Current Situation of Research on Phthalic Acid Esters Plasticizers in Food Contact Plant Fiber Materials. ZHANG Qian. PAEs.

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361004 Phthalic Acid Easters PAEs PAEs TS207 TS761. 7 A DOI 10. 11980 /j. issn. 0254-508X. 2017. 05.

1 Phthalic Acid Easters PAEs PAEs TS207 TS A DOI /j. issn X Current Situation of Research on Phthalic Acid Esters Plasticizers in Food Contact Plant Fiber Materials ZHANG Qian Xiamen Products Quality Supervision & Inspection Institute Xiamen Fujian Province zhangqian@ xmzjy. org Abstract The literatures in recent years about phthalic acid easters PAEs plasticizers in food contact paper materials were introduced from two aspects migration test condition and detection methods. Proper migration testing condition and detection methods with high sensitivity have been the focused points of domestic and overseas scholars but still need to be further studied. Meanwhile the published research works proved the existence of PAEs plasticizers in paper materials harm to consumers it was an early warning signal for paper material manufacturers it also proved a reference for drafting the regulation and standards about specific migration limit and detection method of PAEs plasticizers of food contact paper materials including paper packaging materials paper container and paper towel in China. Key words paper packaging materials plasticizers phthalic acid esters migration test detection methods PAEs GB PAEs 6 PAEs 2-3 Phthalic PAEs Acid Easters PAEs 80% 4 DMP DBP 2-DEHP FJQI

2 PAEs 15 PAEs 16 5 PAEs Tenax PAEs 17 PAEs Tenax 1 18 PAEs Tenax 25 EN Tenax MPPO 7 DIBP % ~ 80% 10 / PAEs % 4% 4 PVC PAEs % 10% % PAEs PAEs 10 PAEs Park 11 7 PAEs 4% 20% 50% PAEs 2- DEHP 12 2 Tenax PAEs PAEs Porapak PAEs PAEs - GC-MS 54 China Pulp & Paper Vol. 36 No

3 0. 1 ~ 40 mg /kg 0. 1 mg /kg 34 GC-MS J ~ 3. 5 μg /kg 3. 1 ~ 12 μg /kg J. DMP GC-MS PAEs 28 PAEs GC-MS PAEs Makkliang 29 PAEs - - PAEs 3 PAEs PAEs / 10 PAEs PAEs 0. 1 mg /kg 30 5 PAEs PAEs ~ mg /kg GB /T PAEs GC-MS 31 PAEs mg /kg GC-MS PAEs Bononi 32 - DIBP 0. 2 ~ 20 μg /L GC-MS PAEs ~ 0. 2 mg /kg GC-MS 3 PAEs 1 Xu Jieling Wang Bo Xu Sizhao et al. Analysis of the harmful substances in paper-made food packaging materials J. Modern Food Science and Technology Yu Li Kuang Hua Xu Liguang et al. Residual contaminant analysis in paper packaging of food J. Packaging Engineering Yue Qingqing. Harmful substance in paper packaging material and its status of migration study J. East China Pulp & Paper Industry

4 J Xiang Bin. Analysis of plasticizers in food packaging J. China Packaging plasticizer J. Modern Chemical Industry J J GB Hygienic standards for uses of additives in food containers and packaging materials S. GB S. Science and Technology EU No 10 /2011 Plastic materials and articles intended to come into contact with food S. 8 EN Paper and board intended to come into contact with foodstuffs-conditions for determination of migration from paper and board using modified polyphenyleneoxide mppo as asimulant S. 9 Cao Xiaomei Wu Xiaoyan Li Hui et al. Determination of phthalate esters in plastic food packing materials by solid phase extraction-gas chromatography J. Food Science Progress of Baking Paper J. China Pulp & Paper J J 10 Yang Bofeng Tang Zhixu Gao Xin et al. Determination of phthalic acid esters released from food paper packaging materials by high performance liquid chromatography J. Journal of Instrumental A- nalysis J J Park Y N Choi M S Rehman S U et al. Simultaneous GC-MS determination of seven phthalates in total and migrated portions of paper cups J. Environmental Science and Pollution Research Triantafyllou V I Akrida-Demertzi K Demertzis P G. A study on the migration of organic pollutants from recycled paperboard packaging materials to solid food matrices J. Food Chemistry Xue Meigui Wang Shuangfei. Selection of solid food simulants formigration test from paper foodpackaging materials J. Packaging Engineering Sibali Linda L Okonkwo Jonathan O McCindle R I. Determination J of selected phthalate esters compounds in water and sediments by 14 Xue Meigui Tian Leyuan Wang Shuangfei. Study on the migration of organic contaminants from paper packaging to solid food J. Packaging and Food Machinery Ma Tingting Teng Ying Christie Peter et al. A new procedure J combining GC-MS with accelerated solvent extraction for the analysis of phthalic acid esters in contaminated soils J. Frontiers of Environmental Science & Engineering Huang Xiuling Wang Zhiwei Hu Changying et al. Migration mod- 31. el of chemical substances from paper andpaperboard through plastic coating layer J. Journal of Chemical Industry and Engineering China J J Wu Jianwen Wang Zhiwei Wang Nan et al. Migration of phthalates from microwave paper to food simulant tenax under microwave heating J. Food Science Tenax J J Zhang Jing Chen Huiming. Hazards and supervision status of phthalate 17 Gao Song Wang Zhiwei Hu Changying. Migration of plasticizers from paper packaging inks to food simulant under microwave heating J. Food Science Huang Congxing Duan Dandan Yang Qifeng et al. Migration of simulated contaminants in paper food packaging materials J. Food. J An Ying Zhou Ying. Study on the migration of phthalic acid ester in paper food packaging materials J. Standard & Quality of Light Industry J LI Zheng LIU Wen LIU Qun-hua. The Properties and Research JIAO Li MA Jinxia DAI Hong-qi. Preparation of Antibacterial and Oil-resistant Paper Using a NaOH-urea-ZnO Solution J. Transactions of China Pulp and Paper Xing Yinghao Wu Jun. Determination of 15 PAEs in fatty food by SPE-GC /MS J. Research on Food Packaging Technology Zhang Fei Zheng Jiagai Lin Qinheng et al. Determination of 14 phthalates in plastic spoon by SFE CO 2 -soxhletextraction and HPLC analysis J. The Food Industry CO 2 / 14 PAEs J Li X J Zeng Z R Chen Y et al. Determination of phthalate acid esters plasticizers in plastic by ultrasonic solvent extraction combined with solid-phase microextraction using calix 4 arenefiber J. Talanta capillary gas chromatography and flame ionization detector J. Journal of Environmental Science and Health Part A Toxic / Hazardous Substances & Environmental Engineering Wu Yumei Cheng Juan Hu Changying et al. Determination of phthalates in food packaging paper and tissue paper J. Packaging Engineering Liu Pengyan Huang Enjie Liu Jinwei et al. Solid-phase microextraction followed by gas chromatography-mass spectrometry for the de- 56 China Pulp & Paper Vol. 36 No

5 termination of volatile residual organic solvents in milk-products packaging J. Chinese Journal of Health Laboratory Technology WANG Cheng-yun XU Rong YANG Zuo-jun et al. Simultaneous Determination of Phthalate Plasticizers in Coated Papers by Gas Chromatography-Tandem Mass Spectrometry Coupled with Micro-. GC-MS wave-assisted Extraction J. China Pulp & Paper J Makklianga F Kanatharanaa P Thavarungkula P et al. Development of magnetic micro-solid phase extraction for analysis of phthalate esters in packaged food J. Food Chemistry Zhang Lianbo Rong Hui Yu Xiaoli et al. Determination of phthalates in plant fiber food packaging materials by gas chromatography J. Chinese Journal of Health Laboratory Technology in food samples using a chemiluminescentenzyme immunoassay J. J. Food Analytical Methods GB /T Determination of phthalates esters in food plastic packaging materials S. Spectral Analysis and analysis of plasticizer dioctyl phthalate J. Spectroscopy and GB /T S. 32 Bononi M Tateo F. Identification of diisobutylphthalate DIBP suspected as possible contaminant in recycled cellulose for take-away pizza boxes J. Packaging Technology & Science J Fu Shanliang Ding Li Jiao Yanna et al. Detection of 26 organic residues in food packaging paper material J. Packaging Engineering J Zhang M Hu Y Liu S et al. Rapid monitoring of dipropylphthalate 36 Liu Yu Wang Hu Wang Yan et al. Raman spectra Calculation J CPP ABB CIPTE QQ QQ zhilinzhan@ sina. com Http / /www. chinapaperexhibition. com

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