MSWD = 1.06, probability = 0.39

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1 MSWD Institute of Geophysics and Planetary Physics Incremental Heating 36Ar(a) 37Ar(ca) 38Ar(cl) 39Ar(k) 40Ar(r) Age (Ma) 40Ar(r) (%) 1B15835D 670 C ± B15836D 730 C ± B15837D 800 C ± B15838D 870 C ± B15839D 950 C ± B15840D 1020 C ± B15841D 1080 C ± B15842D 1130 C ± B15843D 1180 C ± B15844D 1230 C ± B15845D 1280 C ± B15846D 1350 C ± B15847D 1420 C ± B15848D 1500 C ± B15849D 1550 C ± S Information on Analysis Results 40(r)/39(k) Age (Ma) Sample = EY113.4 Material = Groundmass Location = Furnace Analyst = Eric Thern Project = ANTILLES-NICE Mass Discrimination Law = POW Irradiation = I8t2h J = ± GA1550 = ± Ma Age Plateau MSWD = 1.06, probability = 0.39 ± ± ± 4.86% ± 5.05% Full External Error Analytical Error ± ± 0.71 Total Fusion Age ± 8.31% ± 8.41% Full External Error Analytical Error ± ± ± 0.71 ± _3 printed at 14/01/2014 (14:14)

2 Institute of Geophysics and Planetary Physics 39Ar(k) (%) K/Ca ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± Ar(k) (%,n) K/Ca Statistical T Ratio Error Magnification ± ± _3 printed at 14/01/2014 (14:14)

3 MSWD Institute of Geophysics and Planetary Physics Inverse Isochron 39(k)/40(a+r) 36(a)/40(a+r) r.i. 1B15835D 670 C ± ± B15836D 730 C ± ± B15837D 800 C ± ± B15838D 870 C ± ± B15839D 950 C ± ± B15840D 1020 C ± ± B15841D 1080 C ± ± B15842D 1130 C ± ± B15843D 1180 C ± ± B15844D 1230 C ± ± B15845D 1280 C ± ± B15846D 1350 C ± ± B15847D 1420 C ± ± B15848D 1500 C ± ± B15849D 1550 C ± ± Results 40(a)/36(a) 40(r)/39(k) Age (Ma) Inverse Isochron ± ± ± ± 1.53% ± 2.67% ± 3.02% Full External Error ± 0.26 Analytical Error ± Statistics Statistical F ratio 1.75 Convergence Error Magnification Number of Iterations Number of Data Points 14 Calculated Line Weighted York _3 printed at 14/01/2014 (14:15)

4 Institute of Geophysics and Planetary Physics Relative Abundances 36Ar %1s 37Ar %1s 38Ar %1s 39Ar %1s 1B15835D 670 C B15836D 730 C B15837D 800 C B15838D 870 C B15839D 950 C B15840D 1020 C B15841D 1080 C B15842D 1130 C B15843D 1180 C B15844D 1230 C B15845D 1280 C B15846D 1350 C B15847D 1420 C B15848D 1500 C B15849D 1550 C S Information on Analysis and Constants Used in Calculations Results Sample = EY113.4 Material = Groundmass Location = Furnace Analyst = Eric Thern Project = ANTILLES-NICE Mass Discrimination Law = POW Irradiation = I8t2h J = ± GA1550 = ± Ma IGSN = Undefined Preferred Age = Undefined Classification = Undefined Experiment Type = Undefined Extraction Method = Undefined Heating = 60 sec Isolation = 5.00 min Instrument = MAP Lithology = Undefined Lat-Lon = Undefined - Undefined Age Equations = Min et al. (2000) Negative Intensities = Allowed Decay Constant 40K = ± E-10 1/a Decay Constant 39Ar = ± E-07 1/h Decay Constant 37Ar = ± E-04 1/h Decay Constant 36Cl = ± E-06 1/a Production Ratio 36/38 in Cl = ± 13.2 Decay Constant 40K(EC,β+) = ± E-10 1/a Decay Constant 40K(β ) = ± E-10 1/a Abundance Ratio 40K/K = ± E-04 Atomic Weight K = ± g Age Plateau Total Fusion Age Normal Isochron No Convergence Inverse Isochron 18724_3_TabC_Relative Abundances printed at 14/01/2014 (14:20)

5 MSWD Institute of Geophysics and Planetary Physics 40Ar %1s Age s (Ma) 40Ar(r) 39Ar(k) (%) (%) K/Ca s ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± (r)/39(k) s Age s (Ma) 39Ar(k) (%,n) K/Ca s ± ± ± 4.86% ± 5.05% ± Full External Error ± Statistical T Ratio Analytical Error ± Error Magnification ± ± ± ± 8.31% ± 8.41% Full External Error Analytical Error ± 0.71 ± 0.70 ± ± ± 5.59% ± 5.76% 14 Full External Error ± Statistical F ratio Analytical Error ± Error Magnification ± ± ± 2.67% ± 3.02% 14 Full External Error Analytical Error ± ± Statistical F ratio Error Magnification 18724_3_TabC_Relative Abundances printed at 14/01/2014 (14:20)

6 Institute of Geophysics and Planetary Physics Procedure Blanks 36Ar 1s 37Ar 1s 38Ar 1s 39Ar 1s 40Ar 1B15835D 670 C B15836D 730 C B15837D 800 C B15838D 870 C B15839D 950 C B15840D 1020 C B15841D 1080 C B15842D 1130 C B15843D 1180 C B15844D 1230 C B15845D 1280 C B15846D 1350 C B15847D 1420 C B15848D 1500 C B15849D 1550 C _3_TabC_Relative Abundances printed at 14/01/2014 (14:18)

7 Institute of Geophysics and Planetary Physics 1s _3_TabC_Relative Abundances printed at 14/01/2014 (14:18)

8 Institute of Geophysics and Planetary Physics Sample Parameters Sample Material Location 1B15835D 670 C EY113.4 Groundmass Furnace 1B15836D 730 C EY113.4 Groundmass Furnace 1B15837D 800 C EY113.4 Groundmass Furnace 1B15838D 870 C EY113.4 Groundmass Furnace 1B15839D 950 C EY113.4 Groundmass Furnace 1B15840D 1020 C EY113.4 Groundmass Furnace 1B15841D 1080 C EY113.4 Groundmass Furnace 1B15842D 1130 C EY113.4 Groundmass Furnace 1B15843D 1180 C EY113.4 Groundmass Furnace 1B15844D 1230 C EY113.4 Groundmass Furnace 1B15845D 1280 C EY113.4 Groundmass Furnace 1B15846D 1350 C EY113.4 Groundmass Furnace 1B15847D 1420 C EY113.4 Groundmass Furnace 1B15848D 1500 C EY113.4 Groundmass Furnace 1B15849D 1550 C EY113.4 Groundmass Furnace 18724_3 printed at 14/01/2014 (14:22)

9 Temp Institute of Geophysics and Planetary Physics Analyst Eric Thern 670 Eric Thern 730 Eric Thern 800 Eric Thern 870 Eric Thern 950 Eric Thern 1020 Eric Thern 1080 Eric Thern 1130 Eric Thern 1180 Eric Thern 1230 Eric Thern 1280 Eric Thern 1350 Eric Thern 1420 Eric Thern 1500 Eric Thern _3 printed at 14/01/2014 (14:22)

10 Institute of Geophysics and Planetary Physics Standard (in Ma) %1s J %1s MDF %1s Volume Ratio Sensitivity (mol/volt) 18724_3 printed at 14/01/2014 (14:22)

11 Day Month Year Hour Min Resist Nmb Institute of Geophysics and Planetary Physics Irradiation Project Experiment Standard Name 20 APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA APR I8t2h Antilles-Nice verati-plga 01 GA _3 printed at 14/01/2014 (14:22)

12 Institute of Geophysics and Planetary Physics Irradiation Constants 40/36(a) %1s 40/36(c) %1s 38/36(a) %1s 38/36(c) %1s 1B15835D 670 C B15836D 730 C B15837D 800 C B15838D 870 C B15839D 950 C B15840D 1020 C B15841D 1080 C B15842D 1130 C B15843D 1180 C B15844D 1230 C B15845D 1280 C B15846D 1350 C B15847D 1420 C B15848D 1500 C B15849D 1550 C _3 printed at 10/01/2014 (16:28)

13 Institute of Geophysics and Planetary Physics 39/37(ca) %1s 38/37(ca) %1s 36/37(ca) %1s 40/39(k) %1s 38/39(k) %1s 36/38(cl) %1s 18724_3 printed at 10/01/2014 (16:28)

14 Institute of Geophysics and Planetary Physics K/Ca %1s K/Cl %1s Ca/Cl %1s 18724_3 printed at 10/01/2014 (16:28)

15 Age [ Ma ] WAAIF Curtin University, Perth, Australia VERATI-PLGA.AGE >>> EY113.4 >>> ANTILLES-NICE PROJECT MSWD = 1.06, probability = ± 0.43 Ma Ar-Ages in Ma WEIGHTED PLATEAU 8.57 ± 0.43 TOTAL FUSION 8.39 ± 0.71 NORMAL ISOCHRON 8.98 ± 0.52 INVERSE ISOCHRON 8.60 ± 0.26 MSWD Cumulative 39Ar Released [ % ] 18724_3 printed at 10/01/2014 (16:29) ArArCALC v2.50 Sample Info Groundmass Furnace Eric Thern IRR = I8t2h J = ±

16 K/Ca WAAIF Curtin University, Perth, Australia VERATI-PLGA.AGE >>> EY113.4 >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 8.57 ± 0.43 TOTAL FUSION 8.39 ± 0.71 NORMAL ISOCHRON 8.98 ± 0.52 INVERSE ISOCHRON 8.60 ± ± Cumulative 39Ar Released [ % ] 18724_3 printed at 10/01/2014 (16:30) ArArCALC v2.50 Sample Info Groundmass Furnace Eric Thern IRR = I8t2h J = ±

17 40Ar / 36Ar WAAIF Curtin University, Perth, Australia VERATI-PLGA.AGE >>> EY113.4 >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 8.57 ± 0.43 TOTAL FUSION 8.39 ± 0.71 NORMAL ISOCHRON 8.98 ± 0.52 INVERSE ISOCHRON 8.60 ± 0.26 MSWD AR/36AR INTERCEPT ± Sample Info 1000 Groundmass Furnace Eric Thern Ar / 36Ar 18724_3 printed at 10/01/2014 (16:31) ArArCALC v2.50 IRR = I8t2h J = ±

18 36Ar / 40Ar WAAIF Curtin University, Perth, Australia VERATI-PLGA.AGE >>> EY113.4 >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 8.57 ± 0.43 TOTAL FUSION 8.39 ± 0.71 NORMAL ISOCHRON 8.98 ± 0.52 INVERSE ISOCHRON 8.60 ± 0.26 MSWD AR/36AR INTERCEPT ± Ar / 40Ar 18724_3 printed at 10/01/2014 (16:31) ArArCALC v2.50 Sample Info Groundmass Furnace Eric Thern IRR = I8t2h J = ±

S

S MSWD Institute of Geophysics and Planetary Physics Incremental Heating 36Ar(a) 37Ar(ca) 38Ar(cl) 39Ar(k) 40Ar(r) Age (Ma) 40Ar(r) (%) 1B16079D 600 C 4 0.000034 0.033821 0.000003 0.001780 0.001016 0.72

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