TEMPO Nanofibrillated Cellulose NFC NFC NFC. Preparation of NFC by Homogenizing and Ultrasonic Method and the Properties of Its Nanopaper
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1 NFC NFC * TEMPO Nanofibrillated Cellulose NFC NFC 2 h 4 h 2 5 NFC 19 nm 20 kwh 2 h 4 h 2 5 NFC 4h NFC MPa % NFC TQ351 A DOI /j. issn X Preparation of NFC by Homogenizing and Ultrasonic Method and the Properties of Its Nanopaper YAO Zhi-ming CHEN Gang * FANG Zhi-qiang KUANG Yu-di KUANG Qi-tong XU Ya-xi ZHANG Bao-jun State Key Lab of Pulp and Paper Engineering South China University of Technology Guangzhou Guangdong Province * papercg@ scut. edu. cn Abstract NFC was prepared by using bleached krafteucalyptus pulp as new material it was treated with TEMPO oxidation process at first then fibrillated by homogenizing or ultrasonic method finally the nanopaper made of the NFC was fabricated by solution casting method. The effects of different preparation methods on the properties of NFC and its nanopaper were discussed. The results showed that under different energy consumption NFC prepared by ultrasonic treatment 2 h and 4 h had better transparency higher length to diameter ratio and smaller diameter than that prepared by homogenizing 2 times and 5 times the smallest width of the fibril was only 19 nm. Compared with homogenizing treatment the increase of ultrasonic treatment intensity energy consumption was more advantageous to improve the tensile strength and water vapor permeability of the nanopaper when process energy consumption was lower than 20 kwh moreover the nanopaper prepared by ultrasonic 2 h and 4 h showed better optical properties than homogenizing 2 times and 5 times the highest tensile strength and light transmittance of nanopaper was found by ultrasonic treatment 4 h which were MPa and % respectively and superior to the ordinary polymer film it was expected to be applied to the substrate of flexible display electronic devices. Key words homogeneous ultrasonic nanofibrillated cellulose nanopaper NCC NFC 100 nm NCC NFC CB B * papercg@ scut. edu. cn
2 5 INSTRON UV-1800 NFC Multimode8 6 Tsuguyuki Saito 7 Bruker TEMPO NFC NFC 88% 9 NFC MPa 1. 5% 1 mmol /g NaBr 0. 1 mmol /g TEMPO 8 mmol /g NaClO NaOH ph MPa 86. 9% ph NFC NFC 30 min NFC NFC TEMPO 1 1% TEMPO NFC TEMPO MPa D10 1 NFC NFC D Qin 11 TEMPO NFC 5 ~ 10 nm 100 ~ 400 nm Mishra 12 TEMPO NFC 2 h 4 h NFC NFC 2 4 NFC 3 D10 1 NFC 1% 2 h D NFC NFC 1 1 NFC NFC AgNO 3 NaOH NaBr NaClO TEMPO NFC DD2 DD5 2 1% TEMPO DD2 DD5 D 2 4 D10 1 D D10 1 D D h h h /kwh 5 g 25 g /m 2 NFC JB90-SH ph PHSJ kW NanoDeBEE Bluepard 1% NFC NFC XRD X D8ADVANCE X Bruker Instron China Pulp & Paper Vol. 35 No
3 NFC AFM NFC 1% NFC Bluehill Fukuzumi 3 mm 1 cm ~600 nm % TSY-T1H 38 ±1 90 ±2 % NFC NFC NFC TEMPO 1% NFC 0. 01% NFC 2 min 2 NFC JEOL-2100F NFC 3 2 A B D E 2 h 4 h 2 5 NFC 2 NFC 0. 2% 2 NFC VAC-V1 3 NFC 3 NFC 3 NFC
4 NFC 3 D E 3 E 2 h 4 h NFC 2. 2 DD2 NFC 3 A NFC 3 B NFC NFC 3 C NFC AFM 4 NFC AFM 5 13 NFC 10 ~ 50 nm 6 NFC A ~ E nm MPa 2 h 4 h 4 NFC NFC 116 MPa NFC MPa NFC X 5 NFC X NFC 8 5 a NFC I 5 b NFC 60% ~ 70% NFC 2 5 NFC % % 2 h 4 h NFC % % NFC 2 2 h kwh NFC 5 25 g /m 2 20 ~ 25 μm 4 NFC AFM NFC X 22 China Pulp & Paper Vol. 35 No
5 6 GPa NFC NFC 14 7 NFC 7 2 h 4 h 7 NFC h 2 h cm 3 / m 2 d Pa 2 h 4 h NFC NFC 15 2 h g / m 2 24 h NFC NFC
6 9 NFC 9 a 200 ~ 600 nm 200 ~ nm 400 nm 9 b 550 nm 87% ~ 90% % % 2 h 4 h % % h 4 h 2 h 4 h h 4 h 2 5 NFC 19 nm NFC 4 h NFC % kwh 4 h NFC MPa by TEMPO oxidation J. BioResource h 4h h % 1 Akira Isogai T S H F. TEMPO-oxidized cellulose nanofibers J. Nanoscale Eichhorn S J Dufresne A Aranguren M et al. Review current international research into cellulose nanofibres and nanocomposites J. Journal of Materials Science DONG Feng-xia LIU Wen LIU Hong-feng. Preparation and Application of Nanocellulose J. China Pulp & Paper D. niversity J Yang Q Fukuzumi H Saito T et al. Transparent Cellulose Films WANG Jie HU Yun-chu XU Chen-hao et al. Controllable preparation and characterization of nanocellulosein size and shape J. Journal of Central South University of Forestry & Technology J YAO Wen-run XU Qing-hua. Research Development of Nano-cellulose Preparation J. Paper and Paper Making J. 6 DENG Yu BAI Wei HE Xiao et al. Performance and Preparation of Transparent Nanofiber Paper J. Journal of Cellulose Science and Technology J Saito T Kuramae R Wohlert J et al. An Ultrastrong Nanofibrillar Biomaterial the Strength of Single Cellulose Nanofibrils Revealed via Sonication-induced Fragmentation J. Biomacromolecules Zhu Sai-ling LI Mu-zi XIONG Xue-ping et al. Preparation and Characterization of Nano-cellulose from Coconut Litter and Its High-strength Transparent Film J. Packaging Engineering J HU Yue LI Da-gang XU Li et al. The Preparation and Properties of High Strength Transparent Nano Cellulose Film J. Journal of Cellulose Science and Technology J DONG Feng-xia LIU Wen CHEN Xue-feng et al. Preparation of Nanocellulose by Using 4-Acetamido-TEMPO Oxidizing System and Ultrasonic Treatment J. China Pulp & Paper TEMPO J Qin Zhong-Yan Tong Gou-lin Frimle Chin Y C et al. Preparation of ultrasonicassisted high carboxylate content cellulose nanocrystals 12 Shree P Mishra J T A M. Ultrasound-catalyzed TEMPO-mediated Oxidation of Native Cellulose for the Production of Nanocellulose Effect of Process Variables J. BioResource Wu C Saito T Fujisawa S et al. Ultrastrong and High Gas-barrier Nanocellulose /Clay-layered Composites J. Biomacromolecules Sirvi J A Kolehmainen A Visanko M et al. Strong Self-standing Oxygen Barrier Films from Nanocelluloses Modified with Regioselective Oxidative Treatments J. ACS Applied Materials & Interfaces LI Wei. Preparation and Properties of Nanocrystalline Cellulose via Ultrasonication Assisted Method D. Harbin Northeast Forestry U- with High Gas Barrier Properties Fabricated from Aqueous Alkali / U- rea Solutions J. Biomacromolecules CPP ( : ) 24 China Pulp & Paper Vol. 35 No
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