PM Characterization of Organic Carbon OC and Elemental Carbon EC in PM 2. 5 During the Winter in Three Major Cities in Fujian Province China
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1 ENVIRONMENTAL SCIENCE Vol 34 No 5 May 2013 PM * PM 2 5 thermal optical transmission TOT PM 2 5 OC EC OC EC OC /EC PM ± ~ ± μg m - 3 GB PM μg m - 3 OC EC C ± 2 65 ~ ± 1 96 μg m ± 0 50 ~ 3 36 ± 0 41 μg m ~ ~ 2 0 R 2 = 0 70 R 2 = 0 66 PM 2 5 OC EC OC EC OC /EC 5 64 ~ secondary organic carbon SOC 2 47 ~ 7 17 μg m - 3 OC 13 08% ~ 45 67% PM % ~ 7 78% PM 2 5 X513 A Characterization of Organic Carbon OC and Elemental Carbon EC in PM 2 5 During the Winter in Three Major Cities in Fujian Province China CHEN Yan-ting 1 2 CHEN Jin-sheng 2 HU Gong-ren 1 XU Ling-ling 2 YIN Li-qian 2 ZHANG Fu-wang 2 1 Environmental Science and Engineering Department College of Chemical Engineering Huaqiao University Xiamen China 2 Key Laboratory of Urban Environment and Health Institute of Urban Environment Chinese Academy of Sciences Xiamen China Abstract PM 2 5 samples were collected in three cities Fuzhou Xiamen and Quanzhou in Fujian Province China during the winter and were analyzed for organic carbon OC and elemental carbon EC by thermal optical transmission TOT The characteristics such as pollution levels and spatial distributions of PM 2 5 OC and EC correlations between OC and EC OC /EC ratios and secondary organic carbon SOC were discussed in details Average concentrations of PM 2 5 were ranged from ± μg m - 3 to ± μg m - 3 which were in excess of the Ambient Air Quality Standards GB hr massbased standards of 75 μg m - 3 Averages concentrations of OC and EC were fluctuated from ± 2 65 μg m - 3 to ± 1 96 μg m - 3 and 1 99 ± 0 50 μg m - 3 to 3 36 ± 0 41 μg m - 3 respectively which were 1 2 to 1 6 times and 1 2 to 2 0 times more than that in the background site Pingtan in Fuzhou Correlations between OC and EC in PM 2 5 were found to be strong in Pingtan R 2 = 0 70 and Jin'an R 2 = 0 66 Fuzhou suggesting that there were similar primary pollutants of OC and EC Average OC /EC ratios were and all higher than 2 which indicated that the secondary organic carbon SOC was formed The estimated concentrations of SOC were from 2 47 μg m - 3 to 7 17 μg m - 3 which contributed 13 08% % to the OC and 2 20% -7 78% to PM 2 5 Key words PM 2 5 organic carbon OC elemental carbon EC thermal optical transmission TOT three major cities in Fujian Province organic carbon OC elemental carbon EC EC 1 ~ % OC 84 9% EC 2 5 μm 3 OC secondary organic carbon SOC OC EC KZCX2-YW ~ ytchen@ iue ac cn * grhu@ hqu edu cn
2 5 PM PM ~ 14 4 ~ 8 24 h TH-150C 9 ~ 12 PM L min - 1 PM 2 5 OC EC Whatman QFF Φ90 mm PM h 24 h 25 ± PM 2 5 OC EC 1 52 ± 1 % Sartorius T-114 PM OC EC mg PM PM 2 5 OC EC Sunset Lab Model-4 1 / 1 1 thermal optical transmission PM TOT National 7 Institute of Occupational Safety and Health NIOSH 10 EC 7 OC 0 1 μg m - 3 Table 1 / 1 Specific description of sampling sites / /m m ~ m 100 m Table 2 2 Meteorological parameters during sampling / /m s
3 He PM OC He /O 2 98% 2008 He + 2% O 2 EC PM μg m PM 2 5 He He /O 2 MnO 2 CO FID NDIR nm % OC He PM 2 5 He /O 2 EC OC EC ± 2 87 μg m ± 0 50 μg m - 3 OC EC 2 OC EC 4 98 m s - 1 OC 2 EC EC OC EC ± 0 41 μg m ± PM 2 5 OC EC μg m OC ± PM 2 5 OC EC 1 96 μg m ± 2 65 PM 2 5 μg m μg m ± OC EC > μg m ± μg m ± > > μg m ± μg m GB OC EC 2012 PM μg m - 3 PM 2 5 OC EC PM ± 5 17 μg m ± μg m OC EC Table 3 3 PM 2 5 OC EC Average concentrations of PM 2 5 OC and EC in Fuzhou Xiamen and Quanzhou PM 2 5 /μg m - 3 OC /μg m - 3 EC /μg m ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± ± OC EC OC EC 4 PM 2 5 OC EC OC EC OC /EC μg m μg m - 3
4 5 PM ± 29 8 μg m ± 2 4 μg m ± 14 8 μg m ± 2 4 μg m ± 33 2 μg m ± 5 3 μg m - 3 OC EC OC EC 13 OC 44% EC 44% 9% 3% OC EC 14 EC OC EC 20 3 ± 4 8 μg m ± 3 1 μg m - 3 OC PM 2 5 OC EC EC Table 4 4 PM 2 5 OC EC Average concentrations of OC and EC in PM 2 5 during the winter in other cities OC /μg m - 3 EC /μg m / TOR ± ± 2 4 / TOR ~ ± ± 2 2 / TOT ~ ± ± 5 3 / TOR ~ ± ± 1 0 / TOT ~ ± ± 3 1 / TOT ~ / TOT ~ ± ± 2 5 / TOT ~ / TOT ~ / TOT ~ ± ± 0 1 / TOT ~ TOT TOR OC EC TOT OC TOR 2 2 OC EC EC R OC EC = 0 70 R 2 = 0 66 PM 2 5 OC EC OC EC OC EC OC EC OC EC 1 PM 2 5 OC Fig 1 1 PM 2 5 OC EC Correlations between OC and EC in PM 2 5 during the winter in Fuzhou Xiamen and Quanzhou
5 OC /EC OC /EC OC /EC = 3 8 ~ OC / EC OC /EC PM 2 5 OC /EC OC /EC OC PM 2 5 OC /EC 5 64 ± 0 93 ~ 7 71 ± EC OC /EC < OC < 6 10 EC 24 OC /EC 6 47 < 6 88 OC 2 3 EC EC EC EC 2 Fig 2 PM 2 5 OC /EC OC /EC ratios in PM 2 5 during the winter in Fuzhou Xiamen and Quanzhou OC /EC 3 OC OC /EC OC /EC = 4 3 ~ m EC primary organic carbon POC OC secondary organic carbon SOC OC /EC OC /EC SOC OC /EC 1 2 secondary organic carbon SOC SOC = OC tot - OC pri 1 OC pri = EC OC /EC min 2 SOC μg m - 3 OC tot μg m - 3 OC pri μg m - 3 EC μg m - 3 OC /EC min OC /EC OC /EC min OC /EC OC EC OC EC OC EC OC /EC SOC O 3 OC /EC EC SOC 5 OC 5 PM 2 5 SOC OC OC /EC PM 2 5 OC /EC POC SOC TC 8 53 ~ μg m - 3 VOCs 2 47 ~ 7 17 μg m ~ μg m - 3 OC /EC PM 2 5 POC SOC OC /EC 2 93 μg m
6 5 PM Table 5 5 PM 2 5 SOC Levels of secondary organic carbon SOC in PM 2 5 during the winter at Fuzhou Xiamen and Quanzhou POC /μg m - 3 SOC TC 1 /μg m - 3 /μg m - 3 POC /TC EC /TC SOC /TC SOC /OC SOC /PM TC = OC + EC OC = SOC + POC μg m ~ ± 1 96 μg m ± 0 50 ~ ± 0 41 μg m ~ POC TC 46 30% 50% 38 92% 11 30% 20 50% PM 2 5 SOC 2 47 ~ 7 17 PM 2 5 SOC OC μg m - 3 OC PM % ~ 13 08% ~ 45 67% SOC PM % 2 20% ~ 7 78% 2 20% ~ 7 78% 32 SOC 15 SOC 6 33 PM 2 5 SOC OC 35 2% 49 2% 40 7% 48 3% 40% SOC OC 13 08% 24 20% 18 01% 26 58% SOC OC 45 67% 42 10% 3 1 PM ± ~ ± μg m GB PM μg m - 3 OC EC ± ~ OC EC OC EC SOC TC SOC TC 37 11% 3 OC /EC Menon S Hansen J Nazarenko L et al Climate effects of black carbon aerosols in China and India J Science Offenberg J H Barker J E Aerosol size distributions of elemental and organic carbon in urban and over-water atmospheres J Atmospheric Environment Chen S J Liao S H Jian W J et al Particle size distribution of aerosol carbons in ambient air J Environment International Ho K F Lee S C Chan K C et al Characterization of chemical species in PM 2 5 and PM 10 aerosols in Hong Kong J Atmospheric Environment Ye B M Ji X L Yang H Z et al Concentration and chemical composition of PM 2 5 in Shanghai for a 1-year period J Atmospheric Environment Cao J J Lee S C Ho K F et al Characteristics of carbonaceous aerosol in Pearl River Delta Region China during 2001 winter period J Atmospheric Environment Pathak R K Wang T Ho K F et al Characteristics of
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