Metallurgical Analysis. qu) 2 BPB, 1 Table 1 Spectrophotometric determination of copper. / 10 4 (L mol - 1 cm - 1 )
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1 Metallurgical Analysis : (2003) , (, ) : ( ), 147 :; :O :A,,Cu 2 + 4,22 2, ph10 Cu + 2,2 2 (Bi2qu) (BPB) Cu(Bi2 qu) 2 BPB,, [13 ] BPB ( ) Cu + [10 ],,, 22(42, ),,- [11, ], [12 max = 420nm ] 22(32 22,4,52 )252 (CTZADMB) 1,, [13 ] Cu Χ - CAS - CTMAB -, (DDTC) [14, ],, [4 ] [5,6 ] [7 ] - [8 ] Cu Β - SCN - - RhB - Cu, 1 [47,1578 ] [9,,, ] Chromogenic system 1 Table 1 Spectrophotometric of copper Condition of max (ph) / 10 4 (L mol - 1 cm - 1 ) (g/ ml) Cu (DDTC) , [4 ] Cu DDTC , [5 ] Cu DDTC [6 ] Cu DDTC [7 ] : : ( ),(),,,,,, 104, 24
2 Metallurgical Analysis Chromogenic system Condition of max (ph) / 10 4 (L mol - 1 cm - 1 ) (g/ ml) 1 Cu A , [15] Cu S , [16] Cu S ,, [17] Cu ,[18] Cu meso2( ) [ T( , [19] TMAP) P] Cu ,10,152( ) [20] Cu [ 42(42 ) ] [21] 10,15, ,[22] ( TTZAPN) Cu 2 + Cu ( H2 ) [23] Cu (22 ) [ 24 ] Cu [ 32(52 ) ] [ 25 ] 62 Cu S [ 26 ] Cu CAS - CTMAB , [ 27 ] Cu N2 2N2( , [ 28 ] ) Cu (N,N 2 ) [ 29 ] Cu N2 2N 2( ,[ 30 ] ) Cu ( ) ) [ 31 ] Cu (32 ) , [ 32 ] Cu ( )282( ) [ 33 ] ( PANPAQ) Cu (42 ) [ 34 ] (ADA) Cu [ 35 ] Cu ( ) ,[ 36 ] Cu (22 ) [ 37 ] Cu (22 23,52 )232[ , [ 38 ] ( ) ]2 Cu (22 ) [ 39 ] Cu ( )22, [ 40 ] Cu (2 2 ) ,[ 41 ] Cu ( )22, [ 42 ] Cu [ (52222 ) ]22, [ 43 ] (52Br2PAND) - TritonX2100 Cu ( ) [ 44 ] 23,62 (52NO 2 2PAH) Cu H 3 PO [ 45 ] Cu Br2PADAP [ 46 ] 25
3 Metallurgical Analysis Chromogenic system Condition of max (p H) / 10 4 (L mol - 1 cm - 1 ) (g/ ml) 1 Cu (52 21,3,42 ) , [ 47 ] (CTZAN) Cu ( ) , [ 48 ] ( PAHQS) - Cu [ 49 ] Cu [ 50 ] 222 Cu , [ 51 ] Cu ,[ 52 ] Cu [ 53 ] Cu [ 54 ] Cu , [ 55 ] Cu , [ 56 ] Cu ,,, [ 57 ] Cu [ 58 ] Cu meso2(42 ) [ 59 ] Cu [ 42( 22 ) [ 60 ] ]210,15,20 Cu [ 42( 42 ) ] [ 61 ] 10,15,202(42 ) Cu , [ 62 ] Cu [ 63 ] Cu (NHCM) [ 64 ] Cu [ 65 ] Cu [ 66 ] Cu PAN [ 67 ] Cu PAN , [ 68 ] Cu ,52( ) ,, [ 69 ] Cu [ 42(32N2 ) ]210,15,202(42 ) [ 70 ] Cu [ 71 ] Cu (ASA pa) Cu I - - B,, [ 72 ] mol/ L [ 73 ] H 2 SO 4 Cu B - - 1mol/ L ,[ 74 ] H 2 SO 4 Cu PAN - I ,,, [ 75 ] Cu (DPC) - CPB - OP [ 76 ] Cu , [ 77 ] Cu [ 78 ] (CAA) 26
4 Metallurgical Analysis 2,,, [79 ] 22( ) ,62, [84 ] Cu Β - 2,2 2 - (BPB) 640nm, 550nm, BPB, , 0, 0148g/ ml 114g/ ml, [85 ] [80 ] ( PIF) - [86,524nm,582nm, ], p H612 - HCl,p H8915N H 4 Cl - N H 3 H 2 O, ( CPB), max = 600nm, 600 = ,Cu 2 + 0, = , 0 614g/ ml Cu ΧBCO 0120g/ ml 1 3,1h, [87, ] EDTA - 52(5 222, Cu Χ, )22,42 (52NO 2 2PADA T), max = 510nm, g/ ml, Cu Β [81 ], p H ,,Cu Β 1 2, 519nm, 436nm, Cu Β p H110,, 0017g/ ml, [ Cu (SCN) 4 ] 2 -, 519, ,, max = 587nm, max = , N 2 [82 ] Cu Χ - 30mL/ min, 10min,Cu 2 + (DBO K2CPA), p H710 -, Ni 2 +, , g/ L HCl Cu DBO K2, [88 CPA 1 2, ] p H10 NaOH,630nm, Cu Χ - 2,2 2 - (BPB), = BPB, BPB, (CV), CV, BPB, [83 ] 590nm, (BCO), Cu Χ - BCO, 590 = , 0 Ni Χ - BCO, 014mg/ L, [89, Cu Χ - BCO 610nm, ],Cu Χ Ni Χ - BCO 580nm, 610nm, 680nm [ Cu ( SCN) 4 ] 2-27
5 Metallurgical Analysis, 0610ng/ ml,,, max = 587nm,= , 5, ng g/ ml,,, [90 ],, [91 ], 5min,435nm, 2 System 2 Table 2 Catalytic kinetic photometric of copper Condition of max (p H) / 10 4 (L mol - 1 cm - 1 ) (g/ ml) Cu KBrO 3 - B H 2 SO [ 92 ] Cu KBrO ,, [ 93 ] Cu KBrO 3 - K H 2 SO [ 94 ] Cu KIO 3 - H 2 SO ,[ 95 ] Cu KClO (= ) 020 [ 96 ] Cu H 2 O 2 - M H 2 SO [ 97 ] Cu H 2 O [ 98 ] Cu H 2 O [ 99 ] Cu H 2 O [ 100 ] Cu H 2 O , [ 101 ] Cu H 2 O 2 - H 3 PO ,, [ 102 ] Cu H 2 O [ 103 ] Cu H 2 O [ 104 ] Cu H 2 O 2 - H 2 SO [ 105 ] Cu H 2 O 2 - R H 2 SO [ 106 ] Cu H 2 O [ 107 ] Cu H 2 O [ 108 ] Cu H 2 O , [ 109 ] Cu H 2 O , [ 110 ] Cu H 2 O [ 111 ] Cu H 2 O , [ 112 ] Cu H 2 O , [ 113 ] Cu H 2 O , [ 114 ] Cu H 2 O 2 - H 2 SO [ 115 ] Cu H 2 O [ 116 ] Cu H 2 O 2 - CAS , [ 117 ] Cu H 2 O [ 118 ] Cu VC [ 119 ] mol/ L H 2 SO 4 Cu VC - HCl [ 120 ] Cu VC [ 121 ] Cu VC [ 122 ] Cu VC - H 2 SO [ 123 ] Cu VC , [ 124 ] Cu VC , [ 125 ] 28
6 Metallurgical Analysis System Condition of max (p H) / 10 4 (L mol - 1 cm - 1 ) (g/ ml) 2 Cu VC - H 2 SO [ 126 ] Cu VC - B [ 127 ] Cu VC - K [ 128 ] Cu VC [ 129 ] Cu VC - H 3 PO [ 130 ] Cu NaNO 2 - R [ 131 ] Cu SF , [ 132 ] 6, Cu 2 +, g/ L, g/ L, RSD 314 %, 1min,, [133 ] Cu ( )252 ( 52Br2PADAP), 717, [138, ] 12, [ (52222 ) 22,72 (52Br2PADN) [134 ] 4,4 2, TritonX2100, ( TEDA T) Cu Β, (NL PL S) Cu 2 +,, p H415 HAc - NaAc, 500nm, 00180g/ ml, 90 / h,, - CTMAB - [135 ], - Cu, Ni, Cd, Zn [139 ] [140 ] Cu - 52Br2PADAP - OP 0105, K 1105mg/ L, 20g/ L, 36 / h,,lu 3 + CN -, 7 Ni 2 +,Zn 2 +,,, Cu K, -, p H 517, nm, 5nm [136 ] Cu Χ - 1,602nm 11, - - G g/ ml,00156g/ ml,0 0180g/ ml, RSD 0159 %4195 %, [141, p H1016 KOH - H 3 BO 3 95 %105 % ], mg/ L,,, (MCM), mg/L, RSD = 316 % ( n = 10 ), [137 ] Lu 3 +,CN - 52Br2PADN, TritonX2100,,p H910 H 3 BO 3 - KOH, 29
7 Metallurgical Analysis Cu 2 +,Ni 2 +,Zn %,9212 %10218 % ;, g/ ml, g/ ml,01128g/ ml 22(52222 ) 52 (52Br2PADAP),CCD, - [142 ], : 00140g/ ml, g/ ml ; : 0102g/ ml, 0105g/ ml ; : 9313 % Fluorescent system 219 %710 %, 8,,, 3 3 Table 3 Fluorophotometric of copper Condition of ex / em (p H) Detection limit (ng/ ml) (g/ ml) Cu / [ 143 ] Cu (22 ) / [ 144 ] Cu , / [ 145 ] Cu / , [ 146 ] Cu (42 ) / ,,,,,, [ 147 ], [ 20 ] 1 [J ],2000,20 (1) :81 : [ 1 ] 1 [J ],1996,12 (6) :3341 [ 2 ] 1 [J ],1997,13 (1) :281 [ 3 ] 1 () [J ],2000,36 (10) :4741 [ 4 ], 1 [J ],1999,6 (7) :641 [ 5 ] 1 [J ],1998,18 (4) :411 [ 6 ], 1 [J ],2001,21 (2) :71 [ 7 ],,,1 [J ],1999,6 [ 28 ] 1 () [J ],2000,36 (2) :681 (8) :581 [ 29 ] 1 [J ],2000,28 (4) :5251 [ 8 ], 1 () [J ],2002,38 (2) :831 [ 9 ], 1 [J ],2000,23 (1) :541 [ 10 ] 1 ( ) [J ],1999,19 (1) :321 [11 ] 1 ( ) [J ],2000, (1) : 361 [12 ],,,1 [J ], 2001, 29 ( 1) : 1141 [ 13 ] 1 ( ) [J ],2000,22 (1) :441 [ 14 ] 1 () [J ],2001,37 (4) :1821 [ 15 ] 1 () [J ],2001,37 (6) :2471 [ 16 ] 1 [J ],1999,25 (4) : [17 ],,,1 () [J ], 1999, 35 (3) :1261 [ 18 ], 1 [J ],1999,21 (5) :2961 [ 19 ], 1 [J ],1999,10 (3) :321 [ 21 ],, 1 [J ],1999,16 (2) :1651 [22 ],,,1 [J ],2000,17 (5) : 5641 [ 23 ],, 1 [J ],2000,17 (6) :6431 [24 ],,,1 [J ],2001,20 (1) : 451 [25 ], 1 [J ],2000,12 ( ) : 201 [ 26 ] 1 () [J ],1999,35 (12) :5331 [ 27 ] 1 () [J ],2001,37 (4) :1821 [30 ],,,1 () [J ], 1999, 35 (2) :511 [31 ],, () [J ],2001,37 (11) : 5081 [ 32 ],, 1 [J ],1998,18 (5) :121 [33 ],,,1 [J ],1998,15 (6) : 771 [ 34 ],, 1 [J ],1998,15 (6) :251 [35 ] 1 ( ) [J ],2000,26 (2) : 1681 [ 36 ], 1 () [J ],1999,35 (8) :3761
8 Metallurgical Analysis [ 37 ],, 1 [J ],1999,16 (4) :4421 [ 38 ] 1 [J ],1999,18 (4) :3111 [39 ], 1 ( ) [J ],, 2000,23 (1) :541 [40 ],,1 () [J ], 2000, 36 (3) :2591 [ 41 ],, 1 [J ],2000,41 (4) : [42 ],, 1 [J ],2000, [78 ] 1 ( ) [J ],1999,23 (4) : 15 (3) :271 [43 ],,,1 [J ],2000,19 (6) : 241 [44 ],,,1 [J ],2002,21 (1) : 521 [ 45 ],,,1 [J ],2001,21 (2) :91 [ 46 ],, 1 [J ],1999,16 (2) :1861 [ 47 ],, 1 [J ],2000,20 (4) :171 [48 ],,,1 () [J ], 2001, 37 (4) :1741 [ 49 ], 1 [J ],1999,21 (3) :1691 [ 50 ], 1 [J ],2000,17 (3) :3641 [51 ],,,1 [J ],1998,14 (3) :2281 [ 52 ] 1 [J ],1998,17 (3) :2381 [53 ],,,1 () [J ], 1998, 34 (6) :3261 [54 ],,,1 () [J ], 1999, 35 (10) : [55 ],,,1 ( [ 92 ] 1 [J ],2001,20 (4) :941 ) [J ],2000,9 (2) :901 [56 ],,, 1 [J ], , (4) :421 [57 ],,,1 () [J ], 2001, 37 (11) :5121 [ 58 ],,,1 [J ],1998,18 (4) :151 [59 ],, 1 () [J ],1998,34 (7) : 3221 [ 60 ] 1 [J ],2001,18 (3) :3761 [61 ],,,1 [J ],1999,16 (4) : ,29 (1) :301 [ 63 ], 1 [J ],2000,12 (4) :4521 [64 ],,1 [J ],2000,17 (5) : 5611 [ 65 ], 1 [J ],2000,22 (4) :121 [ 66 ], 1 () [J ],2000,36 (2) :721 [67 ],, 1 [J ],2000,12 (1) : 881 [68 ],,,1 [J ],1999,16 (4) : 4251 [ 69 ] 1 [J ],2000,16 (4) :2971 [ 70 ] 1 () [J ],2000,36 (9) :3941 [ 71 ] 1 () [J ],2000,36 (10) :4421 [72 ],,,1 () [J ], 2000, 36 (10) :4531 [ 73 ],,,1 [J ],1998,18 (5) :421 [74 ],,,1 () [J ], 2000, 36 (12) :5551 [75 ],, 1 ( ) [J ],2001,14 (2) :1821 [ 76 ],, 1 [J ],2001,23 (3) :1611 [77 ],, 1 () [J ],1999,35 (12) : 3731 [79 ] 1 ( ) [J ],2000, (4) : 631 [ 80 ],, 1 [J ],1998,15 (6) :281 [ 81 ], 1 [J ],1999,18 (3) :421 [82 ], 1 ( ) [J ],2000,24 (1) :901 [ 83 ] 1 [J ],1999,21 (4) :321 [ 84 ] 1 () [J ],1998,34 (7) :3201 [ 85 ] 1 [J ],1998,26 (7) :9131 [ 86 ],, 1 [J ],1998,18 (4) :261 [ 87 ] 1 [J ],1998,18 (4) :451 [ 88 ],,,1 [J ],1998,5 (11) :711 [89 ],, 1 [J ],1999,19 (1) :1021 [ 90 ],, 1 [J ],2000,27 (5) :461 [91 ],,,1 [J ],1999,18 (3) : [ 93 ],,,, [J ],2001,20 (6) : [ 94 ] 1 [J ],1998,17 (4) :341 [ 95 ],, 1 [J ],2000,19 (3) :481 [ 96 ] 1 [J ],1999, (3) :521 [ 97 ], 1 [J ],2000, (1) :761 [98 ],,1 [J ],2001,20 (5) : 491 [ 99 ], 1 [J ],1999,19 (1) :571 [ 100 ], 1 [J ],1999,15 (3) :2071 [ 101 ], 1 [J ],1999,27 (5) :5741 [ 62 ],, 1 ( ) [J ], [102 ],,,1 [J ],2001,29 (8) : 9071 [ 103 ] 1 [J ],1998,19 (1) :391 [ 104 ], 1 [J ],1998,5 (3) :1841 [ 105 ], 1 [J ],1998,15 (4) :651 [106 ],,,1 [J ], 1998, (4) :571 [ 107 ],, 1 [J ], 2000, 12 (3) :3311 [ 108 ], 1 [J ],2000, (5) :361 [109 ],,,1 [J ],2000,28 (11) : [ 110 ], 1 [J ],2001,28 (1) :531 [ 111 ],, 1 [J ], 2001,23 (2) :391 [ 112 ],, 1 [J ],1999,18 (4) :491 [ 113 ], 1 ( ) [J ],
9 Metallurgical Analysis (3) :1231 [114 ], 1 ( ) [J ], 1999,15 (3) :2071 [ 115 ], 1 () [J ],1999,35 (8) :3641 [116 ],, 1 [J ],1999,15 (5) : 4371 [ 117 ] 1 [J ],2000, (1) :541 [118 ],,1 [J ],2000,18 (3) : 3191 [ 119 ] 1 () [J ],2001,37 (4) :1641 [ 120 ] 1 () [J ],1998,34 (6) :2541 [ 121 ], 1 [J ],1999,25 (1) :251 [ 122 ], 1 () [J ],1999,35 (7) :3501 [ 123 ], [J ],1998,20 (4) :2241 [ 124 ] 1 [J ],2000,20 (6) :241 [ 125 ], 1 [J ],2001,18 (2) :2371 [126 ], 1 () [J ],,2001,37 (4) : 1641 [ 127 ], 1 [J ],2000,19 (4) :731 [ 128 ], 1 [J ],2000,19 (4) :801 [129 ],, 1 [J ],2000,16 (3) : 2201 [ 130 ] 1 [J ],2000,20 (2) :2501 [131 ],, 1 () [J ],2000,36 (12) : 5391 [ 132 ],, 1 [J ],1999,18 (6) :311 [133 ],,,1 () [J ],2001,37 (9) :3881 [134 ],, 1 () [J ],1999,35 (9) : 4021 [ 135 ],, 1 [J ],1999,18 (4) :2631 [ 136 ] 1 [J ],2000,28 (5) :5731 [ 137 ],, 1 [J ],1998,17 (5) :781 [138 ],, 1 [J ],2001,20 (1) : 401 [ 139 ],, [J ],2000,19 (6) :51 [ 140 ], 1 () [J ],2001,37 (6) :2721 [ 141 ],, 1 [J ],2001,21 (3) :11 [142 ],,,1 () [J ],1999,35 (10) :4401 [ 143 ], 1 ( ) [J ],2000,19 (2) :611 [ 144 ], 1 [J ],1999,19 (5) :101 [145 ], 1 ( ) [J ], 1999,22 (4) :3711 [146 ],, 1 [J ],2000,20 (1) :991 [ 147 ], 1 [J ],2001,18 (2) :2191 Progress of photometric analysis of copper in China ZHAI Qing2zhou,FAN Zhi ( Research Center for Nanotechnology,Changchun University of Science and Technology, Changchun ,China) Abstract :A review is given for the progress of the photometric analysis of copper in China according to general photometry,dual2wavelength photometry,three wavelength photometry,extraction photometry,flotation photometry,kinetic photometry,flow injection photometry,calculation photometry,fluorescence spectrophotometry during the recent year ( ) 1One hundred and forty seven references were cited1 Key words :copper ;photometry ;review ( 42 ) Determination of zinc in aluminium alloy by spectrophotometry SHEN Liang2feng (Department of Civil Engineering of Hunan University of Science and Technology,Xiangtan ,China) Abstract :The color reaction of zinc Χ with 22[ (52bromo222pyridyl)2azo ]252diethylaminophenol (52Br2PADAP) was investigated in the presence of surfactant such as cetyltrimethylammonium bromide (CTMAB), Tween220, Triton X2100 in the ammonia2ammonium chloride buffer solution (p H815) 1 It was found that CTMAB had the best enhanced sensitivity effect. Based on this a spectrophotometric method for of trace zinc was proposed1the red complex of Zn Χ with 52Br2PADAP has a maximum absorptivity at 555nm1The apparent molar absorptivity is L mol - 1 cm - 1 1Beer s law is obeyed in the range of 0-15g/ 25mL for zinc1this method has been applied to the of trace zinc in aluminium alloy with satisfactory results1 Key words :zinc ;aluminium alloy ;spectrophotometry 32
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