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1 MSWD Institute of Geophysics and Planetary Physics Incremental Heating 36Ar(a) 37Ar(ca) 38Ar(cl) 39Ar(k) 40Ar(r) Age (Ma) 40Ar(r) (%) 1B16079D 600 C ± B16080D 700 C ± B16081D 800 C ± B16082D 870 C ± B16083D 950 C ± B16084D 1020 C ± B16085D 1080 C ± B16086D 1130 C ± B16087D 1180 C ± B16088D 1230 C ± B16089D 1280 C ± B16090D 1350 C ± B16091D 1420 C ± B16092D 1500 C ± B16093D 1550 C ± B15981D 600 C ± B15982D 700 C ± B15983D 800 C ± B15984D 870 C ± B15985D 950 C ± B15986D 1020 C ± B15987D 1080 C ± B15988D 1130 C ± B15989D 1180 C ± B15990D 1230 C ± B15991D 1280 C ± B15992D 1350 C ± B15993D 1420 C ± B15994D 1500 C ± B15995D 1550 C ± S Information on Analysis Results 40(r)/39(k) Age (Ma) Sample = PLG-F Material = plg Location = Furnace Analyst = Eric Thern Project = ANTILLES-NICE Mass Discrimination Law = POW Irradiation = I8t2h J = ± GA1550 = ± Ma Age Plateau Total Fusion Age ± ± ± 10.29% ± 10.30% 0.98 Full External Error ± Analytical Error ± ± ± ± 12.33% ± 12.34% Full External Error ± 0.16 Analytical Error ± _7 printed at 15/01/2014 (10:54)

2 Institute of Geophysics and Planetary Physics 39Ar(k) (%) K/Ca ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± Ar(k) (%,n) K/Ca Statistical T Ratio Error Magnification ± ± _7 printed at 15/01/2014 (10:54)

3 MSWD Institute of Geophysics and Planetary Physics Inverse Isochron 39(k)/40(a+r) 36(a)/40(a+r) r.i. 1B16079D 600 C ± ± B16080D 700 C ± ± B16081D 800 C ± ± B16082D 870 C ± ± B16083D 950 C ± ± B16084D 1020 C ± ± B16085D 1080 C ± ± B16086D 1130 C ± ± B16087D 1180 C ± ± B16088D 1230 C ± ± B16089D 1280 C ± ± B16090D 1350 C ± ± B16091D 1420 C ± ± B16092D 1500 C ± ± B16093D 1550 C ± ± B15981D 600 C ± ± B15982D 700 C ± ± B15983D 800 C ± ± B15984D 870 C ± ± B15985D 950 C ± ± B15986D 1020 C ± ± B15987D 1080 C ± ± B15988D 1130 C ± ± B15989D 1180 C ± ± B15990D 1230 C ± ± B15991D 1280 C ± ± B15992D 1350 C ± ± B15993D 1420 C ± ± B15994D 1500 C ± ± B15995D 1550 C ± ± Results 40(a)/36(a) 40(r)/39(k) Age (Ma) Inverse Isochron ± ± ± ± 1.06% ± 6.22% ± 6.25% Full External Error ± 0.07 Analytical Error ± Statistics Statistical F ratio 1.51 Convergence Error Magnification Number of Iterations Number of Data Points 27 Calculated Line Weighted York _7 printed at 15/01/2014 (10:57)

4 MSWD Institute of Geophysics and Planetary Physics Relative Abundances Age 40Ar(r) 39Ar(k) 36Ar %1 37Ar %1 38Ar %1 39Ar %1 40Ar %1 K/Ca (Ma) (%) (%) 1B16079D 600 C ± ± B16080D 700 C ± ± B16081D 800 C ± ± B16082D 870 C ± ± B16083D 950 C ± ± B16084D 1020 C ± ± B16085D 1080 C ± ± B16086D 1130 C ± ± B16087D 1180 C ± ± B16088D 1230 C ± ± B16089D 1280 C ± ± B16090D 1350 C ± ± B16091D 1420 C ± ± B16092D 1500 C ± ± B16093D 1550 C ± ± B15981D 600 C ± ± B15982D 700 C ± ± B15983D 800 C ± ± B15984D 870 C ± ± B15985D 950 C ± ± B15986D 1020 C ± ± B15987D 1080 C ± ± B15988D 1130 C ± ± B15989D 1180 C ± ± B15990D 1230 C ± ± B15991D 1280 C ± ± B15992D 1350 C ± ± B15993D 1420 C ± ± B15994D 1500 C ± ± B15995D 1550 C ± ± S Information on Analysis and Constants Used in Calculations Results 40(r)/39(k) Age (Ma) 39Ar(k) (%,n) K/Ca Sample = PLG-F Material = plg Location = Furnace Analyst = Eric Thern Project = ANTILLES-NICE Mass Discrimination Law = POW Irradiation = I8t2h J = ± GA1550 = ± Ma IGSN = Undefined Preferred Age = Undefined Classification = Undefined Experiment Type = Undefined Extraction Method = Undefined Heating = 60 sec Isolation = 5.00 min Instrument = MAP Lithology = Undefined Lat-Lon = Undefined - Undefined Age Equations = Min et al. (2000) Negative Intensities = Allowed Decay Constant 40K = ± E-10 1/a Decay Constant 39Ar = ± E-07 1/h Decay Constant 37Ar = ± E-04 1/h Decay Constant 36Cl = ± E-06 1/a Production Ratio 36/38 in Cl = ± 13.2 Decay Constant 40K(EC,β+) = ± E-10 1/a Decay Constant 40K(β ) = ± E-10 1/a Abundance Ratio 40K/K = ± E-04 Atomic Weight K = ± g ± ± Age Plateau ± 10.29% ± 10.30% ± Full External Error ± Statistical T Ratio Analytical Error ± Error Magnification ± ± 0.16 Total Fusion Age ± 12.33% ± 12.34% Full External Error ± 0.16 Analytical Error ± ± ± ± Normal Isochron ± 14.08% ± 14.09% 27 Full External Error ± Statistical F ratio Analytical Error ± Error Magnification ± ± Inverse Isochron ± 6.22% ± 6.25% 27 Full External Error ± Statistical F ratio Analytical Error ± Error Magnification 18724_7 printed at 15/01/2014 (11:06)

5 Institute of Geophysics and Planetary Physics Procedure Blanks 36Ar 1s 37Ar 1s 38Ar 1s 39Ar 1s 40Ar 1B16079D 600 C B16080D 700 C B16081D 800 C B16082D 870 C B16083D 950 C B16084D 1020 C B16085D 1080 C B16086D 1130 C B16087D 1180 C B16088D 1230 C B16089D 1280 C B16090D 1350 C B16091D 1420 C B16092D 1500 C B16093D 1550 C B15981D 600 C B15982D 700 C B15983D 800 C B15984D 870 C B15985D 950 C B15986D 1020 C B15987D 1080 C B15988D 1130 C B15989D 1180 C B15990D 1230 C B15991D 1280 C B15992D 1350 C B15993D 1420 C B15994D 1500 C B15995D 1550 C _7 printed at 15/01/2014 (11:09)

6 Institute of Geophysics and Planetary Physics 1s 18724_7 printed at 15/01/2014 (11:09)

7 Institute of Geophysics and Planetary Physics Sample Parameters Sample Material Location 1B16079D 600 C Plg-F plg Furnace 1B16080D 700 C Plg-F plg Furnace 1B16081D 800 C Plg-F plg Furnace 1B16082D 870 C Plg-F plg Furnace 1B16083D 950 C Plg-F plg Furnace 1B16084D 1020 C Plg-F plg Furnace 1B16085D 1080 C Plg-F plg Furnace 1B16086D 1130 C Plg-F plg Furnace 1B16087D 1180 C Plg-F plg Furnace 1B16088D 1230 C Plg-F plg Furnace 1B16089D 1280 C Plg-F plg Furnace 1B16090D 1350 C Plg-F plg Furnace 1B16091D 1420 C Plg-F plg Furnace 1B16092D 1500 C Plg-F plg Furnace 1B16093D 1550 C Plg-F plg Furnace 1B15981D 600 C Plg-G plg Furnace 1B15982D 700 C Plg-G plg Furnace 1B15983D 800 C Plg-G plg Furnace 1B15984D 870 C Plg-G plg Furnace 1B15985D 950 C Plg-G plg Furnace 1B15986D 1020 C Plg-G plg Furnace 1B15987D 1080 C Plg-G plg Furnace 1B15988D 1130 C Plg-G plg Furnace 1B15989D 1180 C Plg-G plg Furnace 1B15990D 1230 C Plg-G plg Furnace 1B15991D 1280 C Plg-G plg Furnace 1B15992D 1350 C Plg-G plg Furnace 1B15993D 1420 C Plg-G plg Furnace 1B15994D 1500 C Plg-G plg Furnace 1B15995D 1550 C Plg-G plg Furnace 18724_7 printed at 15/01/2014 (11:11)

8 Temp Institute of Geophysics and Planetary Physics Analyst Eric Thern 600 Eric Thern 700 Eric Thern 800 Eric Thern 870 Eric Thern 950 Eric Thern 1020 Eric Thern 1080 Eric Thern 1130 Eric Thern 1180 Eric Thern 1230 Eric Thern 1280 Eric Thern 1350 Eric Thern 1420 Eric Thern 1500 Eric Thern 1550 Eric Thern 600 Eric Thern 700 Eric Thern 800 Eric Thern 870 Eric Thern 950 Eric Thern 1020 Eric Thern 1080 Eric Thern 1130 Eric Thern 1180 Eric Thern 1230 Eric Thern 1280 Eric Thern 1350 Eric Thern 1420 Eric Thern 1500 Eric Thern _7 printed at 15/01/2014 (11:11)

9 Institute of Geophysics and Planetary Physics Standard (in Ma) %1s J %1s MDF %1s Volume Ratio Sensitivity (mol/volt) 18724_7 printed at 15/01/2014 (11:11)

10 Day Month Year Hour Min Resist Nmb Institute of Geophysics and Planetary Physics Irradiation Project Experiment Standard Name 02 MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA MAY I8t2h Antilles-Nice verati-plgf 01 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA APR I8t2h Antilles-Nice 1B15981D 02 GA _7 printed at 15/01/2014 (11:11)

11 Institute of Geophysics and Planetary Physics Irradiation Constants 40/36(a) %1s 40/36(c) %1s 38/36(a) %1s 38/36(c) %1s 1B16079D 600 C B16080D 700 C B16081D 800 C B16082D 870 C B16083D 950 C B16084D 1020 C B16085D 1080 C B16086D 1130 C B16087D 1180 C B16088D 1230 C B16089D 1280 C B16090D 1350 C B16091D 1420 C B16092D 1500 C B16093D 1550 C B15981D 600 C B15982D 700 C B15983D 800 C B15984D 870 C B15985D 950 C B15986D 1020 C B15987D 1080 C B15988D 1130 C B15989D 1180 C B15990D 1230 C B15991D 1280 C B15992D 1350 C B15993D 1420 C B15994D 1500 C B15995D 1550 C _7 printed at 15/01/2014 (11:12)

12 Institute of Geophysics and Planetary Physics 39/37(ca) %1s 38/37(ca) %1s 36/37(ca) %1s 40/39(k) %1s 38/39(k) %1s 36/38(cl) %1s 18724_7 printed at 15/01/2014 (11:12)

13 Institute of Geophysics and Planetary Physics K/Ca %1s K/Cl %1s Ca/Cl %1s 18724_7 printed at 15/01/2014 (11:12)

14 Age [ Ma ] WAAIF Curtin University, Perth, Australia VERATI-COMBOPLAGF+G.AGE >>> PLG-F >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 1.15 ± 0.12 TOTAL FUSION 1.32 ± 0.16 NORMAL ISOCHRON 1.01 ± 0.14 INVERSE ISOCHRON 1.08 ± 0.07 MSWD Cumulative 39Ar Released [ % ] 18724_7 printed at 15/01/2014 (11:14) ArArCALC v2.50 Sample Info plg Furnace Eric Thern IRR = I8t2h J = ±

15 K/Ca WAAIF Curtin University, Perth, Australia VERATI-COMBOPLAGF+G.AGE >>> PLG-F >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 1.15 ± 0.12 TOTAL FUSION 1.32 ± 0.16 NORMAL ISOCHRON 1.01 ± 0.14 INVERSE ISOCHRON 1.08 ± Cumulative 39Ar Released [ % ] 18724_7 printed at 15/01/2014 (11:15) ArArCALC v2.50 Sample Info plg Furnace Eric Thern IRR = I8t2h J = ±

16 40Ar / 36Ar WAAIF Curtin University, Perth, Australia VERATI-COMBOPLAGF+G.AGE >>> PLG-F >>> ANTILLES-NICE PROJECT 900 Ar-Ages in Ma WEIGHTED PLATEAU 1.15 ± 0.12 TOTAL FUSION 1.32 ± 0.16 NORMAL ISOCHRON 1.01 ± 0.14 INVERSE ISOCHRON 1.08 ± 0.07 MSWD AR/36AR INTERCEPT ± Sample Info plg Furnace Eric Thern Ar / 36Ar 18724_7 printed at 15/01/2014 (11:16) ArArCALC v2.50 IRR = I8t2h J = ±

17 36Ar / 40Ar WAAIF Curtin University, Perth, Australia VERATI-COMBOPLAGF+G.AGE >>> PLG-F >>> ANTILLES-NICE PROJECT Ar-Ages in Ma WEIGHTED PLATEAU 1.15 ± 0.12 TOTAL FUSION 1.32 ± 0.16 NORMAL ISOCHRON 1.01 ± 0.14 INVERSE ISOCHRON 1.08 ± 0.07 MSWD AR/36AR INTERCEPT ± Ar / 40Ar 18724_7 printed at 15/01/2014 (11:17) ArArCALC v2.50 Sample Info plg Furnace Eric Thern IRR = I8t2h J = ±

MSWD = 1.06, probability = 0.39

MSWD = 1.06, probability = 0.39 MSWD Institute of Geophysics and Planetary Physics Incremental Heating 36Ar(a) 37Ar(ca) 38Ar(cl) 39Ar(k) 40Ar(r) Age (Ma) 40Ar(r) (%) 1B15835D 670 C 4 0.000001 0.078288 0.000010 0.001470 0.010633 9.19

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