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Chinese Journal of Ecology 2011 30 12 2803-2808 * 1 2 2 3** 2 2 1 225009 2 210008 3 264003 / GC-MS 3 5-7 7 0. 1 g L -1 0. 1 g L -1 GC-MS Q946. 8 A 1000-4890 2011 12-2803-06 Identification of peanut root exudates and their allelopathic effects. WANG Xiao-bing 1 2 LUO Yong-ming 2 3** LIU Wu-xing 2 LI Zhen-gao 2 1 College of Environmental Sciences and Engineering Yangzhou University Yangzhou 225009 Jiangsu China 2 Key Laboratory of Soil Environment and Pollution Remediation of Chinese Academy of Sciences Institute of Soil Science Chinese Academy of Sciences Nanjing 210008 China 3 Yantai Institute of Coastal Zone Research Chinese Academy of Sciences Ynatai 264003 Shandong China. Chinese Journal of Ecology 2011 30 12 2803-2808. Abstract The root exudates of peanut collected by a modified continuous collecting device and XAD-4 ion exchange resin were identified by GC-MS and their allelophatic effects on Ralstonia solanacearum were studied. The root exudates mainly contained acetophenone glycerol benzoic acid 3 5-dimethyl benzaldehyde stearic acid palmitic acid and lactic acid among which only acetophenone had obvious promotion effect on the growth of R. solanacearum at concentration <0. 1 g L -1 and significant inhibitory effect at concentration >0. 1 g L -1. These findings could provide a credible basis for using acetophenone to control the occurrence of R. solanacearum. Key words peanut root exudates GC-MS Ralstonia solanacearum allelopathy. 2009 2011 2005 Sorensen et al. 2005 2006 2007 2010 Kong * 40432005 KSCX2-YW-G-053-3 Gil et al. ** E-mail ymluo@ issas. ac. cn 2011-05-14 2011-09-02 et al. 2008 Li et al. 2010 Senarathne et al. 2010 2011

2804 30 12 Perez & Oremeno-Nunez 1991 1. 5 75% 1 CRETS min 3 ~ 5 0. 1% HgCl Ralstonia solanacearum 5 min 3 ~ 5 25 2 d 1 1. 1 10 d 3 ~ 4 5 ph 5. 8 2. 2 ms cm -1 5 ml min -1 1. 2 12 Teflon 10 cm 15 15 cm BT100-1L 45 Toflen 10 ml 20 mm 250 mm 30 ml 0. 45 μm 0. 5 ~ 1. 0 mm -20 5 mm 1 1 1. 3 1. 6 GC-MS 2 ml L -1 GC- HCl 24 h 10% HCl 1 MS ph 2 ml CH 2 Cl 2 1 ml 250 μl 170 2 h Teflon 121 20 min 1 /10 Hoagland 16 h 25 8 h 16 60% 5 d BSTFA Sigma 75 ~ 80 1 h 1. 4 / GC-MS Agilent 7890GC- 5975MSD CTC 2010 XAD-4 80 1 min 30 min -1 200 6 min -1 250 5 min 30 min -1 270 5 min 260 Hao et al. 2007 XAD-4 GC MS 280 He Sigma 50 1 1. 2 ml min -1 3 1. 0 μl 24 h 2009 1. 7 20 mm 200 mm 190 mm 175 ml 10 ~ 15 0. 375 g 15

2805 g L -1 ph 7. 0 0. 15 1. 5 3. 0 7. 5 15 g L -1 1 ml 30 ml 0 0. 005 0. 05 0. 1 0. 25 0. 5 g L -1 YGPA 3 d 2 ml 10 μl 200 r min -1 30 18 h 4 5 g L -1 0. 5 g L -1 1 1. 5 ph 7. 0 121 20 min YGPA 10 g 5 g 5 g ph 7. 2 2 2. 1 1 Fig. 1 Cycling collection device of peanut root exudates Shen et al. 2001 Hoffland et al. 2. 2 1989 C 14 McDougall & Rovira 1970 Shen et al. 2005 10 d 3 ~ 4 5 d Tang & Young 1982 microdialysis 2005 / GC-MS2 2 CRETS Tang 15. 3 min Young 1982 3 m /z 149 167 279 1995 2003 2010 1 1 Teflon BSTFA m /z Teflon 73 C n H 2n+1 2 m /z 77 66 65 51 40 39 m /z 91 105 1

2806 30 12 2 Fig. 2 GAS-chromatogram of peanut root exudates 3 Fig. 3 GAS-chromatogram of CK 1 Table 1 Identification of peanut root exudates min % 1 3. 596 10. 15 2 3. 711 2. 95 3 4. 421 10. 15 3 5-4 4. 495 2. 52 5 4. 579 3. 57 6 9. 457 9. 81 7 11. 500 9. 42 2. 3 YGPA C 18 h 2 2. 4 18 h 3 3 0. 1 g L -1 0. 1 g L -1 P<0. 05 0. 1 g L -1 P < 0. 05 3 Uselman 2000 60%

2807 2 Table 2 Absorbance of peanut root exudates on Ralstonia solanacearum 3 5- OD 600 0. 030 0. 021 0. 012 0. 013 0. 024 0. 015 0. 012 0. 068 0. 1 g L -1 Hyder et al. 2002 4 Fig. 4 Effect of acetophenone on Ralstonia solanacearum Tang & Young 1982 Hao et al. 2007. 2003.. 25 6 5-10.. 2005.. 20 3 330-337.. 2003. XAD-4. 35 4 311-313. GC-MS. 2009.. 7 11 4 107-111.. 2009.. 21 8 38-39. 7 GC-MS. 2007.. 2 32-36.. 2005.. 34 2 17-22. NMR. 2011.. 48 4 53-58.. 2010. 2009. 39 2 6-10.. 2010.. 47 4 747-752.. 2006.. 35 1 29-33.. 2010..

2808 30 12 1 52-57. GC /MS. 14 5 17-21. Gil SV Meriles J Conforto C et al. 2011. Response of soil microbial communities to different management practices in surface soils of a soybean agroecosystem in Argentina. European Journal of Soil Biology 47 55-60. Hao ZP Wang Q Christie P et al. 2007. Allelopathic potential of watermelon tissues and root exudates. Scientia Horticulturae 112 315-320. Hoffland E Pindenegg GR Nelemans JA. 1989. Solubilization of rock phosphate by rape Ⅱ. Plant and Soil 113 161-165. Hyder PW Fredrickson EL Estell ME et al. 2002. Transport of phenolic compounds from leaf surface of creosotebush and tarbush to soil surface by precipitation. Journal of Chemical Ecology 28 2475-2482. Kong CH Wang P Zhao H et al. 2008. Impact of allelochemical exuded from allelopathic rice on soil microbial community. Soil Biology and Biochemistry 40 1862-1869. Li CG Li XM Kong WD et al. 2010. Effect of monoculture soybean on soil microbial community in the Northeast China. Plant and Soil 330 423-433. McDougall BM Rovira AD. 1970. Sites of exudation of C-labelled compounds from wheat roots. New Phytologist 69 999-1003. Perez FJ Oremeno-Nunez J. 1991. Root exudates of wild oates Allelopathic effect on spring wheat. Phytochemistry 30 2199-2201. Senarathne HS Dissanayaka NM Vidhana Arachchi LP. 2010.. 1995. Allelopathic potential of Brachiaria brizantha and B. milliformis on seed germination of selected bioassay species. Pakistan Journal of Weed Science Research 16 207-216. Shen H Wang XC Shi WM et al. 2001. Isolation and identification of specific root exudates in elephant grass Pennis lium L. in response to aluminum- and iron-bound phosphates. Journal of Plant Nutrition 24 1131-1144. Shen J Li H Neumann G et al. 2005. Nutrient uptake cluster root formation and exudation of protons and citrate in Lupinus albus as affected by localized supply of phosphorus in a split-root system. Plant Science 168 837-845. Sorensen RB Butts CL Rowland DL. 2005. Five years of subsurface drip irrigation on peanut What have we learned Peanut Science 32 14-19. Tang CS Young CC. 1982. Collection and identification of allelopathic compounds from the undisturbed root system of Bigalta limpograss Hemarthria altissima. Plant Physiology 69 155-160. Uselman SM Qualls RG Thoman RB. 2000. Effects of increased atmospheric CO 2 temperature and soil N availability on root exudation of dissolved organic carbon by a N-fixing tree Robinia pseudoacacia L.. Plant and Soil 222 191-202. 1976 E-mail xbwangxl@ sina. com. cn