (2) (9) (12) H33A * H33B * H33C * C (8) (17) (7) (11) C (9) (17) (7) (10) H * C (8) (17) (7) (10) C (8) (16) (7) (10) H * Atomic displacement parameters (Å 2 ) U 11 U 22 U 33 U 12 U 13 U 23 O (18) (19) (17) (15) (14) (14) O (2) (2) (2) (16) (18) (17) O (19) (17) (19) (14) (15) (14) O (16) (18) (18) (14) (14) (14) O (17) (19) (16) (14) (13) (13) O (3) (2) (2) (18) (18) (16) N (19) (19) (19) (15) (16) (15) N (2) (2) (2) (15) (16) (15) N (19) (19) (19) (15) (16) (15) N (19) (2) (19) (15) (16) (15) C (2) (2) (2) (18) (17) (17) C (2) (2) (2) (18) (18) (18) C (3) (3) (2) (2) (2) (2) C (4) (3) (3) (3) (3) (2) C (2) (2) (2) (18) (18) (17) C (2) (3) (2) (19) (18) (18) C (2) (2) (2) (17) (17) (17) C (2) (2) (2) (17) (16) (17) C (2) (2) (2) (18) (17) (17) C (2) (2) (2) (18) (17) (17) C (3) (2) (2) (2) (2) (18) C (2) (2) (2) (17) (17) (17) sup-4
7 C (2) (2) (2) (18) (18) (17) C (3) (2) (2) (19) (19) (18) C (2) (2) (2) (18) (19) (19) C (3) (3) (3) (2) (2) (2) C (3) (3) (3) (2) (2) (2) C (2) (2) (2) (17) (18) (17) C (2) (2) (2) (17) (17) (17) C (2) (2) (2) (18) (17) (16) C (2) (2) (2) (17) (17) (17) C (2) (2) (3) (18) (2) (19) C (2) (2) (2) (18) (18) (18) C (2) (2) (2) (17) (17) (17) C (2) (2) (2) (18) (17) (18) C (2) (2) (2) (18) (18) (18) C (2) (3) (2) (2) (19) (19) C (2) (2) (2) (17) (17) (18) C (2) (2) (2) (17) (18) (18) C (2) (2) (2) (17) (19) (18) C (2) (2) (3) (18) (19) (2) C (2) (3) (3) (2) (2) (2) C (3) (3) (3) (2) (2) (2) C (3) (3) (2) (2) (2) (19) C (3) (2) (2) (2) (2) (19) C (2) (2) (2) (18) (19) (19) C (3) (2) (2) (2) (2) (18) Geometric parameters (Å, ) O1 C (6) C13 H13A O1 C (6) C13 H13B O2 C (6) C14 C (7) O3 C (6) C14 H14A O3 C (6) C14 H14B O4 C (6) C16 C (8) O5 C (6) C16 H16A O6 C (7) C16 H16B N1 C (6) C17 H17A N1 C (6) C17 H17B N1 H1N 0.88 (3) C17 H17C N2 C (6) C18 C (6) N2 C (6) C19 C (7) N3 C (6) C19 C (6) N3 C (6) C20 C (6) N3 H3N 0.88 (3) C20 C (6) N4 C (6) C20 H N4 C (6) C22 H22A C1 C (7) C22 H22B C1 C (6) C22 H22C C2 C (7) C23 C (7) sup-5
8 C2 C (7) C24 C (7) C3 C (9) C24 C (6) C3 H C26 C (6) C4 H4A C26 C (7) C4 H4B C27 H27A C5 C (6) C27 H27B C5 C (7) C27 H27C C6 H6A C28 C (7) C6 H6B C29 C (7) C6 H6C C29 H C7 C (7) C30 C (7) C8 C (6) C31 C (7) C8 H C31 C (7) C9 C (7) C32 C (8) C10 C (7) C32 H32A C10 C (6) C32 H32B C10 H C33 H33A C11 H11A C33 H33B C11 H11B C33 H33C C11 H11C C34 C (7) C12 C (7) C34 C (7) C12 C (6) C35 H C12 H C36 C (7) C13 C (7) C37 H C15 O1 C (4) C16 C17 H17B C21 O3 C (4) H17A C17 H17B C7 N1 C (4) C16 C17 H17C C7 N1 H1N 131 (6) H17A C17 H17C C1 N1 H1N 116 (6) H17B C17 H17C C9 N2 C (4) N2 C18 C (4) C25 N3 C (4) N2 C18 C (4) C25 N3 H3N 135 (4) C19 C18 C (4) C28 N3 H3N 115 (4) C18 C19 C (4) C36 N4 C (4) C18 C19 C (4) C37 C1 N (4) C25 C19 C (4) C37 C1 C (4) C19 C20 C (4) N1 C1 C (4) C19 C20 C (4) C5 C2 C (5) C21 C20 C (4) C5 C2 C (4) C19 C20 H C3 C2 C (5) C21 C20 H C4 C3 C (5) C23 C20 H C4 C3 H O4 C21 O (4) C2 C3 H O4 C21 C (4) C3 C4 H4A O3 C21 C (4) C3 C4 H4B O3 C22 H22A H4A C4 H4B O3 C22 H22B C2 C5 C (4) H22A C22 H22B C2 C5 C (4) O3 C22 H22C C7 C5 C (4) H22A C22 H22C sup-6
9 C5 C6 H6A H22B C22 H22C C5 C6 H6B O5 C23 C (5) H6A C6 H6B O5 C23 C (4) C5 C6 H6C C24 C23 C (4) H6A C6 H6C C26 C24 C (4) H6B C6 H6C C26 C24 C (4) N1 C7 C (4) C25 C24 C (4) N1 C7 C (4) N3 C25 C (5) C8 C7 C (4) N3 C25 C (4) C7 C8 C (4) C19 C25 C (4) C7 C8 H C24 C26 C (4) C9 C8 H C24 C26 C (4) N2 C9 C (4) C28 C26 C (4) N2 C9 C (4) C26 C27 H27A C8 C9 C (4) C26 C27 H27B C9 C10 C (4) H27A C27 H27B C9 C10 C (4) C26 C27 H27C C11 C10 C (4) H27A C27 H27C C9 C10 H H27B C27 H27C C11 C10 H C29 C28 N (4) C12 C10 H C29 C28 C (4) C10 C11 H11A N3 C28 C (4) C10 C11 H11B C28 C29 C (4) H11A C11 H11B C28 C29 H C10 C11 H11C C30 C29 H H11A C11 H11C N4 C30 C (4) H11B C11 H11C N4 C30 C (4) C18 C12 C (4) C29 C30 C (4) C18 C12 C (4) C34 C31 C (4) C13 C12 C (4) C34 C31 C (5) C18 C12 H C30 C31 C (5) C13 C12 H C31 C32 C (4) C10 C12 H C31 C32 H32A C14 C13 C (4) C33 C32 H32A C14 C13 H13A C31 C32 H32B C12 C13 H13A C33 C32 H32B C14 C13 H13B H32A C32 H32B C12 C13 H13B C32 C33 H33A H13A C13 H13B C32 C33 H33B C15 C14 C (4) H33A C33 H33B C15 C14 H14A C32 C33 H33C C13 C14 H14A H33A C33 H33C C15 C14 H14B H33B C33 H33C C13 C14 H14B C31 C34 C (4) H14A C14 H14B C31 C34 C (5) O2 C15 O (5) C36 C34 C (5) O2 C15 C (5) O6 C35 C (5) O1 C15 C (4) O6 C35 H O1 C16 C (5) C34 C35 H sup-7
10 O1 C16 H16A N4 C36 C (5) C17 C16 H16A N4 C36 C (4) O1 C16 H16B C37 C36 C (5) C17 C16 H16B C1 C37 C (5) H16A C16 H16B C1 C37 H C16 C17 H17A C36 C37 H C7 N1 C1 C (5) C19 C20 C21 O (4) C7 N1 C1 C2 0.6 (5) C23 C20 C21 O (4) C37 C1 C2 C (5) C19 C20 C23 O (4) N1 C1 C2 C5 0.0 (5) C21 C20 C23 O (6) C37 C1 C2 C3 4.1 (8) C19 C20 C23 C (4) N1 C1 C2 C (5) C21 C20 C23 C (4) C5 C2 C3 C (7) O5 C23 C24 C (10) C1 C2 C3 C4 9.4 (11) C20 C23 C24 C (6) C3 C2 C5 C (4) O5 C23 C24 C (5) C1 C2 C5 C7 0.5 (5) C20 C23 C24 C (5) C3 C2 C5 C6 4.8 (8) C28 N3 C25 C (5) C1 C2 C5 C (4) C28 N3 C25 C (5) C1 N1 C7 C (4) C18 C19 C25 N3 0.8 (9) C1 N1 C7 C5 0.9 (5) C20 C19 C25 N (5) C2 C5 C7 N1 0.9 (5) C18 C19 C25 C (4) C6 C5 C7 N (4) C20 C19 C25 C (5) C2 C5 C7 C (4) C26 C24 C25 N3 0.1 (5) C6 C5 C7 C8 2.7 (8) C23 C24 C25 N (4) N1 C7 C8 C9 3.0 (8) C26 C24 C25 C (4) C5 C7 C8 C (4) C23 C24 C25 C (5) C18 N2 C9 C (4) C25 C24 C26 C (5) C18 N2 C9 C (5) C23 C24 C26 C (6) C7 C8 C9 N2 0.3 (8) C25 C24 C26 C (4) C7 C8 C9 C (4) C23 C24 C26 C (9) N2 C9 C10 C (4) C25 N3 C28 C (4) C8 C9 C10 C (6) C25 N3 C28 C (5) N2 C9 C10 C (5) C24 C26 C28 C (5) C8 C9 C10 C (4) C27 C26 C28 C (8) C9 C10 C12 C (4) C24 C26 C28 N3 1.2 (5) C11 C10 C12 C (4) C27 C26 C28 N (4) C9 C10 C12 C (4) N3 C28 C29 C (7) C11 C10 C12 C (4) C26 C28 C29 C (4) C18 C12 C13 C (4) C36 N4 C30 C (4) C10 C12 C13 C (5) C36 N4 C30 C (5) C12 C13 C14 C (5) C28 C29 C30 N4 0.2 (7) C16 O1 C15 O2 1.7 (7) C28 C29 C30 C (5) C16 O1 C15 C (4) N4 C30 C31 C (6) C13 C14 C15 O (7) C29 C30 C31 C (5) C13 C14 C15 O (5) N4 C30 C31 C (5) C15 O1 C16 C (6) C29 C30 C31 C (8) C9 N2 C18 C (4) C34 C31 C32 C (7) C9 N2 C18 C (5) C30 C31 C32 C (6) C13 C12 C18 N (4) C30 C31 C34 C (5) sup-8
11 C10 C12 C18 N (5) C32 C31 C34 C (5) C13 C12 C18 C (6) C30 C31 C34 C (5) C10 C12 C18 C (4) C32 C31 C34 C (9) N2 C18 C19 C (7) C31 C34 C35 O (6) C12 C18 C19 C (4) C36 C34 C35 O6 4.9 (9) N2 C18 C19 C (4) C30 N4 C36 C (5) C12 C18 C19 C (7) C30 N4 C36 C (5) C18 C19 C20 C (6) C31 C34 C36 N4 0.3 (6) C25 C19 C20 C (4) C35 C34 C36 N (5) C18 C19 C20 C (4) C31 C34 C36 C (5) C25 C19 C20 C (5) C35 C34 C36 C (8) C22 O3 C21 O4 1.7 (7) N1 C1 C37 C (9) C22 O3 C21 C (4) C2 C1 C37 C (5) C19 C20 C21 O (6) N4 C36 C37 C1 1.1 (9) C23 C20 C21 O (5) C34 C36 C37 C (5) Hydrogen-bond geometry (Å, ) D H A D H H A D A D H A N1 H1N N (3) 2.48 (9) (6) 111 (7) N1 H1N N (3) 2.42 (8) (6) 127 (8) N3 H3N N (3) 1.99 (4) (5) 139 (5) sup-9
12 Fig. 1 sup-10
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 [1,2-Bis(1H-benzimidazol-2-yl-jN 3 )- ethane]dichloridozinc(ii) Yan-Ling Zhou, a Ming-Hua Zeng a and Seik
Triclinic, P1 a = (2) Å b = (3) Å c = (4) Å = (1) = (1) = (1) Data collection.
organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Benzyl N 0 -(4,6-dimethoxy-2-methyl-3- phenyl-1h-indol-7-ylmethylene)- hydrazinecarbodithioate Hamid Khaldei,
Experimental. Crystal data
organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Terephthalic acid 2,2 0 -dimethyl-1,1 0 - (butane-1,4-diyl)dibenzimidazole (2/3) Hui Jiang and Xian-Wu Dong* Department
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 2,2 0 -Biimidazolium hexaaquamanganese(ii) bis(sulfate) Mukhtar A. Kurawa, Christopher J. Adams and A. Guy
Supplementary Material
Supplementary Material Synthesis of bis-oxathiaaza[3.3.3]propellanes via nucleophilic addition of (1,ω-alkanediyl)bis(N'-organylthioureas) on dicyanomethylene-1,3-indanedione Alaa A. Hassan, a * Kamal
Synthesis of New Heteroscorpionate Iridium(I) and Iridium(III) Complexes
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2015 ELECTRONIC SUPPORTING INFORMATION For Synthesis of New Heteroscorpionate Iridium(I)
Experimental. Crystal data. C 37 H 24 N 2 O 3 M r = Orthorhombic, P a = (1) Å b = (2) Å c = 26.
organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 1,3-Bis(naphthalen-2-ylmethyl)-1H- anthra[1,2-d]imidazole-2,6,11(3h)- trione Zahra Afrakssou, a Youssef Kandri
Supporting Information-B. A Facile Iterative Synthesis of 2,5-Terpyrimidinylenes as Non-peptidic α-helical Mimics
Supporting Information-B A Facile Iterative Synthesis of 2,5-Terpyrimidinylenes as on-peptidic α-helical Mimics Laura Anderson, 1,2 Mingzhou Zhou, 1,2 Vasudha Sharma, 2 Jillian M. McLaughlin, 2 Daniel.
data reports 2-(4-Methylphenyl)-2-oxoethyl 3,4-dimethoxybenzoate Structure description Synthesis and crystallization Refinement
2-(4-Methylphenyl)-2-oxoethyl 3,4-dimethoxybenzoate ISSN 2414-3146 Shamantha Kumar, a Chandra, b B. M. Rajesh, c M. Mahendra b and B. H. Doreswamy a * Received 27 December 2016 Accepted 2 February 2017
organic papers 7,8-Dihydroxy-3-methyl-10-oxo-1H,10Hpyrano[4,3-b]chromene-9-carboxylic
![organic papers 7,8-Dihydroxy-3-methyl-10-oxo-1H,10Hpyrano[4,3-b]chromene-9-carboxylic](/thumbs/91/105777620.jpg "organic papers 7,8-Dihydroxy-3-methyl-10-oxo-1H,10Hpyrano[4,3-b]chromene-9-carboxylic")
organic papers Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 7,8-Dihydroxy-3-methyl-10-oxo-1H,10Hpyrano[4,3-b]chromene-9-carboxylic acid Jian-Feng Wang, a * Yong-Jie Zhang, b
Experimental. Crystal data. C 23 H 27 ClN 2 O M r = Triclinic, P1 a = (3) Å b = (6) Å c = (7) Å = (4) = 80.
organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 8-{(E)-[(4-Chlorophenyl)imino]methyl}- 1,1,7,7-tetramethyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinolin-9-ol
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Pentakis(2-oxo-2,3-dihydropyrimidin-1- ium) di-l 3 -chlorido-tri-l 2 -chlorido-hexachloridotricadmate(ii)
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Triethylammonium bis(oxalato)- oxido(triphenylphosphane)rhenate(v) Philipp Grimminger and Peter Klüfers*
Enantioselective Synthesis of the Anti-inflammatory Agent ( )-Acanthoic Acid
Enantioselective Synthesis of the Anti-inflammatory Agent ( )-Acanthoic Acid Taotao Ling, a Chinmay Chowdhury, a Bryan A. Kramer, a Binh G. Vong, a Michael A. Palladino b and Emmanuel A. Theodorakis a
IV. ANHANG 179. Anhang 178
Anhang 178 IV. ANHANG 179 1. Röntgenstrukturanalysen (Tabellen) 179 1.1. Diastereomer A (Diplomarbeit) 179 1.2. Diastereomer B (Diplomarbeit) 186 1.3. Aldoladdukt 5A 193 1.4. Aldoladdukt 13A 200 1.5. Aldoladdukt
Supporting Information File 2. Crystallographic data of syn-bis-quinoxaline, 16c CH 3 CO 2 C 2 H 5 ;
Supporting Information File 2 Crystallographic data of syn-bis-quinoxaline, 16c CH 3 CO 2 C 2 H 5 ; Preparation, structures and host guest chemistry of fluorinated syn-bisquinoxaline molecular tweezers
Supplementary information
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2015 Supplementary information Hybrids of acylated homoserine lactone and nitric
Enantioselective Organocatalytic Michael Addition of Isorhodanines. to α, β-unsaturated Aldehydes
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2016 Enantioselective Organocatalytic Michael Addition of Isorhodanines to α,
Cycloaddition of Homochiral Dihydroimidazoles: A 1,3-Dipolar Cycloaddition Route to Optically Active Pyrrolo[1,2-a]imidazoles
![Cycloaddition of Homochiral Dihydroimidazoles: A 1,3-Dipolar Cycloaddition Route to Optically Active Pyrrolo[1,2-a]imidazoles](/thumbs/89/100111450.jpg "Cycloaddition of Homochiral Dihydroimidazoles: A 1,3-Dipolar Cycloaddition Route to Optically Active Pyrrolo[1,2-a]imidazoles")
X-Ray crystallographic data tables for paper: Supplementary Material (ESI) for Organic & Biomolecular Chemistry Cycloaddition of Homochiral Dihydroimidazoles: A 1,3-Dipolar Cycloaddition Route to Optically
2-Carboxyquinolinium-2,4,6-trinitrobenzenesulfonatequinolinium-2-carboxylate
2-Carboxyquinolinium-2,4,6-trinitrobenzenesulfonatequinolinium-2-carboxylate (1/1/1) Author Smith, Graham, Wermuth, Urs, M. White, Jonathan Published 2008 Journal Title Acta Crystallographica. Section
Supporting Information. Palladium Complexes with Bulky Diphosphine. Synthesis of (Bio-) Adipic Acid from Pentenoic. Acid Mixtures.
Supporting Information Palladium Complexes with Bulky Diphosphine Ligands as Highly Selective Catalysts for the Synthesis of (Bio-) Adipic Acid from Pentenoic Acid Mixtures. Choon Heng Low, James D. Nobbs,*
Pyrrolo[2,3-d:5,4-d']bisthiazoles: Alternate Synthetic Routes and a Comparative Study to Analogous Fused-ring Bithiophenes
![Pyrrolo[2,3-d:5,4-d']bisthiazoles: Alternate Synthetic Routes and a Comparative Study to Analogous Fused-ring Bithiophenes](/thumbs/92/108867714.jpg "Pyrrolo[2,3-d:5,4-d']bisthiazoles: Alternate Synthetic Routes and a Comparative Study to Analogous Fused-ring Bithiophenes")
SUPPORTING INFORMATION Pyrrolo[2,3-d:5,4-d']bisthiazoles: Alternate Synthetic Routes and a Comparative Study to Analogous Fused-ring Bithiophenes Eric J. Uzelac, Casey B. McCausland, and Seth C. Rasmussen*
2. Experimental Crystal data. C 22 H 29 F 3 O 5 S M r = Orthorhombic, P a = (10) Å b = (12) Å c = 27.
data reports ISSN 2056-9890 Crystal structure of 3b-acetoxyandrosta- 5,16-dien-17-yl trifluoromethanesulfonate Shengjun Zhou, a Huaqi Huang, b Ting Zhang, b Dangfeng Wang b and Rongbin Huang b * a Hangzhou
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Chlorido(chlorodiphenylphosphine-jP)- (diphenylpiperidinophosphine-jp)- (g 5 -pentamethylcyclopentadienyl)-
NH-Type of chiral Ni(II) complexes of glycine Schiff base: design, structural evaluation, reactivity and synthetic applications
Supporting Information NH-Type of chiral Ni(II) complexes of glycine Schiff base: design, structural evaluation, reactivity and synthetic applications Mackenzie Bergagnini, a Kazunobu Fukushi, b Jianlin
Supporting Information
Supporting Information Vinylogous elimination/heck coupling/allylation domino reactions: access to 2- substituted 2,3-dihydrobenzofurans and indolines Jianguo Yang, *, Hanjie Mo, Xiuxiu Jin, Dongdong Cao,
2. Experimental. 2.1. Crystal data
data reports ISSN 2056-9890 Crystal structure of N-[(morpholin-4- yl)(thiophen-2-yl)methyl]benzamide S. Arun Prabhu, a M. Suresh, b A. Abdul Jameel, c M. Syed Ali Padusha b and B. Gunasekaran d * a Department
Electronic Supplementary Information (ESI)
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Electronic Supplementary Information (ESI) Cyclopentadienyl iron dicarbonyl (CpFe(CO) 2 ) derivatives
Supporting Information
One-Pot, Three-Component Assembly of Indoloquinolines: Total Synthesis of Isocryptolepine Alexander V. Aksenov,* Dmitrii A. Aksenov, Naila A. Orazova, Nicolai A. Aksenov, Georgii D. Griaznov, Annelise
Patrycja Miszczyk, Dorota Wieczorek, Joanna Gałęzowska, Błażej Dziuk, Joanna Wietrzyk and Ewa Chmielewska. 1. Spectroscopic Data.
; doi:10.3390/molecules22020254 S1 of S23 Supplementary Materials: Reaction of 3-Amino-1,2,4-Triazole with Diethyl Phosphite and Triethyl Orthoformate: Acid-Base Properties and Antiosteoporotic Activities
chlorostibine Iou-Sheng Ke and François P. Gabbai Department of Chemistry, Texas A&M University, College Station, TX
σ-donor/acceptor confused ligands: The case of a chlorostibine Iou-Sheng Ke and François P. Gabbai Department of Chemistry, Texas A&M University, College Station, TX 77843-3255. *To whom correspondence
Supporting Information
Supporting Information 1,3,5-Triazapentadienes by Nucleophilic Addition to 1,3- and 1,4-Dinitriles - Sterically Constrained Examples by Incorporation into Cyclic Peripheries: Synthesis, Aggregation and
Nickel and Platinum PCP Pincer Complexes Incorporating an Acyclic Diaminoalkyl Central Moiety Connecting Imidazole or Pyrazole Rings
ickel and Platinum PCP Pincer Complexes Incorporating an Acyclic Diaminoalkyl Central Moiety Connecting Imidazole or Pyrazole Rings Braulio M. Puerta Lombardi, Rudy M. Braun, Chris Gendy, Chia Yun Chang,
Mouhamadou Birame Diop, a * Libasse Diop a and Allen G. Oliver b
Dimethyl N-cyanodithioiminocarbonate data reports ISSN 2414-3146 Mouhamadou Birame Diop, a * Libasse Diop a and Allen G. Oliver b a Laboratoire de Chimie Minérale et Analytique, Département de Chimie,
Supporting Information. Research Center for Marine Drugs, Department of Pharmacy, State Key Laboratory
Supporting Information Dysiherbols A C and Dysideanone E, Cytotoxic and NF-κB Inhibitory Tetracyclic Meroterpenes from a Dysidea sp. Marine Sponge Wei-Hua Jiao,, Guo-Hua Shi,, Ting-Ting Xu,, Guo-Dong Chen,
Single Crystal X-Ray Structure Determination of Compounds 8a, 8b and 11a
Single Crystal X-Ray Structure Determination of Compounds 8a, 8b and 11a General: Preliminary examination and data collection were carried out on an area detecting system (Kappa-CCD; Nonius) using graphite-monochromated
Synthesis, Crystal Structure and Supramolecular Understanding of 1,3,5-Tris(1-phenyl-1H-pyrazol-5- yl)benzenes
Supplementary information Synthesis, Crystal Structure and Supramolecular Understanding of 1,3,5-Tris(1-phenyl-1H-pyrazol-5- yl)benzenes Marcos A. P. Martins 1 *, Alexandre R. Meyer 1, Paulo R. S. Salbego
Supporting Information. Pd(0)-Catalyzed Decarboxylative Coupling and Tandem C H Arylation/Decarboxylation for the. Synthesis of Heteroaromatic Biaryls
Supporting Information Pd()-Catalyzed Decarboxylative Coupling and Tandem C H Arylation/Decarboxylation for the Synthesis of Heteroaromatic Biaryls Debkumar andi, Yang-Ming Jhou, Jhen-Yi Lee, Bing-Chiuan
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 = 91.155 (4) = 108.148 (4) = 111.344 (3) V = 894.09 (7) Å 3 Z =1 Mo K radiation = 17.13 mm 1 T = 295 K 0.41
Multifunctinality and Crystal Dynamics of Highly Stable Porous Metal-Organic Framework [Zn 4 O(NTB) 2 ]
![Multifunctinality and Crystal Dynamics of Highly Stable Porous Metal-Organic Framework [Zn 4 O(NTB) 2 ]](/thumbs/92/109256432.jpg "Multifunctinality and Crystal Dynamics of Highly Stable Porous Metal-Organic Framework [Zn 4 O(NTB) 2 ]")
Supporting Information Multifunctinality and Crystal Dynamics of Highly Stable Porous Metal-Organic Framework [Zn 4 O(NTB) 2 ] Eun Young Lee, Seung Yeon Jang, and Myunghyun Paik Suh* School of Chemistry,
Supporting Information for. Catalytic C H α-trifluoromethylation of α,β-unsaturated Carbonyl Compounds
Supporting Information for Catalytic C H α-trifluoromethylation of α,β-unsaturated Carbonyl Compounds Zhongxue Fang, a Yongquan Ning, a Pengbing Mi, a Peiqiu Liao, a Xihe Bi* a,b a Department of Chemistry,
Photo-Induced Self-Assembly of Pt(II)-Linked Rings and Cages via the Photolabilization of a Pt(II) Pyridine Bond
Photo-Induced Self-Assembly of Pt(II)-Linked Rings and Cages via the Photolabilization of a Pt(II) Pyridine Bond Ken-ichi Yamashita, Kei-ichi Sato, Masaki Kawano and Makoto Fujita* Contents; Figure S1.
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 {Bis[2-(diphenylphosphanyl)phenyl] ether-j 2 P,P 0 }(1,1 0 -dibenzyl-1h,1 0 H-4,4 0 - bi-1,2,3-triazole-j
2-(5-Bromo-1H-indol-3-yl)-4-(4-bromophenyl)-5- (4-chlorobenzoyl)-1H-pyrrole-3-carbonitrile dimethyl sulfoxide monosolvate
ISSN 2414-3146 2-(5-Bromo-1H-indol-3-yl)-4-(4-bromophenyl)-5- (4-chlorobenzoyl)-1H-pyrrole-3-carbonitrile dimethyl sulfoxide monosolvate Y. AaminaNaaz, a Jayabal Kamalraja, b G. Vimala, a Paramasivam T.
Supporting Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Supporting Information Domino reaction of cyclic sulfamidate imines with
SUPPORTING INFORMATION. Diastereoselective synthesis of nitroso acetals from (S,E)- -aminated
SUPPORTING INFORMATION for Diastereoselective synthesis of nitroso acetals from (S,E)- -aminated nitroalkenes via multicomponent [4 + 2]/[3 + 2] cycloadditions promoted by LiCl or LiClO 4 Leandro Lara
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 [l-bis(diphenylarsino)methane- 1:2j 2 As:As 0 ]nonacarbonyl- 1j 3 C,2j 3 C,3j 3 C-tricyclohexylphosphine-
ANNEXE 2 : SPECTRES DE RÉSONANCE MAGNÉTIQUE NUCLÉAIRE
ANNEXE 2 : SPECTRES DE RÉSONANCE MAGNÉTIQUE NUCLÉAIRE 175 4-Oxopentyl acetate (1-9) 27.56 17.91 63.49 39.76 29.86 22.66 2.82 2. 1.97 2.91 2.96 2.9 4. 3.98 3.96 2.47 2.44 2.42 2.7 1.95 1.86 1.84 1.82 1.79
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2008
Supporting Information Copyright Wiley-VC Verlag Gmb & Co. KGaA, 69451 Weinheim, 2008 Copper Complexes of Mono- and Ditopic [(Methylthio)methyl]borates: Missing Links and Linked Systems En Route to Copper
Electronic supplementary information (ESI) Bodipy functionalized ortho-carborane dyads for low-energy photosensitization
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2014 Electronic supplementary information (ESI) Bodipy functionalized ortho-carborane dyads
Synthesis and Biological Evaluation of Novel Acyclic and Cyclic Glyoxamide derivatives as Bacterial Quorum Sensing and Biofilm Inhibitors
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Synthesis and Biological Evaluation of Novel Acyclic and Cyclic Glyoxamide
Stereochemistry and mechanistic insight in the [2 k +2 i +2 i ] annulations of ketenes and imines
![Stereochemistry and mechanistic insight in the [2 k +2 i +2 i ] annulations of ketenes and imines](/thumbs/83/87678994.jpg "Stereochemistry and mechanistic insight in the [2 k +2 i +2 i ] annulations of ketenes and imines")
Stereochemistry and mechanistic insight in the [2 k +2 i +2 i ] annulations of ketenes and imines Zhanhui Yang, Wei He, Baoxiang Cheng and Jiaxi Xu* State Key Laboratory of Chemical Resource Engineering,
Tunable Ligand Emission of Napthylsalophen Triple-Decker Dinuclear Lanthanide (III) Sandwich Complexes
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2017 Supplemental Information Tunable Ligand Emission of Napthylsalophen Triple-Decker Dinuclear
Supporting Information for: Intramolecular Hydrogen Bonding-Assisted Cyclocondensation of. 1,2,3-Triazole Synthesis
Supporting Information for: Intramolecular Hydrogen Bonding-Assisted Cyclocondensation of α-diazoketones with Various Amines: A Strategy for Catalytic Wolff 1,2,3-Triazole Synthesis Zikun Wang, a Xihe
Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic acids with the assistance of isocyanide
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic
data reports a molecular salt Structure description
ISSN 2414-3146 N,N,N-Triethylethanaminium 5,11,17,23-tetra-tertbutyl-25-[(ethoxycarbonyl)methoxy]-26,28-dihydroxy-27-oxido-2,8,14,20-tetrathiacalix[4]arene: a molecular salt Received 14 September 2016
Elizabeth M. Horstman, a Jeffery A. Bertke, b Toby J. Woods b * and Paul J. A. Kenis a
research communications ISSN 2056-9890 Crystal structure of a 2:1 piroxicam gentisic acid co-crystal featuring neutral and zwitterionic piroxicam molecules Elizabeth M. Horstman, a Jeffery A. Bertke, b
Zebra reaction or the recipe for heterodimeric zinc complexes synthesis
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 05 Supporting Information Zebra reaction or the recipe for heterodimeric zinc complexes synthesis
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%.
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%. S1 Supplementary Figure S2. Single X-ray structure 5a at probability ellipsoids of 20%. S2 H 15 Ph Ac Ac I AcH Ph Ac
Supplementary Information. Living Ring-Opening Polymerization of Lactones by N-Heterocyclic Olefin/Al(C 6 F 5 ) 3
Supplementary Information Living Ring-Opening Polymerization of Lactones by N-Heterocyclic Olefin/Al(C 6 F 5 ) 3 Lewis Pairs: Structures of Intermediates, Kinetics, and Mechanism Qianyi Wang, Wuchao Zhao,
Free Radical Initiated Coupling Reaction of Alcohols and. Alkynes: not C-O but C-C Bond Formation. Context. General information 2. Typical procedure 2
Free Radical Initiated Coupling Reaction of Alcohols and Alkynes: not C-O but C-C Bond Formation Zhongquan Liu,* Liang Sun, Jianguo Wang, Jie Han, Yankai Zhao, Bo Zhou Institute of Organic Chemistry, Gannan
Multi odd-even effects on cell parameters, melting. points, and optical properties of chiral crystal solids. based on S-naproxen
Electronic Supplementary Material (ESI) for CrystEngComm. This journal is The Royal Society of Chemistry 2015 Supplementary Information Multi odd-even effects on cell parameters, melting points, and optical
Nitric oxide (NO) reactivity studies on mononuclear Iron(II) complexes supported by a tetradentate Schiff base Ligand
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Nitric oxide (NO) reactivity studies on mononuclear Iron(II) complexes supported by a tetradentate
Four- and Five-membered Cobaltacycles by Regioselective Cyclometalation. of Benzylsulfide Derivatives via Co(V) intermediates
Electronic Supplementary Information for Dalton Transactions This journal is The Royal Society of Chemistry 2008 Supporting Information for: Four- and Five-membered Cobaltacycles by Regioselective Cyclometalation
Table of Contents 1 Supplementary Data MCD
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2017 Supporting Information for Magnetic circular dichroism and density functional theory
Supplementary information
Electronic Supplementary Material (ESI) for MedChemComm. This journal is The Royal Society of Chemistry 2015 Supplementary information Synthesis of carboxyimidamide-substituted benzo[c][1,2,5]oxadiazoles
Supporting Information
Supporting Information for AgOTf-catalyzed one-pot reactions of 2-alkynylbenzaldoximes with α,β-unsaturated carbonyl compounds Qiuping Ding 1, Dan Wang 1, Puying Luo* 2, Meiling Liu 1, Shouzhi Pu* 3 and
College of Life Science, Dalian Nationalities University, Dalian , PR China.
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2018 Postsynthetic modification
metal-organic compounds
metal-organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Bis(tetrabutylammonium) bis(3,4,5- trioxocyclopent-1-ene-1,2-dithiolatoj 2 S,S 0 )cadmate(ii) 0.25-hydrate
Electronic Supplementary Information (ESI)
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2016 Electronic Supplementary Information (ESI) CPh 3 as a functional group in P-heterocyclic
Supporting Information. for
Supporting Information for A general synthetic route to [Cu(X)(NHC)] (NHC = N- heterocyclic carbene, X =Cl, Br, I) complexes Orlando Santoro, Alba Collado, Alexandra M. Z. Slawin, Steven P. Nolan and Catherine
Supporting Information
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 2016 Supporting Information Abnormal N-Heterocyclic Carbene Based Nickel Complex for Catalytic
Electronic Supporting Information. 3-Aminothiophenecarboxylic acid (3-Atc)-induced folding in peptides
Electronic Supplementary Material (ESI for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 2016 Electronic Supporting Information
Metal-free Oxidative Coupling of Amines with Sodium Sulfinates: A Mild Access to Sulfonamides
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting information for Metal-free Oxidative Coupling of Amines with Sodium Sulfinates:
organic compounds 5-Chloro-3-methyl-4-[3-(4-nitro- phenyl)-4,5-dihydro-1h-pyrazol-5-yl]- 1-phenyl-1H-pyrazole: a chain of fused hydrogen-bonded rings
![organic compounds 5-Chloro-3-methyl-4-[3-(4-nitro- phenyl)-4,5-dihydro-1h-pyrazol-5-yl]- 1-phenyl-1H-pyrazole: a chain of fused hydrogen-bonded rings](/thumbs/82/86135443.jpg "organic compounds 5-Chloro-3-methyl-4-[3-(4-nitro- phenyl)-4,5-dihydro-1h-pyrazol-5-yl]- 1-phenyl-1H-pyrazole: a chain of fused hydrogen-bonded rings")
organic compounds Acta Crystallographica Section C Crystal Structure Communications ISSN 0108-2701 5-Chloro-3-methyl-4-[3-(4-nitro- phenyl)-4,5-dihydro-1h-pyrazol-5-yl]- 1-phenyl-1H-pyrazole: a chain of
C H Activation of Cp* Ligand Coordinated to Ruthenium. Center: Synthesis and Reactivity of a Thiolate-Bridged
Supporting Information C H Activation of Cp* Ligand Coordinated to Ruthenium Center: Synthesis and Reactivity of a Thiolate-Bridged Diruthenium Complex Featuring Fulvene-like Cp* Ligand Xiaoxiao Ji, Dawei
Supporting Information. Asymmetric Binary-acid Catalysis with Chiral. Phosphoric Acid and MgF 2 : Catalytic
Supporting Information Asymmetric Binary-acid Catalysis with Chiral Phosphoric Acid and MgF 2 : Catalytic Enantioselective Friedel-Crafts Reactions of β,γ- Unsaturated-α-Ketoesters Jian Lv, Xin Li, Long
Copper-Catalyzed Oxidative Dehydrogenative N-N Bond. Formation for the Synthesis of N,N -Diarylindazol-3-ones
Electronic Supplementary Material (ESI) for Organic Chemistry Frontiers. This journal is the Partner Organisations 2016 Supporting information Copper-Catalyzed Oxidative Dehydrogenative - Bond Formation
Supporting Information
Supporting Information Wiley-VC 007 9 Weinheim, Germany ew ear Infrared Dyes and Fluorophores Based on Diketopyrrolopyrroles Dipl.-Chem. Georg M. Fischer, Dipl.-Chem. Andreas P. Ehlers, Prof. Dr. Andreas
Electronic Supplementary Information. Carbon dioxide as a reversible amine-protecting
Electronic Supplementary Information Carbon dioxide as a reversible amine-protecting agent in selective Michael additions and acylations Annelies Peeters, Rob Ameloot and Dirk E. De Vos * Centre for Surface
Palladium-Catalyzed Direct ortho-sulfonylation of. Azobenzenes with Arylsulfonyl Chlorides via C H. Table of Contents
Electronic upplementary Material (EI) for RC Advances. This journal is The Royal ociety of Chemistry 205 upporting Information Palladium-Catalyzed Direct ortho-ulfonylation of Azobenzenes with Arylsulfonyl
Synthesis and effects of oxadiazole derivatives on tyrosinase activity and SK-MEL-28 malignant melanoma cells
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 06 Synthesis and effects of oxadiazole derivatives on tyrosinase activity and human SK-MEL-8 malignant
Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3
Supporting Information Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3 Shohei Shimokawa, Yuhsuke Kawagoe, Katsuhiko Moriyama, Hideo Togo* Graduate
Supporting information. An unusual bifunctional Tb-MOF for highly sensing of Ba 2+ ions and remarkable selectivities of CO 2 /N 2 and CO 2 /CH 4
Electronic Supplementary Material (ESI) for Journal of Materials Chemistry A. This journal is The Royal Society of Chemistry 2015 Supporting information An unusual bifunctional Tb-MOF for highly sensing
A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Bloco A, Cidade Universitária, Ilha do Fundão, Rio de Janeiro, RJ, Brazil. Contents Pages
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2016 Supporting Information Copper(II) Catalyzed Synthesis of Novel Helical
organic compounds 78 HeÂctor Novoa de Armas et al. C 24 H 36 O 6 Acta Cryst. (2000). C56, 78±79 Comment Experimental
organic compounds Acta Crystallographica Section C Crystal Structure Communications ISSN 0108-2701 In connection with our studies on the synthesis and characterization of bioactive steroids, we determined
Synthesis, Characterization, and Computational Study of Three-Coordinate SNS-Copper(I) Complexes Based on Bis-Thione Precursors
For Synthesis, Characterization, and Computational Study of Three-Coordinate SNS-Copper(I) Complexes Based on Bis-Thione Precursors John R. Miecznikowski a *; Matthew A. Lynn b ; Jerry P. Jasinski c ;
Experimental. Crystal data. C 13 H 17 N 3 O 2 M r = Monoclinic, Cc a = (4) Å b = (4) Å c = (3) Å = 111.
Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 4-[2-(4-Hydroxyphenyl)ethyl]-3-propyl- 1H-1,2,4-triazol-5(4H)-one Experimental Crystal data C 13 H 17 N 3 O 2 M r = 247.30 Monoclinic,
Supporting Information. Experimental section
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting Information Experimental section General. Proton nuclear magnetic resonance ( 1
Experimental. Crystal data
organic compounds Acta Crystallographica Section E Structure Reports Online ISSN 1600-5368 Enrofloxacin hydrochloride dihydrate Jorge E. Miranda-Calderón, a Lilia Gutiérrez, a Marcos Flores-Alamo, b Ponciano
Supporting Information. Generation Response. Physics & Chemistry of CAS, 40-1 South Beijing Road, Urumqi , China. China , USA
Supporting Information Pb 3 B 6 O 11 F 2 : A First Noncentrocentric Lead Fluoroborate with Large Second Harmonic Generation Response Hongyi Li, a Hongping Wu, a * Xin Su, a Hongwei Yu, a,b Shilie Pan,
Supporting Information
Supporting Information Montmorillonite KSF-Catalyzed One-pot, Three-component, Aza-Diels- Alder Reactions of Methylenecyclopropanes With Arylaldehydes and Aromatic Amines Li-Xiong Shao and Min Shi* General
Supporting Information. A catalyst-free multicomponent domino sequence for the. diastereoselective synthesis of (E)-3-[2-arylcarbonyl-3-
Supporting Information for A catalyst-free multicomponent domino sequence for the diastereoselective synthesis of (E)-3-[2-arylcarbonyl-3- (arylamino)allyl]chromen-4-ones Pitchaimani Prasanna 1, Pethaiah
Controlling Growth of Molecular Crystal Aggregates with Distinct Linear and Nonlinear Optical Properties
Supporting Information Controlling Growth of Molecular Crystal Aggregates with Distinct Linear and Nonlinear Optical Properties Yusen Luo,,,# Chunqing Yuan,,# Jialiang Xu*, Yongjun Li*, Huibiao Liu, Sergey
(M = Mn, Fe, Co, Ni, Cu and Zn)----Mimicking the M II - Substituted Quercetin 2,3-Dioxygenase
Electronic Supplementary Material (ESI) for Dalton Transactions. This journal is The Royal Society of Chemistry 215 Supplementary material Catalytic Dioxygenation of Flavonol by M II Complexes (M = Mn,
Synthesis of novel 1,2,3-triazolyl derivatives of pregnane, androstane and D-homoandrostane. Tandem Click reaction/cu-catalyzed D-homo rearrangement
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information Synthesis of novel 1,2,3-triazolyl derivatives of
SUPPORTING INFORMATION. Pyramidanes: The Covalent Form of the Ionic Compounds
SUPPORTING INFORMATION Pyramidanes: The Covalent Form of the Ionic Compounds Vladimir Ya. Lee, 1 * Olga A. Gapurenko, 2 Yuki Ito, 1 Takahiko Meguro, 1 Haruka Sugasawa, 1 Akira Sekiguchi, 1 *, Ruslan M.
Supporting Information
Supporting Information Lewis acid catalyzed ring-opening reactions of methylenecyclopropanes with diphenylphosphine oxide in the presence of sulfur or selenium Min Shi,* Min Jiang and Le-Ping Liu State
Supporting Information
Supporting Information Transition-metal-free Ring Expansion Reactions of Indene-1,3-dione: Synthesis of Functionalized Benzoannulated Seven-Membered Ring Compounds Qiyi Yao, Lingkai Kong, Mengdan Wang,