Available online at
|
|
|
- Νέφθυς Αγάθη Μαυρογένης
- 6 χρόνια πριν
- Προβολές:
Transcript
1 J. Serb. Chem. Soc. 76 (12) S1 S5 (2011) Supplementary material SUPPLEMENTARY MATERIAL TO Synthesis of quinoline-attached furan-2(3h)-ones having anti-inflammatory and antibacterial properties with reduced gastro-intestinal toxicity and lipid peroxidation MOHAMMAD M. ALAM 1 *, DEBA PRIYA SARKAR 1, ASIF HUSAIN 1, AKRANTH MARELLA 1, MOHAMMAD SHAQUIQUZZAMAN 1, MYMOONA AKHTER 1, MOHAMMAD SHAHARYAR 1, OZAIR ALAM 1 and FAIZUL AZAM 2 1 Department of Pharmaceutical Chemistry, Faculty of Pharmacy, Jamia Hamdard (Hamdard University), New Delhi , India and 2 Department of Medicinal Chemistry, Faculty of Pharmacy, Seventh of October University, P. O. Box 2247, Misurata, Libya J. Serb. Chem. Soc. 76 (12) (2011) ANALYTICAL AND SPECTRAL DATA OF THE SYNTHESIZED COMPOUNDS The splitting pattern abbreviations for the NMR signals are as follows: s, singlet; d, doublet; dd, double doublet; t, triplet; q, quartet; m, multiplet. 3-[(2-Chloroquinolin-3-yl)methylene]-5-phenyl furan-2(3h)-one (3a). Yield: 52 %; R f 0.72; m.p. 136 C; Anal. Calcd. for C 20 H 12 ClNO 2 : C, 71.97; H, 3.62; N, 4.20 %. Found: C, 71.93; H, 3.61; N, 4.21 %; IR (KBr, cm 1 ): 1740 (lactone C=O), 1560 (ArC=C), 1070 (ArC N), 864 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 6.84 (1H, s, βh), (5H, m, H-2,3,4,5,6, phenyl ring), 7.43 (2H, m, H-5,7, quinoline ring), 7.68 (1H, t, J = 7.3 Hz, H-6, quinoline ring), 7.92 (1H, m, H-8, quinoline ring), 8.28 (1H, s, H-4, quinoline ring), 8.38 (1H, s, olefinic H); 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 98.86, , , , , , , , , , , , , , , , , ; MS (m/z): 334 (M + ), 336 (M+2). 3-[(2,6-Dichloroquinolin-3-yl)methylene]-5-phenyl furan-2(3h)-one (3b). Yield: 56 %; R f : 0.74; m.p. 184 C; Anal. Calcd. for C 20 H 11 Cl 2 NO 2 : C, ; H, 3.01; N, 3.80 %. Found: C, 65.12; H, 3.02; N, 3.81 %; IR (KBr, cm 1 ): 1740 (lactone C=O), 1562 (ArC=C), 1068 (ArC N), 822 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 6.60 (1H, s, βh), (5H, m, H-2,3,4,5,6, phenyl ring), 7.62 (1H, d, J = 1.9 Hz, H-5, quinoline ring), 7.68 (1H, dd, J = 8.6, 1.9Hz, H-7, quinoline ring), 7.80 (1H, d, J = 8.5 Hz, H-8, quinoline ring), 7.94 (1H, s, H-4, quinoline ring), 8.24 (1H, s, olefinic H); 13 C-NMR (100 MHz, CDCl 3, δ / / ppm): 99.04, , , , , , , , , * Corresponding author. drmmalam@gmail.com S1
2 S2 FATIMA et al , , , , , , , ; MS (m/z): 368 (M + ), 370 (M+2). 3-[(2-Chloro-6-methoxyquinolin-3-yl)methylene]-5-phenyl furan-2(3h)-one (3c). Yield: 64 %; R f : 0.82; m.p. 154 C; Anal. Calcd. for C 21 H 14 ClNO 3 : C, ; H, 3.88; N, 3.85 %. Found: C, 69.58; H, 3.87; N, 3.86 %; IR (KBr, cm 1 ): 1740 (lactone C=O), 1562 (ArC=C), 1066 (ArC N), 816 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 3.86 (3H, s, OCH 3 ), 6.62 (1H, s, βh), (5H, m, H-2,3,4,5,6, phenyl ring), 7.54 (1H, d, J = 1.8 Hz, H-5, quinoline ring), 7.60 (1H, dd, J = 8.0, 1.8 Hz, H-7, quinoline ring), 7.72 (1H, d, J = 8.0 Hz, H-8, quinoline ring), 7.92 (1H, s, H-4, quinoline ring), 8.02 (1H, s, olefinic H); 13 C- -NMR (100 MHz, CDCl 3, δ / ppm): 55.56, 98.93, , , , , , , , , , , , , , , , ; MS (m/z): 364 (M + ), 366 (M+2). 3-[(2-Chloro-6-methylquinolin-3-yl)methylene]-5-phenyl furan-2(3h)-one (3d). Yield: 64 %; R f : 0.80; m.p. 176 C; Anal. Calcd. for C 21 H 14 ClNO 2 : C, ; H, 4.06; N, 4.03 %. Found: C, 72.53; H, 4.07; N, 4.01 %; IR (KBr, cm 1 ): 1740 (lactone C=O), 1558 (ArC=C), 1062 (ArC N), 810 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.15 (3H, s, CH 3 ), 6.88 (1H, s, βh), (5H, m, H-2,3,4,5,6, phenyl ring), 7.49 (1H, d, J = 1.6 Hz, H-5, quinoline ring), 7.56 (1H, dd, J = 7.8, 1.6 Hz, H-7, quinoline ring), 7.84 (1H, d, J = 7.8 Hz, H-8, quinoline ring), 8.26 (1H, s, H-4, quinoline ring), 8.34 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.06, , , , , , , , , , , , , , , , , , ; MS (m/z): 348 (M + ), 350 (M+2). 3-[(2-Chloroquinolin-3-yl)methylene]-5-(4-methylphenyl) furan-2(3h)-one (3e). Yield: 34 %; R f : 0.89; m.p. 204 C; Anal. Calcd. for C 21 H 14 ClNO 2 : C, ; H, 4.06; N, 4.03 %. Found: C, 72.33; H, 4.05; N, 4.03 %; IR (KBr, cm 1 ): 1742 (lactone C=O), 1562 (ArC=C), 1066 (ArC N), 812 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.18 (3H, s, CH 3 ), 6.84 (1H, s, βh), 7.20 (2H, d, J = = 8.3 Hz, H-3,5, phenyl ring), 7.39 (2H, d, J = 8.2 Hz, H-2,6, phenyl ring), 7.46 (2H, m, H-5,7, quinoline ring), 7.70 (2H, m, H-6,8, quinoline ring), 8.18 (1H, s, H-4, quinoline ring), 8.38 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / / ppm): 21.14, , , , , , , , , , , , , , , , , , ; MS (m/z): 348 (M + ), 350 (M+2). 3-[(2,6-Dichloroquinolin-3-yl)methylene]-5-(4-methylphenyl) furan-2(3h)-one (3f). Yield: 32 %; R f : 0.9; m.p. 264 C; Anal. Calcd. for C 21 H 13 Cl 2 NO 2 : C, ; H, 3.43; N, 3.66 %. Found: C, 65.88; H, 3.42; N, 3.64 %; IR (KBr, cm 1 ): 1744 (lactone C=O), 1562 (ArC=C), 1064 (ArC N), 822 (ArC H); 1 H-NMR NMR (400 MHz, CDCl 3, δ / ppm): 2.22 (3H, s, CH 3 ), 6.77 (1H, s, βh), 7.25 (2H, d, J = 8.0 Hz, H-3,5, phenyl ring), 7.49 (2H, d, J = 8.0 Hz, H-2,6, phenyl ring),
3 SUPPLEMENTARY MATERIAL S (1H, d, J = 2.1 Hz, H-5, quinoline ring), 7.64 (1H, dd, J = 8.6, 2.1 Hz, H-7, quinoline ring), 7.84 (1H, d, J = 8.6 Hz, H-8, quinoline ring), 8.02 (1H, s, H-4, quinoline ring), 8.34 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.18, , , , , , , , , , , , , , , , , , ; MS (m/z): 382 (M + ), 384 (M+2). 3-[(2-Chloro-6-methoxyquinolin-3-yl)methylene]-5-(4-methylphenyl) furan- -2(3H)-one (3g). Yield: 48 %; R f : 0.82; m.p. 242 C; Anal. Calcd. for C 22 H 16 ClNO 3 : C, ; H, 4.27; N, 3.71 %. Found: C, 70.12; H, 4.28; N, 3.72 %; IR (KBr, cm 1 ): 1796 (lactone C=C), 1557 (ArC=C), 1060 (ArC N), 817 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.16 (3H, s, CH 3 ), 3.87 (3H, s, OCH 3 ), 6.85 (1H, s, βh), 7.21 (2H, d, J = 8.2 Hz, H-3,5, phenyl ring), 7.38 (2H, d, J = 8.1 Hz, H-2,6, phenyl ring), 7.32 (1H, d, J = 1.8 Hz, H-5, quinoline ring), 7.68 (1H, s, H-4, quinoline ring), 7.81 (1H, d, J = 8.1 Hz, H-7, quinoline ring), 8.26 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.16, 55.62, , , , , , , , , , , , , , , , , ; MS (m/z): 378 (M + ), 380 (M+2). 3-[(2-Chloro-6-methylquinolin-3-yl)methylene]-5-(4-methylphenyl) furan- -2(3H)-one (3h). Yield: 48 %; R f : 0.81; m.p. 190 C; Anal. Calcd. for C 22 H 16 ClNO 2 : C, 73.03; H, 4.46; N, 3.87 %. Found: C, 72.95; H, 4.45; N, 3.85 %; IR (KBr, cm 1 ): 1795 (lactone C=O), 1558 (ArC=C), 1062 (ArC N), 820 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.24 and 2.26 (6H, s, 2 CH 3 ), 6.63 (1H, s, βh), 7.28 (2H, d, J = 8 Hz, H-3,5, phenyl ring), 7.42 (2H, d, J = 8.1 Hz, H-2,6, phenyl ring), 7.53 (1H, d, J = 1.6 Hz, H-5, quinoline ring), 7.59 (1H, dd, J = 8.4, 1.6 Hz, H-7, quinoline ring), 7.74 (1H, d, J = 8.4 Hz, H-8, quinoline ring), 7.88 (1H, s, H-4, quinoline ring), 8.27 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.11, 21.29, , , , , , , , , , , , , , , , , , ; MS (m/z): 362 (M + ), 364 (M+2). 3-[(2-Chloroquinolin-3-yl)methylene]-5-(2,4-dimethylphenyl) furan-2(3h)-one (3i). Yield: 36 %; R f : 0.92; m.p. 138 C; Anal. Calcd. for C 22 H 16 ClNO 2 : C, 73.03; H, 4.46; N, 3.87 %. Found: C, 73.18; H, 4.45; N, 3.86 %; IR (KBr, cm 1 ): 1741 (lactone C=O), 1560 (ArC=C), 1064 (ArC N), 824 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.18 and 2.22 (6H, s, 2 x CH 3 ), 6.61 (1H, s, βh), (3H, m, H-3,5,6, phenyl ring), (5H, m, H-4,5,6,7,8, quinoline ring), 8.25 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.42, 22.19, , , , , , , , , , , , , , , , , , , ; MS (m/z): 362 (M + ), 364 (M+2).
4 S4 FATIMA et al. 3-[(2,6-Dichloroquinolin-3-yl)methylene]-5-(2,4-dimethylphenyl) furan- -2(3H)-one (3j). Yield: 42 %; R f : 0.87; m.p. 184 C; Anal. Calcd. for C 22 H 15 Cl 2 NO 2 : C, ; H, 3.82; N, 3.53 %. Found: C, 66.72; H, 3.80; N, 3.54 %; IR (KBr, cm 1 ): 1742 (lactone C=O), 1562 (ArC=C), 1062 (ArC N), 821 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.28 and 2.32 (6H, s, 2 x CH 3 ), 6.60 (1H, s, βh), 7.06 (1H, d, J = 1.5 Hz, H-3, phenyl ring), 7.14 (1H, dd, J = = 7.2, 1.5 Hz, H-5, phenyl ring), 7.32 (1H, d, J = 7.2 Hz, H-6, phenyl ring), 7.56 (1H, d, J = 1.7 Hz, H-5, quinoline ring), 7.62 (1H, dd, J = 7.4, 1.7 Hz, H-7, quinoline ring), 7.80 (1H, d, J = 7.4 Hz, H-8, quinoline ring), 8.10 (1H, s, H-4, quinoline ring), 8.28 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.49, 22.21, , , , , , , , , , , , , , , , , , , ; MS (m/z): 396 (M + ), 398 (M+2). 3-[(2-Chloro-6-methoxyquinolin-3-yl)methylene]-5-(2,4-dimethylphenyl) furan-2(3h)-one (3k). Yield: 36 %; R f : 0.92; m.p. 200 C; Anal. Calcd. for C 23 H 18 ClNO 3 : C, 70.50; H, 4.63; N, 3.57 %. Found: C, 70.66; H, 4.62; N, 3.58 %; IR (KBr, cm 1 ): 1756 (lactone C=O), 1612 (ArC=C), 1060 (ArC N), 818 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.28 and 2.34 (6H, s, 2 CH 3 ), 3.98 (3H, s, OCH 3 ), 6.62 (1H, s, βh), 6.96 (1H, d, J = 1.6 Hz, H-3, phenyl ring), 7.11 (1H, dd, J = 7.2, 1.6 Hz, H-5, phenyl ring), 7.26 (1H, d, J = 7.2 Hz, H-6, phenyl ring), 7.34 (1H, d, J = 1.8 Hz, H-5, quinoline ring), 7.52 (1H, dd, J = 7.7, 1.8 Hz, H-7, quinoline ring), 7.64 (1H, d, J = 7.6 Hz, H-8, quinoline ring), 7.72 (1H, s, H-4, quinoline ring), 8.26 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 21.45, 22.11, , , , , , , , , , , , , , , , , , , ; MS (m/z): 392 (M + ), 394 (M+2). 3-[(2-Chloro-6-methylquinolin-3-yl)methylene]-5-(2,4-dimethylphenyl) furan-2(3h)-one (3l). Yield: 32 %; R f : 0.91; m.p. 174 C; Anal. Calcd. for C 23 H 18 ClNO 2 : C, 73.50; H, 4.83; N, 3.73 %. Found: C, 73.53; H, 4.82; N, 3.72 %; IR (KBr, cm 1 ): 1755 (lactone C=O), 1610 (ArC=C), 1068 (ArC N), 824 (ArC H); 1 H-NMR: 2.20, 2.24 and 2.30 (9H, s, 3 CH 3 ), 6.60 (1H, s, βh), (3H, m, H-3,5,6, phenyl ring), 7.48 (1H, d, J = 1.7 Hz, H-5, quinoline ring), 7.56 (1H, dd, J = 7.8, 1.7 Hz, H-7, quinoline ring), 7.68 (1H, d, J = 7.7 Hz, H-8, quinoline ring), 7.78 (1H, s, H-4, quinoline ring), 8.28 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 20.98, 21.31, 21.84, , , , , , , , , , , , , , , , , , , ; MS (m/z): 376 (M + ), 378 (M+2). 5-(4-Bromophenyl)3-[(2-chloroquinolin-3-yl)methylene] furan-2(3h)-one (3m). Yield: 30 %; R f : 0.85; m.p. 216 C; Anal. Calcd. for C 20 H 11 BrClNO 2 : C, ; H, 2.69; N, 3.39 %. Found: C, 58.38; H, 2.70; N, 3.38 %; IR (KBr, cm 1 ): 1748
5 SUPPLEMENTARY MATERIAL S5 (lactone C=O), 1612 (ArC=C), 1062 (ArC N), 826 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 6.71 (1H, s, βh), 7.36 (2H, d, J = 8.8 Hz, H-3,5, phenyl ring), 7.48 (2H, d, J = 8.7 Hz, H-2,6, phenyl ring), (4H, m, H-5,6,7,8, quinoline ring), 8.08 (1H, s, H-4, quinoline ring), 8.16 (1H, s, olefinic H). 13 C- -NMR (100 MHz, CDCl 3, δ / ppm): 99.34, , , , , , , , , , , , , , , , ; MS (m/z): 413 (M + ), 415 (M+2). 5-(4-Bromophenyl)-3-[(2,6-dichloroquinolin-3-yl)methylene] furan-2(3h)-one (3n). Yield: 32 %; R f : 0.86; m.p. 156 C; Anal. Calcd. for C 20 H 10 BrCl 2 NO 2 : C, 53.73; H, 2.25; N, 3.13 %. Found: C, 53.62; H, 2.23; N, 3.12 %; IR (KBr, cm 1 ): 1750 (lactone C=O), 1580 (ArC=C), 1060 (ArC N), 818 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 6.60 (1H, s, βh), (7H, m, H-5,7,8 of quinoline ring merged with H-2,3,5,6 of phenyl ring), 8.04 (1H, s, H-4, quinoline ring), 8.21 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): , , , , , , , , , , , , , , , , ; MS (m/z): 447 (M + ), 449 (M+2). 5-(4-Bromophenyl)-3-[(2-chloro-6-methoxyquinolin-3-yl)methylene] furan- -2(3H)-one (3o). Yield: 38 %; R f : 0.89; m.p. 264 C; Anal. Calcd. for C 21 H 13 BrClNO 3 : C, 56.98; H, 2.96; N, 3.16 %. Found: C, 56.83; H, 2.97; N, 3.17 %; IR (KBr, cm 1 ): 1748 (lactone C=O), 1612 (ArC=C), 1064 (ArC N), 812 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 3.78 (1H, s, OCH 3 ), 6.64 (1H, s, βh), (7H, m, H-5,7,8 of quinoline ring merged with H-2,3,5,6 of phenyl ring), 7.94 (1H, s, H-4, quinoline ring), 8.08 (1H, s, olefinic H). 13 C- -NMR (100 MHz, CDCl 3, δ / ppm): 55.68, 99.14, , , , , , , , , , , , , , , , ; MS (m/z): 443 (M + ), 445 (M+2). 5-(4-Bromophenyl)-3-[(2-chloro-6-methylquinolin-3-yl)methylene] furan- -2(3H)-one (3p). Yield: 42 %; R f : 0.83; m.p. 174 C; Anal. Calcd. for C 21 H 13 BrClNO 2 : C, ; H, 3.07; N, 3.28 %. Found: C, 58.96; H, 3.08; N, 3.29 %; IR (KBr, cm 1 ): 1748 (lactone C=O), 1602 (ArC=C), 1066 (ArC N), 810 (ArC H); 1 H-NMR (400 MHz, CDCl 3, δ / ppm): 2.20 (1H, s, CH 3 ), 6.60 (1H, s, βh), 7.34 (2H, d, J = 8.6 Hz, H-3,5, phenyl ring), 7.44 (2H, d, J = 8.6 Hz, H-2,6, phenyl ring), 7.50 (1H, d, J = 1.9 Hz, H-5, quinoline ring), 7.60 (1H, dd, J = 8.3, 1.9 Hz, H-7, quinoline ring), 7.78 (1H, d, J = 8.4 Hz, H-8, quinoline ring), 7.96 (1H, s, H-4, quinoline ring), 8.21 (1H, s, olefinic H). 13 C-NMR (100 MHz, CDCl 3, δ / ppm): 20.93, 99.44, , , , , , , , , , , , , , , , ; MS (m/z): 427 (M + ), 429 (M+2).
Available online at shd.org.rs/jscs/
J. Serb. Chem. Soc. 78 (12) S131 S136 (2013) Supplementary material SUPPLEMENTARY MATERIAL TO New 9-aminoacridine derivatives as inhibitors of botulinum neurotoxins and P. falciparum malaria MIKLOŠ TOT
SUPPLEMENTARY MATERIAL
10.1071/CH16014_AC The Authors 2016 Australian Journal of Chemistry 2016, 69(9), 1049-1053 SUPPLEMENTARY MATERIAL A Green Approach for the Synthesis of Novel 7,11-Dihydro-6H-chromeno[3,4- e]isoxazolo[5,4-b]pyridin-6-one
Available online at shd.org.rs/jscs/
J. Serb. Chem. Soc. 78 (1) S1 S8 (2013) Supplementary material SUPPLEMENTARY MATERIAL TO Metal complexes of N'-[2-hydroxy-5-(phenyldiazenyl)- benzylidene]isonicotinohydrazide. Synthesis, spectroscopic
Copper-Catalyzed Oxidative Dehydrogenative N-N Bond. Formation for the Synthesis of N,N -Diarylindazol-3-ones
Electronic Supplementary Material (ESI) for Organic Chemistry Frontiers. This journal is the Partner Organisations 2016 Supporting information Copper-Catalyzed Oxidative Dehydrogenative - Bond Formation
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2006
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2006 A new route to enantiopure b-aryl-substituted b-amino acids and 4-aryl-substituted b-lactams through lipase-catalyzed
SUPPLEMENTARY MATERIAL. A Facile and Convenient Approach for the Synthesis of Novel Sesamol-Oxazine and Quinoline- Oxazine Hybrids
10.1071/CH17272_AC CSIRO 2017 Australian Journal of Chemistry 2017, 70(12), 1285-1290 SUPPLEMENTARY MATERIAL A Facile and Convenient Approach for the Synthesis of Novel Sesamol-Oxazine and Quinoline- Oxazine
Vilsmeier Haack reagent-promoted formyloxylation of α-chloro-narylacetamides
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 205 Vilsmeier aack reagent-promoted formyloxylation of α-chloro-arylacetamides by formamide Jiann-Jyh
The Free Internet Journal for Organic Chemistry
The Free Internet Journal for Organic Chemistry Paper Archive for Organic Chemistry Arkivoc 2018, part iii, S1-S6 Synthesis of dihydropyranones and dihydropyrano[2,3- d][1,3]dioxine-diones by cyclization
Supporting Information
Supporting Information for AgOTf-catalyzed one-pot reactions of 2-alkynylbenzaldoximes with α,β-unsaturated carbonyl compounds Qiuping Ding 1, Dan Wang 1, Puying Luo* 2, Meiling Liu 1, Shouzhi Pu* 3 and
Supporting Information
Supporting Information Ceric Ammonium Nitrate (CAN) catalyzed efficient one-pot three component aza-diels-alder reactions for a facile synthesis of tetrahydropyranoquinoline derivatives Ravinder Goud Puligoundla
Supporting Information
Supporting Information Montmorillonite KSF-Catalyzed One-pot, Three-component, Aza-Diels- Alder Reactions of Methylenecyclopropanes With Arylaldehydes and Aromatic Amines Li-Xiong Shao and Min Shi* General
Electronic Supplementary Information
Electronic Supplementary Information Unprecedented Carbon-Carbon Bond Cleavage in Nucleophilic Aziridine Ring Opening Reaction, Efficient Ring Transformation of Aziridines to Imidazolidin-4-ones Jin-Yuan
Supporting Information. Asymmetric Binary-acid Catalysis with Chiral. Phosphoric Acid and MgF 2 : Catalytic
Supporting Information Asymmetric Binary-acid Catalysis with Chiral Phosphoric Acid and MgF 2 : Catalytic Enantioselective Friedel-Crafts Reactions of β,γ- Unsaturated-α-Ketoesters Jian Lv, Xin Li, Long
Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via double C(sp 2 )-H thiolation
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Iodine-catalyzed synthesis of sulfur-bridged enaminones and chromones via
Supporting Information One-Pot Approach to Chiral Chromenes via Enantioselective Organocatalytic Domino Oxa-Michael-Aldol Reaction
Supporting Information ne-pot Approach to Chiral Chromenes via Enantioselective rganocatalytic Domino xa-michael-aldol Reaction Hao Li, Jian Wang, Timiyin E-Nunu, Liansuo Zu, Wei Jiang, Shaohua Wei, *
Supporting Information. for. A novel application of 2-silylated 1,3-dithiolanes for the. synthesis of aryl/hetaryl-substituted ethenes and
Supporting Information for A novel application of 2-silylated 1,3-dithiolanes for the synthesis of aryl/hetaryl-substituted ethenes and dibenzofulvenes Grzegorz Mlostoń *1, Paulina Pipiak 1, Róża Hamera-Fałdyga
Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic acids with the assistance of isocyanide
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 Copper-catalyzed formal O-H insertion reaction of α-diazo-1,3-dicarb- onyl compounds to carboxylic
Discovery of multi-target receptor tyrosine kinase inhibitors as novel anti-angiogenesis agents
Discovery of multi-target receptor tyrosine kinase inhibitors as novel anti-angiogenesis agents Jinfeng Wang, Lin Zhang, Xiaoyan Pan, Bingling Dai, Ying Sun, Chuansheng Li, Jie Zhang School of Pharmacy,
Supporting Information
Supporting Information Synthesis and Electroactive Properties of Poly(amidoamine) Dendrimers with an Aniline Pentamer Shell Wei-I Hung a, Chih-Bing Hung a, Ya-Han Chang a, Jiun-Kuang Dai a, Yan Li b, Hai
Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes
Supporting Information for Lewis Acid Catalyzed Propargylation of Arenes with O-Propargyl Trichloroacetimidate: Synthesis of 1,3-Diarylpropynes Changkun Li and Jianbo Wang* Beijing National Laboratory
A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2014 A facile and general route to 3-((trifluoromethyl)thio)benzofurans and 3-((trifluoromethyl)thio)benzothiophenes
Supporting Information
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2015 Synthesis of 3-omosubstituted Pyrroles via Palladium- Catalyzed Intermolecular Oxidative Cyclization
Supporting Information
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2017 Modular Synthesis of Propargylamine Modified Cyclodextrins by a Gold(III)-catalyzed Three Component
Eco-friendly synthesis of diverse and valuable 2-pyridones by catalyst- and solvent-free thermal multicomponent domino reaction
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2015 SUPPRTIG IFRMATI Eco-friendly synthesis of diverse and valuable 2-pyridones by catalyst-
Aluminium triflate as a Lewis acid catalyst for the ring opening of epoxides in alcohols
Aluminium triflate as a Lewis acid catalyst for the ring opening of epoxides in alcohols D. Bradley G. Williams* and Michelle Lawton a Department of Chemistry, University of Johannesburg, P.O. Box 524,
Efficient Synthesis of Ureas by Direct Palladium-Catalyzed. Oxidative Carbonylation of Amines
S1 Supporting Information for Efficient Synthesis of Ureas by Direct Palladium-Catalyzed Oxidative Carbonylation of Amines Bartolo Gabriele,*, Giuseppe Salerno, Raffaella Mancuso, and Mirco Costa Dipartimento
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%.
Supplementary Figure S1. Single X-ray structure 3a at probability ellipsoids of 20%. S1 Supplementary Figure S2. Single X-ray structure 5a at probability ellipsoids of 20%. S2 H 15 Ph Ac Ac I AcH Ph Ac
Site-Selective Suzuki-Miyaura Cross-Coupling Reactions of 2,3,4,5-Tetrabromofuran
1 Site-Selective Suzuki-Miyaura Cross-Coupling Reactions of 2,3,4,5-Tetrabromofuran Munawar Hussain, a Rasheed Ahmad Khera, a Nguyen Thai Hung, a Peter Langer* a,b a Institut für Chemie, Universität Rostock,
Supporting Information
Supporting Information for Lewis acid-catalyzed redox-neutral amination of 2-(3-pyrroline-1-yl)benzaldehydes via intramolecular [1,5]-hydride shift/isomerization reaction Chun-Huan Jiang, Xiantao Lei,
Ligand-free Cu(II)-mediated aerobic oxidations of aldehyde. hydrazones leading to N,N -diacylhydrazines and 1,3,4-oxadiazoles
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2017 Ligand-free Cu(II)-mediated aerobic oxidations of aldehyde hydrazones leading
Supporting Information. Synthesis and in vitro pharmacological evaluation of N-[(1-benzyl-1,2,3-triazol-4-
Supporting Information Synthesis and in vitro pharmacological evaluation of N-[(1-benzyl-1,2,3-triazol-4- yl)methyl]-carboxamides on D-secoestrone scaffolds Johanna Szabó a, Ildikó Bacsa a, János Wölfling
Rhodium-Catalyzed Oxidative Decarbonylative Heck-type Coupling of Aromatic Aldehydes with Terminal Alkenes
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2015 Electronic Supplementary Information Rhodium-Catalyzed Oxidative Decarbonylative Heck-type
Supporting information
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 204 Supporting information Palladium nanoparticles supported on triazine functionalised mesoporous
SUPPLEMENTARY DATA. Waste-to-useful: Biowaste-derived heterogeneous catalyst for a green and sustainable Henry reaction
Electronic Supplementary Material (ESI) for New Journal of Chemistry. This journal is The Royal Society of Chemistry and the Centre National de la Recherche Scientifique 209 SUPPLEMENTARY DATA Waste-to-useful:
Supporting Information
Electronic upplementary Material (EI) for Green Chemistry. This journal is The Royal ociety of Chemistry 204 upporting Information ynthesis of sulfonamides via I 2 -mediated reaction of sodium sulfinates
Divergent synthesis of various iminocyclitols from D-ribose
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 205 Divergent synthesis of various iminocyclitols from D-ribose Ramu Petakamsetty,
Supporting Information for Iron-catalyzed decarboxylative alkenylation of cycloalkanes with arylvinylic carboxylic acids via a radical process
Supporting Information for Iron-catalyzed decarboxylative alkenylation of cycloalkanes with arylvinylic carboxylic acids via a radical process Jincan Zhao 1, Hong Fang 1, Jianlin Han* 1,2 and Yi Pan* 1
Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3
Supporting Information Direct Transformation of Ethylarenes into Primary Aromatic Amides with N-Bromosuccinimide and I 2 -aq NH 3 Shohei Shimokawa, Yuhsuke Kawagoe, Katsuhiko Moriyama, Hideo Togo* Graduate
Supporting Information. A catalyst-free multicomponent domino sequence for the. diastereoselective synthesis of (E)-3-[2-arylcarbonyl-3-
Supporting Information for A catalyst-free multicomponent domino sequence for the diastereoselective synthesis of (E)-3-[2-arylcarbonyl-3- (arylamino)allyl]chromen-4-ones Pitchaimani Prasanna 1, Pethaiah
Supplementary information
Electronic Supplementary Material (ESI) for MedChemComm. This journal is The Royal Society of Chemistry 2015 Supplementary information Synthesis of carboxyimidamide-substituted benzo[c][1,2,5]oxadiazoles
Supporting Information
Supporting Information Copper/Silver Cocatalyzed Oxidative Coupling of Vinylarenes with ICH 2 CF 3 or ICH 2 CHF 2 Leading to β-cf 3 /CHF 2 -Substituted Ketones Niannian Yi, Hao Zhang, Chonghui Xu, Wei
multicomponent synthesis of 5-amino-4-
Supporting Informartion for Molecular iodine-catalyzed one-pot multicomponent synthesis of 5-amino-4- (arylselanyl)-1h-pyrazoles Camila S. Pires 1, Daniela H. de Oliveira 1, Maria R. B. Pontel 1, Jean
Synthesis of novel 1,2,3-triazolyl derivatives of pregnane, androstane and D-homoandrostane. Tandem Click reaction/cu-catalyzed D-homo rearrangement
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information Synthesis of novel 1,2,3-triazolyl derivatives of
Electronic Supplementary Information
Electronic Supplementary Information NbCl 3 -catalyzed [2+2+2] intermolecular cycloaddition of alkynes and alkenes to 1,3-cyclohexadiene derivatives Yasushi Obora,* Keisuke Takeshita and Yasutaka Ishii*
Supporting information
Supporting information Spectroscopic data of compounds 1a-f Benzyl bromide (1a) Yield: 81%. Colorless oil. b.p. 79-82 o C/15 mmhg (Lit. 83.5 84 o C/13 mmhg). 1 1 H NMR (CDCl 3 ): δ 4.45 (2H, s, PhCH 2
D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical and experimental study
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 D-Glucosamine-derived copper catalyst for Ullmann-type C- N coupling reaction: theoretical
Supporting Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2018 Supporting Information Silver or Cerium-Promoted Free Radical Cascade Difunctionalization
Copper-mediated radical cross-coupling reaction of 2,2-dichloro-1,1,1-trifluoroethane (HCFC-123) with phenols or thiophenols. Support Information
Copper-mediated radical cross-coupling reaction of 2,2-dichloro-1,1,1-trifluoroethane (HCFC-123) with phenols or thiophenols Dr. Xiao un Tang and Prof. Qing un Chen* Key Laboratory of Organofluorine Chemistry,
phase: synthesis of biaryls, terphenyls and polyaryls
Supporting Information for Studies on Pd/NiFe 2 O 4 catalyzed ligand-free Suzuki reaction in aqueous phase: synthesis of biaryls, terphenyls and polyaryls Sanjay R. Borhade and Suresh B. Waghmode* Address:
First Total Synthesis of Antimitotic Compound, (+)-Phomopsidin
First Total Synthesis of Antimitotic Compound, (+)-Phomopsidin Takahiro Suzuki, a Kenji Usui, a Yoshiharu Miyake, a Michio Namikoshi, b and Masahisa Nakada a, * a Department of Chemistry, School of Science
3018 Σύνθεση του 3-φαινυλοβενζοϊκού οξέος από 3-ιωδο βενζοϊκό οξύ
3018 Σύνθεση του 3-φαινυλοβενζοϊκού οξέος από 3-ιωδο βενζοϊκό οξύ COOH COOH + PhB(OH) 2 NaOH/PdCl 2 I Ph C 7 H 5 IO 2 (248.0) C 6 H 7 BO 2 (121.9) NaOH PdCl 2 (40.0) (177.3) C 13 H 10 O 2 (198.2) Βιβλιογραφία
Supporting Information. Synthesis and biological evaluation of 2,3-Bis(het)aryl-4-azaindoles Derivatives as protein kinases inhibitors
Supporting Information Synthesis and biological evaluation of 2,3-Bis(het)aryl-4-azaindoles Derivatives as protein kinases inhibitors Frédéric Pin, a Frédéric Buron, a Fabienne Saab, a Lionel Colliandre,
Supporting Information
Supporting Information Selective Synthesis of xygen-containing Heterocycles via Tandem Reactions of 1,2-Allenic Ketones with Ethyl 4-Chloroacetoacetate Qiang Wang, a, b Zhouqing Xu b and Xuesen Fan a *
Rh(III)-Catalyzed C-H Amidation with N-hydroxycarbamates: A. new Entry to N-Carbamate Protected Arylamines
Rh(III)-Catalyzed C-H Amidation with N-hydroxycarbamates: A new Entry to N-Carbamate Protected Arylamines Bing Zhou,* Juanjuan Du, Yaxi Yang,* Huijin Feng, Yuanchao Li Shanghai Institute of Materia Medica,
Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information
![Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information](/thumbs/64/50937700.jpg "Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans. Supporting Information")
Novel and Selective Palladium-Catalyzed Annulation of 2-Alkynylphenols to Form 2-Substituted 3-Halobenzo[b]furans Liang Yun, Shi Tang, Xu-Dong Zhang, Li-Qiu Mao, Ye-Xiang Xie and Jin-Heng Li* Key Laboratory
Supporting Information
Supporting Information Nano WO3-supported sulfonic acid: New, efficient and high recyclable heterogeneous nano catalyst Ali Amoozadeh* and Salman Rahmani* Department of Chemistry, Semnan University, Semnan,
Facile construction of the functionalized 4H-chromene via tandem. benzylation and cyclization. Jinmin Fan and Zhiyong Wang*
Facile construction of the functionalized 4H-chromene via tandem benzylation and cyclization Jinmin Fan and Zhiyong Wang* Hefei National Laboratory for Physical Science at Microscale, Joint- Lab of Green
Supplementary Material (ESI) for Organic & Biomolecular Chemistry This journal is (c) The Royal Society of Chemistry 2008
Palladium(0)-catalyzed direct cross-coupling reaction of allylic alcohols with aryland alkenylboronic acids Hirokazu Tsukamoto, Tomomi Uchiyama, Takamichi Suzuki and Yoshinori Kondo Graduate School of
Supporting Information
Supporting Information Regioselective Reversal in the Cyclization of 2-Diazo-3,5-dioxo-6-ynoates (ynones, ynamide): Construction of -Pyrones and 3(2H)-Furanones Starting from Identical Materials Feng Wang,
Direct Palladium-Catalyzed Arylations of Aryl Bromides. with 2/9-Substituted Pyrimido[5,4-b]indolizines
![Direct Palladium-Catalyzed Arylations of Aryl Bromides. with 2/9-Substituted Pyrimido[5,4-b]indolizines](/thumbs/87/95187440.jpg "Direct Palladium-Catalyzed Arylations of Aryl Bromides. with 2/9-Substituted Pyrimido[5,4-b]indolizines")
Direct Palladium-Catalyzed Arylations of Aryl Bromides with 2/9-Substituted Pyrimido[5,4-b]indolizines Min Jiang, Ting Li, Linghua Meng, Chunhao Yang,* Yuyuan Xie*, and Jian Ding State Key Laboratory of
New Cytotoxic Constituents from the Red Sea Soft Coral Nephthea sp.
SUPPLEMENTARY MATERIAL New Cytotoxic Constituents from the Red Sea Soft Coral Nephthea sp. Mohamed-Elamir F. Hegazy a,*, Amira M. Gamal-Eldeen b, Tarik A. Mohamed a, Montaser A. Alhammady c, Abuzeid A.
Supporting Information. Synthesis and biological evaluation of nojirimycin- and
Supporting Information for Synthesis and biological evaluation of nojirimycin- and pyrrolidine-based trehalase inhibitors Davide Bini 1, Francesca Cardona 2, Matilde Forcella 1, Camilla Parmeggiani 2,3,
Regioselectivity in the Stille coupling reactions of 3,5- dibromo-2-pyrone.
Regioselectivity in the Stille coupling reactions of 3,5- dibromo-2-pyrone. Won-Suk Kim, Hyung-Jin Kim and Cheon-Gyu Cho Department of Chemistry, Hanyang University, Seoul 133-791, Korea Experimental Section
Supporting Materials
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2016 Carbonylative Coupling of Aryl Tosylates/triflates with Arylboronic Acids under CO Atmosphere
Supporting Information
Supporting Information Direct Olefination of Alcohols with Sulfones by Using Heterogeneous Platinum Catalysts S. M. A. Hakim Siddiki, [a] Abeda Sultana Touchy, [b] Kenichi Kon, [b] [a, b] and Ken-ichi
Supporting Information. Experimental section
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting Information Experimental section General. Anhydrous solvents were transferred by
Supplementary Information for
Supplementary Information for Organocatalytic Asymmetric Intramolecular [3+2] Cycloaddition: A Straightforward Approach to Access Multiply Substituted Hexahydrochromeno[4,3-b]pyrrolidine Derivatives in
Selective mono reduction of bisphosphine
Griffith Research Online https://research-repository.griffith.edu.au Selective mono reduction of bisphosphine oxides under mild conditions Author etersson, Maria, Loughlin, Wendy, Jenkins, Ian ublished
Supporting Information
Supporting Information Wiley-VCH 2008 69451 Weinheim, Germany Ligand-Free Pd-Catalyzed Highly Selective Arylation of Allylic Esters with Retention of the Traditional Leaving Group (Supporting Information)
Supporting Information
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2014 Supporting Information Facile diverted synthesis of pyrrolidinyl triazoles
Supporting information
Electronic upplementary Material (EI) for New Journal of Chemistry. This journal is The Royal ociety of Chemistry and the Centre National de la Recherche cientifique 7 upporting information Lipase catalyzed,-addition
SUPPORTING INFORMATION. Polystyrene-immobilized DABCO as a highly efficient and recyclable organocatalyst for Knoevenagel condensation
Electronic Supplementary Material (ESI) for RSC Advances This journal is The Royal Society of Chemistry 213 SUPPORTING INFORMATION Polystyrene-immobilized DABCO as a highly efficient and recyclable organocatalyst
Aminofluorination of Fluorinated Alkenes
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2018 Synthesis of ɑ CF 3 and ɑ CF 2 H Amines via Aminofluorination of Fluorinated Alkenes Ling Yang,
Metal-free Oxidative Coupling of Amines with Sodium Sulfinates: A Mild Access to Sulfonamides
Electronic Supplementary Material (ESI) for RSC Advances. This journal is The Royal Society of Chemistry 2014 Supporting information for Metal-free Oxidative Coupling of Amines with Sodium Sulfinates:
Free Radical Initiated Coupling Reaction of Alcohols and. Alkynes: not C-O but C-C Bond Formation. Context. General information 2. Typical procedure 2
Free Radical Initiated Coupling Reaction of Alcohols and Alkynes: not C-O but C-C Bond Formation Zhongquan Liu,* Liang Sun, Jianguo Wang, Jie Han, Yankai Zhao, Bo Zhou Institute of Organic Chemistry, Gannan
Tributylphosphine-Catalyzed Cycloaddition of Aziridines with Carbon Disulfide and Isothiocyanate
upporting Information Tributylphosphine-Catalyzed Cycloaddition of Aziridines with Carbon Disulfide and Isothiocyanate Jing-Yu Wu, Zhi-Bin Luo, Li-Xin Dai and Xue-Long Hou* a tate Key Laboratory of Organometallic
ΚΕΦΑΛΑΙΟ ΕΝΑΤΟ ΑΝΑΛΥΣΗ ΚΑΙ ΕΡΜΗΝΕΙΑ ΦΑΣΜΑΤΩΝ 1 Η ΚΑΙ 13 C NMR. 9.1. Ονοματολογία Συστημάτων Spin
ΚΕΦΑΛΑΙΟ ΕΝΑΤΟ ΑΝΑΛΥΣΗ ΚΑΙ ΕΡΜΗΝΕΙΑ ΦΑΣΜΑΤΩΝ 1 Η ΚΑΙ 13 C NMR Στην εισαγωγή του Πυρηνικού Μαγνητικού Συντονισμού (κεφάλαιο 6) εξετάσθηκαν απλά φάσματα πρώτης-τάξης, όπου οι χημικές μετατοπίσεις και οι
First DMAP-mediated direct conversion of Morita Baylis. Hillman alcohols into γ-ketoallylphosphonates: Synthesis of
Supporting Information File 1 for First DMAP-mediated direct conversion of Morita Baylis Hillman alcohols into γ-ketoallylphosphonates: Synthesis of γ-aminoallylphosphonates Marwa Ayadi 1,2, Haitham Elleuch
Phenylpropanoids, Sesquiterpenoids and Flavonoids from Pimpinella tragium Vill. subsp. lithophila (Schischkin) Tutin
Supporting Information Rec. Nat. Prod. 10:2 (2016) 207-213 Phenylpropanoids, Sesquiterpenoids and Flavonoids from Pimpinella tragium Vill. subsp. lithophila (Schischkin) Tutin Hilal Özbek 1, Zühal Güvenalp
Room Temperature Highly Diastereoselective Zn-Mediated. Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled
Supporting Information for: Room Temperature Highly Diastereoselective Zn-Mediated Allylation of Chiral N-tert-Butanesulfinyl Imines: Remarkable Reaction Condition Controlled Stereoselectivity Reversal
Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/ bromides in water using oxone-kx(x= Cl or Br)
Electronic Supplementary Material (ESI) for Green Chemistry. This journal is The Royal Society of Chemistry 2014 Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/ bromides in water using
Supporting Information for Fe-Catalyzed Reductive Coupling of Unactivated Alkenes with. β-nitroalkenes. Contents. 1. General Information S2
Supporting Information for Fe-Catalyzed Reductive Coupling of Unactivated Alkenes with β-nitroalkenes Jing Zheng, Dahai Wang, and Sunliang Cui* College of Pharmaceutical Sciences, Zhejiang University,
Cu-catalyzed stereoselective conjugate addition of arylboronic acids to alkynoates
Cu-catalyzed stereoselective conjugate addition of arylboronic acids to alkynoates Yoshihiko Yamamoto,* Naohiro Kirai and Yu arada Department of Applied Chemistry, Graduate School of Science and Engineering,
Asymmetric Synthesis of New Chiral β-amino Acid Derivatives by Mannich-type Reactions of Chiral N- Sulfinyl Imidates with N-Tosyl Aldimines
Asymmetric Synthesis of New Chiral β-amino Acid Derivatives by Mannich-type Reactions of Chiral N- Sulfinyl Imidates with N-yl Aldimines Filip Colpaert, Sven Mangelinckx, and Norbert De Kimpe Department
Electronic Supplementary Information (ESI)
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry Electronic Supplementary Information (ESI) For Iron-Catalysed xidative Amidation of Alcohols with Amines Silvia Gaspa, a Andrea
Supporting Information. Direct Heptafluoroisopropylation of Arylboronic Acids via. Hexafluoropropene (HFP)
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 2015 Supporting Information Direct Heptafluoroisopropylation of Arylboronic Acids via Hexafluoropropene
Highly enantioselective cascade synthesis of spiropyrazolones. Supporting Information. NMR spectra and HPLC traces
Highly enantioselective cascade synthesis of spiropyrazolones Alex Zea a, Andrea-Nekane R. Alba a, Andrea Mazzanti b, Albert Moyano a and Ramon Rios a,c * Supporting Information NMR spectra and HPLC traces
Supporting Information
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2014 A Family of Click Nucleosides for Metal-Mediated Base Pairing: Unravelling the Principles of Highly Stabilizing Metal-Mediated
Supporting Information
Supporting Information Lewis acid catalyzed ring-opening reactions of methylenecyclopropanes with diphenylphosphine oxide in the presence of sulfur or selenium Min Shi,* Min Jiang and Le-Ping Liu State
Supplement: Intramolecular N to N acyl migration in conformationally mobile 1 -acyl-1- systems promoted by debenzylation conditions (HCOONH 4
Cent. Eur. J. Chem. 9(5) 2011 S164-S175 DI: 10.2478/s11532-011-0082-y Central European Journal of Chemistry Supplement: Intramolecular to acyl migration in conformationally mobile 1 -acyl-1- benzyl-3,4
Supporting Information
Supporting Information Wiley-VC 007 9 Weinheim, Germany ew ear Infrared Dyes and Fluorophores Based on Diketopyrrolopyrroles Dipl.-Chem. Georg M. Fischer, Dipl.-Chem. Andreas P. Ehlers, Prof. Dr. Andreas
Supporting Information
S1 Supporting Information Benzannulation from Alkyne without tallic Catalysts at Room Temperature to 100 o C Tienan Jin,* Fan Yang and Yoshinori Yamamoto* Department of Chemistry, Graduate School of Science,
KOtBu-Mediated Stereoselective Addition of Quinazolines to. Alkynes under Mild Conditions
KOtBu-Mediated Stereoselective Addition of Quinazolines to Alkynes under Mild Conditions Dan Zhao, Qi Shen, Yu-Ren Zhou, and Jian-Xin Li* State Key lab of Analytical Chemistry for Life Science, School
Supporting Information
Electronic Supplementary Material (ESI) for ChemComm. This journal is The Royal Society of Chemistry 15 Supporting Information For Visible-light-induced photocatalytic oxytrifluoromethylation of -allylamides
Supplementary Material ON WATER REACTIVITY AND REGIOSELECTIVITY OF QUINONES IN C-N COUPLING WITH AMINES
10.1071/CH13355_AC CSIRO 2014 Australian Journal of Chemistry 2014, 67(2), 217-224 Supplementary Material ON WATER REACTIVITY AND REGIOSELECTIVITY OF QUINONES IN C-N COUPLING WITH AMINES Maximiliano Martínez-Cifuentes,
Supporting Information
S1 Supporting Information Synthesis of 2-Arylated Hydroxytyrosol Derivatives via Suzuki-Myaura Cross-Coupling Roberta Bernini, a Sandro Cacchi, b* Giancarlo Fabrizi, b* Eleonora Filisti b a Dipartimento
Kishore Natte, Jianbin Chen, Helfried Neumann, Matthias Beller, and Xiao-Feng Wu*
Electronic Supplementary Material (ESI) for rganic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 204 Kishore Natte, Jianbin Chen, Helfried Neumann, Matthias Beller, and Xiao-Feng
Enantioselective Organocatalytic Michael Addition of Isorhodanines. to α, β-unsaturated Aldehydes
Electronic Supplementary Material (ESI) for Organic & Biomolecular Chemistry. This journal is The Royal Society of Chemistry 2016 Enantioselective Organocatalytic Michael Addition of Isorhodanines to α,
Supporting Information
Electronic Supplementary Material (ESI) for rganic Chemistry Frontiers. This journal is the Partner rganisations 2018 Palladium-catalyzed direct approach to α-cf 3 aryl ketones from arylboronic acids Bo
Supporting Information. Copyright Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, 2006
Supporting Information Copyright Wiley-VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, 2006 1 A Facile Way to Synthesize 2H-Chromenes: Reconsideration of the Reaction Mechanism between Salicylic Aldehyde and