DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients 5 45 4 35 3 25 2 15 1 5 Berlin Veg Bloom N P K Ca Mg S
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients 5 45 4 35 3 25 2 15 1 5 Hash Bud Veg Bloom N P K Ca Mg S
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients 5 45 4 35 3 25 2 15 1 5 White Rhino Veg Bloom N P K Ca Mg S
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients 3 25 2 15 1 5 Micro Nutrient Analysis Veg Bloom Fe Mn Zn Cu B Mo
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 COMMENTS: Total Metals, Samples Digested 22 Nov 2 METHODS: Standard Methods for the Examination of Water and Wastewater Client ID: HB Finish (Reg) HB 6 Jan 21 HB 5 Jan 15 HB 4 Jan 8 HB 3 Reg Jan 1 BCRI ID#: DL 23138 231381 231382 231383 231384 Prep ID: CAN 8b CAN 9b CAN 1b CAN 11b CAN 12b (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 <.3 <.3 Al Aluminum 1 5 7 9 6 5 As Arsenic 1 <1 <1 <1 <1 <1 B Boron 3 42 43 53 57 61 Ba Barium.5.93.9 1.17 1.42 1.81 Be Beryllium.5 <.5 <.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 <3 <3 Ca Calcium 1 15 985 18 145 149 Cd Cadmium.5.8.8.6.7.7 Co Cobalt.3 <.3 <.3 <.3 <.3 <.3 Cr Chromium.3.7.6.6.5.7 Cu Copper.5 5 3.5 3.3 3.7 5.7 Fe Iron 1 292 331 31 235 254 K Potassium 3 365 462 558 445 455 Li Lithium.5 <.5 <.5 <.5.7 <.5 Mg Magnesium 1 67 622 497 525 562 Mn Manganese.5 262 234 211 232 226 Mo Molybdenum.5 1.2.9.8.8.7 Na Sodium 3 42 61 147 116 92 Ni Nickel.3 <.3 <.3 <.3.3.3 P Phosphorous 2 16 113 112 961 15 Pb Lead 1 <1 <1 <1 <1 <1 S Sulfur 1 383 397 42 372 414 Sb Antimony 1 <1 <1 <1 <1 <1 Se Selenium 1 <1 <1 <1 <1 <1 Si Silicon 3 354 317 34 355 367 Sn Tin 1 2 1 <1 <1 <1 Sr Strontium.5 4.6 37.7 35.2 45.9 44.4 Ti Titanium.5 <.5 <.5 <.5 <.5 <.5 Tl Thallium 1 <1 <1 <1 <1 <1 U Uranium 3 <3 <3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 <.5 <.5 Zn Zinc.3 1 15 9.2 79.7 9.9 Page 1 of 4
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Berlin 7 Jan 29 Client ID: HB 2 Dec 25 HB 1 Dec 18 HB Veg (Day 49) Berlin 6 Jan 21 BCRI ID#: DL 231385 231386 231387 231396 231388 Prep ID: CAN 13b CAN 14b CAN 15b CAN 15b CAN 16b (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 <.3 <.3 Al Aluminum 1 4 17 28 28 4.5 As Arsenic 1 <1 <1 <1 <1 <1 B Boron 3 51 46 46 47 46 Ba Barium.5 1.69 3.39 2.91 2.94.84 Be Beryllium.5 <.5 <.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 <3 <3 Ca Calcium 1 136 186 182 185 126 Cd Cadmium.5 <.5 <.5.7.8.6 Co Cobalt.3 <.3 <.3 <.3 <.3 <.3 Cr Chromium.3.4.8.7.6.8 Cu Copper.5 4.2 4.2 4.5 4.8 6.2 Fe Iron 1 162 124 462 469 158 K Potassium 3 359 349 345 35 439 Li Lithium.5 <.5 1.8.74.83 <.5 Mg Magnesium 1 466 518 54 549 64 Mn Manganese.5 169 155 287 292 25 Mo Molybdenum.5.8.8 <.5 <.5 1.1 Na Sodium 3 6 242 59 65 3 Ni Nickel.3 <.3.4 <.3 <.3 <.3 P Phosphorous 2 83 724 525 53 143 Pb Lead 1 <1 <1 <1 <1 <1 S Sulfur 1 355 366 358 357 472 Sb Antimony 1 <1 <1 <1 <1 <1 Se Selenium 1 <1 <1 <1 <1 <1 Si Silicon 3 379 362 368 458 24 Sn Tin 1 <1 <1 <1 <1 <1 Sr Strontium.5 35.1 53.7 57.4 57.7 39.9 Ti Titanium.5 <.5 <.5 1.5 1.6 <.5 Tl Thallium 1 <1 <1 <1 <1 <1 U Uranium 3 <3 <3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 <.5 <.5 Zn Zinc.3 74.8 66.2 65.7 67.2 141 Page 2 of 4
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Berlin 4 Jan 8 Client ID: Berlin 6 Jan 21 Berlin 5 Jan 15 (Reg) BCRI ID#: DL 231389 23139 231391 Prep ID: CAN 17b CAN 18b CAN 19b (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 Al Aluminum 1 9 8 2 As Arsenic 1 <1 <1 <1 B Boron 3 42 49 7 Ba Barium.5.7.92 3.35 Be Beryllium.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 Ca Calcium 1 688 899 25 Cd Cadmium.5 <.5 <.5 <.5 Co Cobalt.3 <.3 <.3 <.3 Cr Chromium.3 2.8.7.8 Cu Copper.5 5.5 4.3 6.3 Fe Iron 1 149 116 178 K Potassium 3 473 398 476 Li Lithium.5 <.5 <.5.6 Mg Magnesium 1 53 44 52 Mn Manganese.5 153 145 199 Mo Molybdenum.5 1.2 1 1.7 Na Sodium 3 57 72 112 Ni Nickel.3 1.4 <.3.4 P Phosphorous 2 122 944 917 Pb Lead 1 <1 <1 <1 S Sulfur 1 399 385 474 Sb Antimony 1 <1 <1 <1 Se Selenium 1 <1 <1 <1 Si Silicon 3 227 234 44 Sn Tin 1 <1 <1 2 Sr Strontium.5 39 42 66.8 Ti Titanium.5 <.5 <.5 <.5 Tl Thallium 1 <1 <1 <1 U Uranium 3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 Zn Zinc.3 92.1 73.4 99.5 Page 3 of 4
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients COMMENTS: Total Metals, Samples Digested February 23 METHODS: Standard Methods for the Examination of Water and Wastewater White Rhino Client ID: Berlin 3 Jan 1 Berlin 2 Dec 25 Berlin 1 Dec 18 Berlin Veg 56 Days BCRI ID#: DL 231397 231398 231399 2314 23141 Prep ID: CAN 2b CAN 21b CAN 22b CAN 23b CAN 24b (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 <.3 <.3 Al Aluminum 1 7 4 4 7 7.4 As Arsenic 1 <1 <1 <1 <1 <1 B Boron 3 46 44 47 46 36 Ba Barium.5 1.62 2.14 2.25 3.1.36 Be Beryllium.5 <.5 <.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 <3 <3 Ca Calcium 1 144 175 193 23 565 Cd Cadmium.5 <.5 <.5 <.5 <.5 <.5 Co Cobalt.3 <.3 <.3 <.3 <.3 <.3 Cr Chromium.3.5.3.4 <.3.9 Cu Copper.5 5.4 5 4.6 3.5 4.3 Fe Iron 1 149 95 122 88 145 K Potassium 3 46 413 36 261 457 Li Lithium.5 <.5 <.5.7 1 <.5 Mg Magnesium 1 454 318 42 311 574 Mn Manganese.5 153 77 148 78.2 11 Mo Molybdenum.5 1.2 1 1.3.9 1 Na Sodium 3 43 38 55 32 41 Ni Nickel.3 <.3 <.3 <.3 <.3.3 P Phosphorous 2 872 747 71 475 19 Pb Lead 1 <1 <1 <1 <1 <1 S Sulfur 1 397 366 383 319 45 Sb Antimony 1 <1 <1 <1 <1 <1 Se Selenium 1 <1 <1 <1 <1 <1 Si Silicon 3 242 15 298 25 12 Sn Tin 1 2 2 2 1 1 Sr Strontium.5 46.4 24.9 48.8 29.2 32.7 Ti Titanium.5 <.5 <.5 <.5 <.5 <.5 Tl Thallium 1 <1 <1 <1 <1 <1 U Uranium 3 <3 <3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 <.5 <.5 Zn Zinc.3 75.3 62.5 83 6.1 72.3 Page 1 of 4
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients White Rhino 7 White Rhino 6 White Rhino 5 White Rhino 4 White Rhino 3 Client ID: (49 days Reg) Jan 21 Jan 15 Jan 8 Jan 1 (Reg) BCRI ID#: DL 23142 23143 23144 23145 23146 Prep ID: CAN 25b CAN 26b CAN 27b CAN 28b CAN 29b (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 <.3 <.3 Al Aluminum 1 3 3 6 5 15 As Arsenic 1 <1 <1 <1 <1 <1 B Boron 3 33 37 57 52 65 Ba Barium.5.82.53.69 1.14 2.5 Be Beryllium.5 <.5 <.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 <3 <3 Ca Calcium 1 54 646 996 119 21 Cd Cadmium.5 <.5 <.5 <.5 <.5 <.5 Co Cobalt.3 <.3 <.3 <.3 <.3 <.3 Cr Chromium.3.4.5.8.5.8 Cu Copper.5 3.8 4.5 4.4 4.3 5.4 Fe Iron 1 152 179 182 251 397 K Potassium 3 464 452 438 485 481 Li Lithium.5 <.5.51 <.5 <.5.9 Mg Magnesium 1 553 555 628 53 647 Mn Manganese.5 97 19 123 139 211 Mo Molybdenum.5.8 1.1.9 1.4 1.1 Na Sodium 3 33 52 47 46 7 Ni Nickel.3 <.3 <.3.3 <.3.5 P Phosphorous 2 12 17 13 888 834 Pb Lead 1 <1 <1 <1 <1 <1 S Sulfur 1 363 45 43 365 434 Sb Antimony 1 <1 <1 <1 <1 <1 Se Selenium 1 <1 <1 <1 <1 <1 Si Silicon 3 162 79 245 12 284 Sn Tin 1 1 1 1 1 <1 Sr Strontium.5 34.3 38.9 47.7 46.2 64.1 Ti Titanium.5 <.5 <.5 1.8 <.5 2 Tl Thallium 1 <1 <1 <1 <1 <1 U Uranium 3 <3 <3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 <.5 <.5 Zn Zinc.3 67.8 77.1 76.5 72.6 12 Page 2 of 4
DATE of Analysis: 5 March 23 BC RESEARCH INC DATE of Report: 7 March 23 365 Westbrook Mall PROJECT No.: 8-3-124 Vancouver, B.C. APPROVED BY: Anna Becalska TEL: (64) 224-4331 FAX: (64) 224-54 Advanced Nutrients White Rhino 2 White Rhino 1 White Rhino White Rhino Client ID: Dec 25 Dec 18 Veg Veg BCRI ID#: DL 23147 23148 23149 23141 Prep ID: CAN 3b CAN 31b CAN 32b CAN 32b (mg/kg) (mg/kg) (mg/kg) (mg/kg) (mg/kg) Ag Silver.3 <.3 <.3 <.3 <.3 Al Aluminum 1 5 4 15 13 As Arsenic 1 <1 <1 <1 <1 B Boron 3 43 46 74 74 Ba Barium.5 1.33 1.56 2.37 2.3 Be Beryllium.5 <.5 <.5 <.5 <.5 Bi Bismuth 3 <3 <3 <3 <3 Ca Calcium 1 137 153 228 225 Cd Cadmium.5 <.5 <.5 <.5 <.5 Co Cobalt.3 <.3 <.3 <.3 <.3 Cr Chromium.3.9.5.5.5 Cu Copper.5 4.6 4.9 6.2 6.1 Fe Iron 1 29 295 223 217 K Potassium 3 388 395 312 31 Li Lithium.5.5.8 1.5 1.4 Mg Magnesium 1 417 418 52 56 Mn Manganese.5 156 173 24 23 Mo Molybdenum.5.9.8.7.9 Na Sodium 3 38 49 6 46 Ni Nickel.3 <.3 <.3 <.3 <.3 P Phosphorous 2 642 686 657 649 Pb Lead 1 <1 <1 <1 <1 S Sulfur 1 321 353 5 489 Sb Antimony 1 <1 <1 <1 <1 Se Selenium 1 <1 <1 <1 <1 Si Silicon 3 84 219 323 99 Sn Tin 1 <1 4 2 <1 Sr Strontium.5 43.4 44.3 59.9 58.9 Ti Titanium.5 <.5 <.5 <.5 <.5 Tl Thallium 1 <1 <1 <1 <1 U Uranium 3 <3 <3 <3 <3 V Vanadium.5 <.5 <.5 <.5 <.5 Zn Zinc.3 72.2 9.5 136 137 Page 3 of 4
1471 Palmberg Rd. Richmond, BC, V6W 1C5 Advanced Nutrients 19-3163 Wheel Ave. Abbotsford, B.C. V2T 6H1 Attention: Michael November 28, 23 Certificate of Analysis P.O. 11223a Data Summary Advanced Nutrients Tester Northern Lights #1 CODE SAMPLE DESCRIPTION CBD % CBN % ^9-THC % THC-A % TOTAL THC % AN-1 week 1 vegetive.1..1 1.2 1.3 AN-2 week 1 flower.1..1.9 1. AN-3 week 2 flower.1..2 1. 1.2 AN-4 week 3 flower.1.1.1 2.4 2.5 AN-5 week 4 flower.5.1.1 5.2 5.3 AN-6 week 5 flower.6.1 1.2 14.5 14.5 AN-7 week 6 flower.7 1..3 18.3 18.6 AN-8 week 7 flower 1. 1.4.3 22.6 22.9 BHT listed in the chromatograms is an antioxidant added to one of the solvents and is irrelevant to the results. CBD is a total of CBDA and CBD thus total CBD potential. Thank you for using Hedron A. Paul Hornby, Ph.D. Laboratory Manager
Data File C:\HPCHEM\1\DATA\MJ-1129\-11.D Sample Name: NL week 1 veg Injection Date : 11/28/3 5:9:4 PM Seq. Line : 1 Sample Name : NL week 1 veg Vial : Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 5:8:4 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 5:5:8 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\-11.D) Norm. 125 1 75 5 25.548 3.35 1.874 2.382 2.673 2.911 3.84 4.98 4.53 4.748 9.94 - CBD 9.617 - CBDA 13.332 - CBN Area: 13.238 16.714 - BHT 21.18 - ^9-THC 27.456 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.94 1 PBA 53.96772 2.61517e-5 2.82269e-2 CBD 9.617 1 VBA 7.14821 2.56423e-5 3.59753e-2 CBDA 13.332 1 MM 13.2368 2.56423e-5 5.29443e-2 CBN 16.714 1 BBA 2615.8569 1.e-8 5.2317e-4 BHT 21.18 1 PBA 243.8828 2.56423e-5 1.2573e-1 ^9-THC 27.456 1 BBA 245.598 2.56423e-5 1.23343 THC-A Totals: 1.47617 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\1-21.D Sample Name: NL week 1 flower Injection Date : 11/28/3 12:2:46 PM Seq. Line : 2 Sample Name : NL week 1 flower Vial : 1 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 12:2:48 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:21:4 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\1-21.D) Norm. 1 5.248 2.327 3.295 2.625 2.87 3.791 4.285 4.725 9.3 - CBD 9.539 - CBDA 13.243 - CBN Area: 57.88 16.58 - BHT 2.824 - ^9-THC 27.2 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.3 1 PBA 31.92193 2.61517e-5 1.66962e-2 CBD 9.539 1 VBA 58.31347 2.56423e-5 2.9959e-2 CBDA 13.243 1 MM 57.877 2.56423e-5 2.96429e-2 CBN 16.58 1 BBA 2615.1126 1.e-8 5.2322e-4 BHT 2.824 1 PBA 246.48412 2.56423e-5 1.2649e-1 ^9-THC 27.2 1 BBA 1844.427 2.56423e-5 9.4599e-1 THC-A Totals: 1.1499 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\2-31.D Sample Name: NL week 2 flower Injection Date : 11/28/3 1:2:33 PM Seq. Line : 3 Sample Name : NL week 2 flower Vial : 2 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 1::57 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\2-31.D) Norm. 1 5 1.946 2.386 2.114 3.298 2.754 2.89 3.793 4.729 5.169 9.45 - CBD 9.542 - CBDA 13.28 - CBN 16.621 - BHT Area: 15.58465 2.869 - ^9-THC 27.254 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.45 1 BBA 2.8835 2.61517e- 1.9225e-2 CBD 9.542 1 PBA 13.38315 2.56423e- 5 6.68666e-2 CBDA 13.28 1 MM 15.58465 2.56423e- 5 7.99254e-3 CBN 16.621 1 BBA 2573.67944 1.e- 5 5.14736e-4 BHT 2.869 1 PBA 457.8468 2.56423e- 8 2.3485e-1 ^9-THC 27.254 1 BBA 228.7916 2.56423e- 5 1.446 THC-A 5 Totals: 1.36156 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\3-41.D Sample Name: NL week 3 flower Injection Date : 11/28/3 1:42:24 PM Seq. Line : 4 Sample Name : NL week 3 flower Vial : 3 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 1:41:46 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\3-41.D) Norm. 1 5 3.299 2.4 2.327 2.651 2.94 3.798 4.294 4.734 9.61 - CBD 9.565 - CBDA 13.256 - CBN 14.95 16.638 - BHT 2.881 - ^9-THC 27.221 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.61 1 PBA 31.12697 2.61517e-5 1.6285e-2 CBD 9.565 1 VBA 194.5293 2.56423e-5 9.9752e-2 CBDA 13.256 1 BBA 11.19268 2.56423e-5 5.18963e-2 CBN 16.638 1 BBA 2492.9659 1.e-8 4.98593e-4 BHT 2.881 1 PBA 23.6618 2.56423e-5 1.17989e-1 ^9-THC 27.221 1 BBA 464.7827 2.56423e-5 2.36155 THC-A Totals: 2.64796 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\4-51.D Sample Name: NL week 4 flower Injection Date : 11/28/3 2:23:13 PM Seq. Line : 5 Sample Name : NL week 4 flower Vial : 4 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 2:22:36 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. Norm. 2 1 DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\4-51.D) 2.4 2.327 2.651 2.94 2.874 3.35 3.66 4.298 4.738 5.189 5.71 9.85 - CBD 9.569 - CBDA 1.39 12.995 13.291 - CBN 14.842 16.638 - BHT 2.964 - ^9-THC 27.33 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.85 1 PBA 34.66558 2.61517e-5 1.81313e-2 CBD 9.569 1 VBA 962.583 2.56423e-5 4.93619e-1 CBDA 13.291 1 VBA 23.5376 2.56423e-5 1.17982e-1 CBN 16.676 1 BBA 2649.5127 1.e-8 5.2981e-4 BHT 2.964 1 PBA 248.53271 2.56423e-5 1.27459e-1 ^9-THC 27.33 1 BBA 1.1863e4 2.56423e-5 5.22399 THC-A Totals: 5.98171 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\5-61.D Sample Name: NL week 5 flower Injection Date : 11/28/3 3:4:1 PM Seq. Line : 6 Sample Name : NL week 5 flower Vial : 5 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 3:3:25 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\5-61.D) Norm. 6 4 2 1.852 1.926 2.186 2.681 2.357 2.747 3.2 3.895 3.375 4.655 4.212 4.743 5.178 5.359 5.974 5.763 6.912 7.48 7.856 9.99 - CBD 9.586 - CBDA 1.396 11.7 11.747 13.12 13.34 - CBN 14.963 16.682 - BHT 19.668 2.986 - ^9-THC 27.337 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.99 1 PB 74.37617 2.61517e-5 3.8912e-2 CBD 9.586 1 VBA 1248.97961 2.56423e-5 6.4535e-1 CBDA 13.34 1 VBA 1832.7853 2.56423e-5 9.39938e-1 CBN 16.682 1 BBA 281.5731 1.e-8 5.6314e-4 BHT 2.986 1 PBA 2264.62964 2.56423e-5 1.16141 ^9-THC 27.337 1 BBA 2.81953e4 2.56423e-5 14.45985 THC-A Totals: 17.24119 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\MJ-1129\6-71.D Sample Name: NL week 6 flower Injection Date : 11/28/3 3:44:51 PM Seq. Line : 7 Sample Name : NL week 6 flower Vial : 6 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:24:33 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (MJ-1129\6-71.D) Norm. 8 6 4 2 2.38 2.126 2.852 3.98 2.681 2.567 3.569 3.291 3.621 4.37 4.73 5.19 5.77 9.83 - CBD 9.569 - CBDA 1.372 12.866 13.285 - CBN 14.936 16.665 - BHT 2.986 - ^9-THC 27.286 - THC-A 5 1 15 2 25 3 35 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.83 1 PBA 72.2349 2.61517e-5 3.7789e-2 CBD 9.569 1 VBA 1376.2496 2.56423e-5 7.5782e-1 CBDA 13.285 1 VBA 1749.7477 2.56423e-5 8.97352e-1 CBN 16.665 1 BBA 264.76562 1.e-8 5.2953e-4 BHT 2.968 1 PBA 674.85474 2.56423e-5 3.4697e-1 ^9-THC 27.286 1 BBA 3.56347e4 2.56423e-5 18.27515 THC-A Totals: 2.26268 Results obtained with enhanced integrator! *** End of Report ***
Data File C:\HPCHEM\1\DATA\SNAPSHOT.D Sample Name: NL week 7 flower Injection Date : 11/28/3 4:12:28 PM Seq. Line : 8 Sample Name : NL week 7 flower Vial : 7 Acq. Operator : Felipe Inj : 1 Inj Volume : 5 μl Acq. Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:31:52 PM by Felipe Analysis Method : C:\HPCHEM\1\METHODS\MJ-1A.M Last changed : 11/28/3 4:33:21 PM by Felipe Method for Cannabinoid Analysis: New Zorbax SBC18 Donated by Tom T. Isocratic. Detection by Diode Array at 219 nm. DAD1 A, Sig=219,4 Ref=45,8 (SNAPSHOT.D) Norm. 1 75 5 25 1.871 2.87 2.28 2.783 2.58 2.988 3.3 3.824 4.32 4.721 5.192 5.78 5.963 9.77 - CBD 9.56 - CBDA 1.372 12.977 13.279 - CBN 14.912 16.654 - BHT 2.81 2.942 - ^9-THC 27.21 - THC-A 5 1 15 2 25 min External Standard Report Sorted By : Retention Time Calib. Data Modified : 11/28/3 12:9:12 PM Multiplier :.2 Dilution : 1. Signal 1: DAD1 A, Sig=219,4 Ref=45,8 RetTime Sig Type Area Amt/Area Amount Grp Name [min] [mau*s] [%] --------- -- ------ ---------- ---------- ---------- -- -------------- 9.77 1 PB 95.52151 2.61517e-5 4.9961e-2 CBD 9.56 1 VBA 1924.84973 2.56423e-5 9.87153e-1 CBDA 13.279 1 VBA 273.9659 2.56423e-5 1.457 CBN 16.654 1 BBA 258.7593 1.e-8 5.16152e-4 BHT 2.942 1 VBA 485.39163 2.56423e-5 2.48932e-1 ^9-THC 27.21 1 BBA 4.4752e4 2.56423e-5 22.6383 THC-A Totals: 25.2996 Results obtained with enhanced integrator! *** End of Report ***