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Mini-Review Acta Microbiologica Sinica 52 2 146-151 4 February 2012 ISSN 0001-6209 CN 11-1995 /Q http / /journals. im. ac. cn /actamicrocn 2 2 1* 1 400715 2 400716 200 HIV Q935 A 0001-6209 2012 02-0146-06 Tuberculosis TB Mycobacterium tuberculosis MTB 800 200 1 /3 1 HIV 4 1-2 Mycolic acid mycolate Stodola 1938 3 2012ZX10003-003 81071316 * Tel + 86-23-68367108 E-mail georgex@ swu. edu. cn 1975 - E-mail hongli75@ swu. edu. cn 2011-09-27 2011-11-07

. / 2012 52 2 147 1 7 Corynebacterium - C 38 Nocardia C 40 - C 60 α- β- Mycobacterium C 70 - C 90 5 3 α- α-mycolic acid methoxy- 6 mycolic acid keto-mycolic acid 1 1 C 20 Fig. 1 1 Molecular structures of mycolic acids. There are three types of mycolic acids in Mycobacterium tuberculosis illustrated with α-mycolic acid methoxy-mycolic acid and keto-mycolic acid. 3 α- 70% 10% - 15% FAS-Ⅰ 1 FAS-Ⅱ FAS-Ⅰ α- FAS-Ⅱ C 20 -S-CoA claisen-type C 26 -S-CoA FAS-Ⅱ FAS-ⅡA FAS-Ⅱ FAS-ⅡB 8 A 2 1 A 2 FAS-Ⅰ C 20 -S-CoA C 26 -S-CoA FAS-Ⅱ α- C 20 -S-CoA -S-CoA C 56-64 C 24-26 ACP FabD β-ketoacyl-acp Ⅲ

148 Hongli Luo et al. /Acta Microbiologica Sinica 2012 52 2 FabH β-ketoacyl-acp MabA β- methoxy- hydroxyacyl-acp HadABC 2-trans-enoyl- ACP EchA10 /11 C 20 C 22 meroacyl-s-acp keto-meroacyl-s-acp 3 FadD32 FAS-Ⅱ A FabD β-ketoacyl-acp fatty acyl-amp α- methoxy- KasA MabA β-hydroxyacyl-acp keto-meroacyl-s-acp meroacyl-amp HadABC 2-trans-enoyl-ACP InhA C 26 -S-CoA FAS-Ⅰ AccD4 5 C 32 FAS-Ⅱ AccD5 acyl-coa 2-carboxyl-C 26 - FabD KasA /B MabA β-hydroxyacyl-acp S-CoA meroacyl-amp 2-carboxyl-C 26 -S-CoA HadABC EchA10 /11 Pks13 13 FAS-ⅡB FAS-Ⅱ C 34 KasB 2 Pks13 KasA C 50 MmaA2 5 PPB N /C-terminal phosphopantetheinebingding KS ketoacyl-synthase PcaA α-meroacyl-s-acp AT acyltransferase α-meroacyl-s-acp TE thioesterase 5 MmaA4 MmaA1 MmaA3 MmaA2 CmaA2 MmaA4 MmaA1 MmaA2 CmaA2 Redox 1 Fig. 2 2 Biosynthesis pathway of Mycobacterium tuberculosis mycolic acid and well-characterized antibiotics targets. 3 Rv2989 fabd lsr2

. / 2012 52 2 149 Table 1 1 Enzymes and corresponding genes involved in the biosynthesis of Mycobacterium tuberculosis mycolic acid System or step Gene Enzyme Sanger identification FAS-Ⅰ Fas Fatty acid synthetase-Ⅰ Rv2524c FAS-Ⅰto FAS-Ⅱ FabD Malonyl-CoA ACP transacylase Rv2243 acpm Acyl carrier protein Rv2244 fabh β-ketoacyl-acp synthase Ⅲ Rv0533c FAS-Ⅱ KasA / B β-ketoacyl-acp synthase Rv2245 /2246 MabA β-ketoacyl-acp reductase Rv1483 echa10 /11 2-trans-Enoly-ACP isomerase Rv1142c /1141c inha 2-trans-Enoly-ACP reductase Rv1484 Methyltransferases mmaa1 mmaa2 MmaA1 MmaA2 Rv0645c Rv0644c mmaa3 mmaa4 MmaA3 MmaA4 Rv0643c Rv0642c cmaa2 pcaa CmaA2 PcaA Rv0503c Rv0470c Claisen-type condensation accd4 /5 Acyl-CoA carboxylase Rv3799c /3280 fadd32 pks13 Fatty acyl-amp ligase Polyketide synthase-13 Rv3801c /3800c FAS-Ⅱ 2 fabd-acpm-kasa-kasb-accd6 maba-inha 9 fabd Rv2242 MabR for Mycolic acid biosynthesis Regulator EMSA TSS FAS-Ⅱ 10 FAS-Ⅰ 85 Antigen 85 complex Ag85A Ag85B Ag85C InhA FAS-Ⅱ fbpa fbpb fbpc 15 16-5- 4- -substituted peperazines InhA Genz-8575 TDM Rv2327 MabR 17 KAS fbpa fbpc fbpa fbpc 17 11 STPKs STPKs fbpa fbpc 11 FAS-Ⅰ C 26 -S-CoA / STPKs FAS-Ⅱ FabH KasA KasB STPKs C 26 -S-CoA STPKs 12 2010 Romain STPKs MabA MabA MabA 13 4 14 FAS-Ⅱ 18

150 Hongli Luo et al. /Acta Microbiologica Sinica 2012 52 2 biosynthesis and sites of drug action. Current Opinion in Chemical Biology 1997 1 4 579-588. 7 Daffe M Draper P. The envelope layers of mycobacteria with reference to their pathogenicity. Advances in Microbial Physiology 1997 39 131-203. 8 Yuan Y Lee RE Besra GS Belisle JT Barry CE. Identification of a gene involved in the biosynthesis of cyclopropanated mycolic acids in Mycobacterium tuberculosis. Proceedings of National Academy of Sciences USA 1995 92 14 6630-6634. 9 Cole ST Brosch R Parkhill J Garnier T Churcher C Harris D Gordon SV Eiglmeier K Gas S Barry CE Tekaia F Badcock K Basham D Brown D Chillingworth T Connor R Davies R Devlin K Feltwell T Gentles S Hamlin N Holroyd S Hornsby T Jagels K Krogh A Mclean J Moule S Murphy L Oliver K Osborne J Quail MA Rajandream MA Rogers J Rutter S Seeger K Skelton J Squares R Squares S Sulston JE Taylor K Whitehead S Barrell BG. Deciphering the biology of Mycobacterium tuberculosis from the complete genome sequence. Nature 1998 393 537-544. 10 Salzman V Mondino S Sala C Cole ST Gago G Gramajo H. Transcriptional regulation of lipid homeostasis in mycobacteria. Molecular Microbiology 2010 78 1 64-77. 11 Romero IC Mehaffy C Burchmore RJ Dobos-Elder K Brennan P Walker J. Identification of promoter-binding 1 Takayama K Wang C Besra GS. Pathway to synthesis proteins of the fbp A and C genes in Mycobacterium and processing of mycolic acids in mycobacterium tuberculosis. Tuberculosis 2010 90 1 25-30. tuberculosis. Clinical Microbiology Review 2005 18 12 Veyron-Churlet R Molle V Taylor RC Brown AK 1 81-101. Besra GS Zanella-Cleon I Futterer K Kremer L. The 2.. Mycobacterium tuberculosis _ β-ketoacyl-acyl carrier Chinese Journal of Antituberculosis 2010 32 7 protein synthase Ⅲ activity is inhibited by 397-402. phosphorylation on a single threonine residue. The 3 Stodola FH Lesuk A Anderson RJ. The chemistry of Journal of Biological Chemistry 2009 284 10 6414- the lipids of tubercle bacilli. LIV. The isolation and 6424. properties of mycolic acid. The Journal of Biological 13 Veyron-Churlet R Zanella-Cleon I Cohen-Gonsaud M Chemistry. 1938 126 505-513. Molle V Krener L. Phosphorylation of the 4 Banerjee R Vats P Dahale S Kasibhatla SM Joshi R. Comparative genomics of cell envelope components in mycobacterium tuberculosis β-ketoacyl-acyl carrier protein reductase MabA regulates mycolic acid biosynthesis. The mycobacteria. PLoS One 2011 6 5 e19280. Journal of Biological Chemistry 2010 285 17 5 Asselineau J Lederer E. Structure of the mycolic acids of mycobacteria. Nature 1950 166 782-783. 12714-12725. 14 Gao LY Laval F Lawson EH Groger RK Woodruff 6 Chatterjee D. The mycobacterial cell wall structure A Morisaki JH Cox JS Daffe M Brown EJ. Requirement for kasb in Mycobacterium mycolic acid biosynthesis cell wall impermeability and intracellular survival implications for therapy. Molecular Microbiology 2003 49 6 1547-1563. 15 Vilcheze C Moribidoni HR Weisbrod TR Iwamoto H Kuo M Sacchettini JC Jacobs WR. Inactivation of the inha-encoded fatty acid synthase II FASII enoyl-acyl carrier protein reductase induces accumulation of the FASI end products and cell lysis of Mycobacterium smegmatis. Journal of Bacteriology 2000 182 14 4059-4067. 16 Marrakchi H Laneelle G Quemard A. InhA a target of the antituberculous drug isoniazid is involved in a mycobacterial fatty acid elongation system FAS-II. Microbiology 2000 146 2 289-296. 17 Ballell L Field RA Duncan K Young RJ. New smallmolecule synthetic antimycobacterials. Antimicrobial agents and chemotherapy 2005 49 6 2153-2163. 18 Wehenkel A Bellinzoni M Grana M Duran R Villarino A Fernandez P Andre-Leroux G England P Takiff H Cervenansky C Cole ST Alzari PM. Mycobacterial Ser /Thr protein kinases and phosphatases Physiological roles and therapeutic potential. Biochimica et Biophysica Acta 2008 1784 1 193-202.

. / 2012 52 2 151 Biosynthesis and regulation of mycolic acids in mycobacterium tuberculosis A review Hongli Luo 2 Lei Pang 2 Jianping Xie 1* 1 Institute of Modern Biopharmaceuticals State Key Laboratory Breeding Base of Eco-Environment and Bio-Resource of the Three Gorges Area School of Life Sciences Southwest University Chongqing 400715 China 2 College of Pharmaceutical Sciences Southwest University Chongqing 400716 China Abstract Tuberculosis TB is one of the world s deadliest diseases. Approximately eight million individuals develop active tuberculosis annually and two million die of tuberculosis. The emergence of multi-drug resistance strains HIV coinfection and an increasing aging population further worsen this scenario. Mycolic acids MAs also mycolate are integral cell wall components of Mycobacterium tuberculosis other mycobacterium and most actinomycetes engaging in the remarkable survival ability of Mycobacterium tuberculosis within infected hosts virulence and evasion of immunity. The biosynthesis and regulation of mycolic acids are rife with anti-tuberculosis drug targets. First-line tuberculosis drugs such as isoniazid and ethambutol target this pathway. In-depth investigation of this aspect will provide more opportunities to find better measures to combat tuberculosis. To this end we reviewed the structures classification biosynthesis pathway regulation factors in pathway of mycolic acid as well as promising drug targets. Keywords Mycobacterium tuberculosis mycolic acids biosynthesis regulation drug targets Supported by the National Megprojects for Key Infectious Disease 2012ZX10003-003 and by the National Natural Science Foundation of China 81071316. * Corresponding author. Tel + 86-23-68367108 E-mail georgex@ swu. edu. cn Received 27 September 2011 /Revise 7 November 2011 檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶檶 1953 2008 1 http / /journals. im. ac. cn / actamicrocn 2012 2 1953-1956 1-4 1-2 1957-1958 5-6 1-4 1959 7 1-2 1959-1962 3 1962 8 3-4 1963-1965 9-11 1-4 1966 12 1-2 1966-1972 6 1973-1988 13-28 1-4 1989-2007 29-47 1-6 2008-2011 48-51 1-12 2012 52 2